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101	Author	R. Kipka, Hk Müller-Buschbaum	Requires cookie*
	Title	Über Oxocuprate, XVI Ba9Cu7015Cl2 mit Cu 2+ in neuer Koordination About Oxocuprates, XVI Ba9Cu7015Cl2 with Cu 2+ in a New Coordination
	Abstract	Single crystals of BagC^OisC^ were prepared and investigated by X-ray diffraction methods. They crystallize with hexagonal symmetry (a =1125.7; c = 585.3 pm, Space group D\|h-P6/mmm). Cu 2 + has the well-known square 0 2--coordination. The squares are connected to rings of 6-fold symmetry. Another Cu 2+ has a so for unknown coordination of 12 0 2 ~-neighbours. The differences in respect of other oxohalogenocuprates are discussed.
	Reference	(Z. Naturforsch. 31b, 1067—1069 [1976]; eingegangen am 24. März 1976)
	Published	1976
	Keywords	Barium, Copper Oxide Chloride, Crystal Structure
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-1067.pdf
	Identifier	ZNB-1976-31b-1067
	Volume	31

102	Author	Jürgen Weis, Herbert Schäfer, Günter Schön	Requires cookie*
	Title	Neue ternäre Telluride und Selenide der Alkalimetalle mit Elementen der 3. Hauptgruppe New Ternary Element(I)/Element(III)-Tellurides and Selenides
	Abstract	The new ternary compounds NaAlSe2, NaAlTe2, NaGaTe2 and KAlTe2 crystallize in the Tl I Tl III Se2-structure type. The analogous Tl-compounds build up the same structure but show a variable composition within the limits (NaJTli_a.)TlSe2 (Oca; <0.47) and (Ka.Tli_jr)TlSe2 (0 <x <0.56). The compounds KAlSe2, KGaSe2, KInSe2 and KGaTe2 crystallize in a new structure type.
	Reference	(Z. Naturforsch. 31b, 1336—1340 [1976]; eingegangen am 5. Juli 1976)
	Published	1976
	Keywords	Ternary Tellurides, Ternary Selenides, Crystal Structure
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-1336.pdf
	Identifier	ZNB-1976-31b-1336
	Volume	31

103	Author	Brigitte Eisenmann, Gerhard Savelsberg, Herbert Schäfer	Requires cookie*
	Title	Zur Darstellung und Kristallstruktur von Na2CuAs, K2CuAs und K2CuSb Preparation and Crystal Structure of Na2CuAs, K2CuAs and K2CuSb
	Abstract	The three new compounds crystallize orthorhombic, space group Cmcm with Na2CuAs: a = 8.86(2) A, b = 7.22(2) A, c = 5.34(2) A; K2CuAs: a = 10.02(2) A, b = 7.56(2) A, c = 5.89(2) A; KsCuSb: a = 10.50(2) A, b = 7.93(2) A, c = 6.23(2) A. There are Cu-E(V)-Cu-E(V)-zigzag-chains in the structure, in which the Cu-atoms are linearly bonded to the E(V)-atoms.
	Reference	(Z. Naturforsch. 31b, 1344—1346 [1976]; eingegangen am 15. Juli 1976)
	Published	1976
	Keywords	Intermetallic Compounds, Crystal Structure, Ternary Arsenides, Ternary Antimonides
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-1344.pdf
	Identifier	ZNB-1976-31b-1344
	Volume	31

104	Author	Helmut Rieskamp, Rainer Mattes	Requires cookie*
	Title	Fluorreiche Oxofluorovanadate(V): Die Kristallstruktur von [enH2] [VOF5]
	Abstract	The crystal structure of triclinic [enH2][VOF5], prepared in aqueous solution, has been determined from X-ray diffractometer data (i? = 0.076 for 527 reflections). The structure contains monomeric [VOFs] 2--ions. The bond distances are 1.54(1) Ä (terminal oxygen), 1.80(1) (average for the cis-fluorine atoms) and 2.10(1) Ä for the fluorine atom in trans-position to the terminal oxygen atom. This fluorine atom is involved in strong hydrogen bonds originating from the [NHaCH^CH^NEy 2 " 1 -cation with cisoid conformation. Earlier results about the existence of K2VOF5 could not be confirmed.
	Reference	(Z. Naturforsch. 31b, 1453—1455 [1976]; eingegangen am 2. August 1976)
	Published	1976
	Keywords	Oxopentafluorovanadates(V), Crystal Structure, Vibrational Spectra
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-1453.pdf
	Identifier	ZNB-1976-31b-1453
	Volume	31

105	Author	Gerhard Cordier, Herbert Schäfer	Requires cookie*
	Title	Neue intermetallische Verbindungen im arcJi-Ce202S-Strukturtyp New Intermetallic Compounds in the awfa"-Ce202S-Structure Type
	Abstract	The new intermetallic compounds CaMn2Sb2, SrMn2Sb2 and CaMn2Bi2 have been prepared and structurally characterized. They are isotypic and crystallize trigonal in the an^-Ce202S-structure with the lattice constants: CaMn2Sb2: a = 4.54(1), c = 7.48(1), c/a = 1.65. SrMn2Sb2: a = 4.56(1), c = 7.70(1), c/a = 1.69. CaMn2Bi2: a = 4.63(1), c = 7.64(1), c/a = 1.65.
	Reference	(Z. Naturforsch. 31b, 1459—1461 [1976]; eingegangen am 13. August 1976)
	Published	1976
	Keywords	Intermetallic Compounds, Crystal Structure, Ternary Antimonides, Ternary Bismutides
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-1459.pdf
	Identifier	ZNB-1976-31b-1459
	Volume	31

106	Author	Z. Naturforsch	Requires cookie*
	Title	Sr3In2P4 und Ca3ln2As4, Zintlphasen mit Bänderanionen aus kanten-und ecken verknüpften InP4-bzw. InAs4-Tetraedern
	Abstract	The new com pounds Sr3In2P4 and Ca3In2A s4 crystallize in the orthorhom bic system , space group Pnnm (N o. 58), with the follow ing lattice constants: Sr3In,P4: a = 1632.3(6), b = 682.8(3), c = 428.9(2); Ca3In2A s4: a = 1621.2(6), b = 659.5(3), c -430.6(2). In the anionic partial lattice InP4 (In A s4) tetrahedra are connected by com m on edges and corners and form (InP21-)" ((In A s23_)") strings o f alternating four-m em bered and eight-m em -bered rings.
	Reference	Z. Naturforsch. 41b, 1416 (1986); eingegangen am 14. Juli 1986
	Published	1986
	Keywords	Interm etallic C om pounds, Zintl Phases, Crystal Structure
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	TEI-XML for	default:Reihe_B/41/ZNB-1986-41b-1416.pdf
	Identifier	ZNB-1986-41b-1416
	Volume	41

107	Author	Petra Prokop, Rainer Richter, Lothar Beyer	Requires cookie*
	Title	Zur Reaktion von 2,4-Dioxo-4-ferrocenyl-butansäureethylester mit primären aromatischen Aminen On the Reaction of Ethyl 2,4-Dioxo-4-ferrocenyl-butanoate with Primary Aromatic Amines
	Abstract	Starting from ethyl 2,4-dioxo-4-ferrocenyl-butanoate (1) a series of new ferrocene derivatives has been prepared. While the reaction with o-phenylene diamine leads to two ferrocene-con taining heterocyclic compounds, 4-ferrocenyl-3//-l,5-benzodiazepine-2-carbonic acid ethyl ester (3) and 3-(2-ferrocenyl-2-oxo-ethylidene)-3,4-dihydro-l//-quinoxalin-2-one • H20 (4), reactions with m-and /?-phenylene diamine give both the mono-and disubstituted products 5 -8, respectively. The conversion of 4 by Lawesson's reagent results in 2-ferrocenvl-thieno[2,3-b]quinoxaline (9). The new compounds have been characterized by their 'H , 1 C NMR, and mass spectra. The molecular structures of 4-ferrocenyl-4-oxo-2-phenylamino-but-2-enoic acid ethyl ester 2, and of 4 and 9 have been determined by X-ray crystal structure analysis.
	Reference	Z. Naturforsch. 54b, 849—857 (1999); eingegangen am 12. März 1999
	Published	1999
	Keywords	Ferrocene, /3-Diketones, Enaminoketones, NMR Data, Crystal Structure
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	TEI-XML for	default:Reihe_B/54/ZNB-1999-54b-0849.pdf
	Identifier	ZNB-1999-54b-0849
	Volume	54

108	Author	Tsutomu Okuda, Yoshihiro Kinoshita, Hiromitsu Terao, Koji Yamada	Requires cookie*
	Title	Structure and Bonding of Bromoantimonate (III) Complexes with Unusual Valency by Means of NQR and Powder X-Ray Diffraction
	Abstract	NQR and powder X-ray diffraction were observed for several bromoantimonate (III) complexes which contain C"H2n+ jNF^ (n = 1 -3) or (C"H2lt + 1)2N H 2 (n = 1 -4) as a cation. The bond character, anion structure, crystal structure, and phase transition are discussed on the basis of the three-center-four-electron bond. A good correlation was found between the halogen NQR frequency and the Sb-X bond length.
	Reference	Z. Naturforsch. 49a, 185—192 (1994); received July 23 1993
	Published	1994
	Keywords	81Br NQR, Temperature dependence, Phase transition, Crystal structure
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	TEI-XML for	default:Reihe_A/49/ZNA-1994-49a-0185.pdf
	Identifier	ZNA-1994-49a-0185
	Volume	49

109	Author	Jacek Zaleski	Requires cookie*
	Title	Crystal Structure and Phase Transitions of [C(NH2)3]3Sb2C l9 * 0.9 H 20 A dam Pietraszko
	Abstract	The room temperature structure of [C(NH2)3]3Sb2C l9 ■ 0.9 H 20 (GNCA) was solved. It crystal lizes in the monoclinic C2/c space group with a = 15.275, b = 8.794, c = 17.904 (in Ä), ß = 96.40°, V = 2390 Ä 3, Z = 4. Refinement of the atomic parameters by a least squares methods gave R = 0.042, wR = 0.039 for 1958 reflections with F>4ct(F). The structure consists of polyanionic (Sb2Cl\|_)n layers built of deformed corner connected SbX^-octahedra. Two crystallographically inequivalent guanidinium cations are present, one situated between polyanionic layers, the other one together with a disordered water molecule inside cavities formed by polyanions. Temperature X-ray scattering experiments together with DSC studies were carried out above room temperature. Temperature dependence of the lattice parameters between 300 K and 380 K was determined and a phase transition of mixed order at 364 K was revealed.
	Reference	Z. Naturforsch. 49a, 895—901 (1994); received June 7 1994
	Published	1994
	Keywords	Guanidinium, Chloroantimonate, Crystal structure, Phase transition, DSC
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	TEI-XML for	default:Reihe_A/49/ZNA-1994-49a-0895.pdf
	Identifier	ZNA-1994-49a-0895
	Volume	49

110	Author	Hiroyuki Ishida, Hironobu Maeda, Akiko Hirano, Tamotsu Fujimoto, Yoshihiro Kubozono, Setsuo Kashino, Shuichi Emura	Requires cookie*
	Title	E X A F S S tu d y o n th e P h a s e T r a n s itio n ( P h a s e a ' -5) in C H 3 N H 3 I
	Abstract	The local structure of CH3NH3I around the I" ion in Phase a 'and 8 was studied by iodine K-edge EXAFS. The crystal structure in Phase a ' was redetermined by single crystal X-ray diffraction. The Debye-Waller factor <r(2) derived from EXAFS spectra shows an anomalous behavior around the order-disorder transition temperature from Phase 8 to a '. The phase transition has been interpreted as the disordering process which involves not only the H atoms but also the C atoms in the cation.
	Reference	Z. Naturforsch. 50a, 876—880 (1995); received June 16 1995
	Published	1995
	Keywords	Crystal structure, EXAFS, Phase transition, X-ray diffraction
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	TEI-XML for	default:Reihe_A/50/ZNA-1995-50a-0876.pdf
	Identifier	ZNA-1995-50a-0876
	Volume	50

111	Author	Hiroyuki Ishida, Hiroshi Ono, Ryuichi Ikeda	Requires cookie*
	Title	Crystal Structure of the High-temperature Solid Phases of Choline Tetrafluoroborate and Iodide
	Abstract	The crystal structure of the highest-and second highest-temperature solid phases of choline tetrafluoroborate and iodide was determined by X-ray powder diffraction. The structure in the highest-temperature phase of both salts is NaCl-type cubic (a = 10.16(2) Ä, Z = 4 for tetrafluorobo-rate; a = 10.08(2) A, Z = 4 for iodide). The second highest-temperature phase of tetrafluoroborate and iodide is CsCl-type cubic (a = 6.198(6) Ä and Z = 1) and tetragonal (a = 8.706(2) A, c = 6.144(6) Ä, and Z = 2), respectively. DSC was carried out for the iodide, where the presence of three solid-solid phase transitions was confirmed. Enthalpy and entropy changes of these transitions were evaluated.
	Reference	Z. Naturforsch. 52a, 679—680 (1997); received June 17 1997
	Published	1997
	Keywords	Crystal structure, Powder X-ray diffraction, Phase transition
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	TEI-XML for	default:Reihe_A/52/ZNA-1997-52a-0679_n.pdf
	Identifier	ZNA-1997-52a-0679_n
	Volume	52

112	Author	J. Pirnat, Z. Trontelj, Z. Jagličić, K. Lutar, H. Borrmann	Requires cookie*
	Title	Arsenic NQR in the Paramagnetic Complex Co(AsF 6 ) 2 -2AsF 3
	Abstract	Arsenic NQR in Co(AsF 6) 2 .2AsF 3 reveals three lines: one near 122 MHz and two near 50 MHz. Relations of the spectral lines to the structure and to thermal vibrations are discussed. Possible influence of paramagnetic Co is examined.
	Reference	Z. Naturforsch. 55a, 212—214 (2000); received October 13 1999
	Published	2000
	Keywords	Co(AsF 6 ) 2, Complex, NQR, Paramagnet, Crystal Structure
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	TEI-XML for	default:Reihe_A/55/ZNA-2000-55a-0212.pdf
	Identifier	ZNA-2000-55a-0212
	Volume	55

113	Author	Hideta Ishihara, Keizo Horiuchi, ThorstenM. Gesing, Shi-Qi Dou, J.-Christian Buhl, Hiromitsu Terao	Requires cookie*
	Title	I NQR and Crystal Structure Studies of [N(CH 3 ) 4 ] 2 CdI 4
	Abstract	The temperature dependence of 127 1 NQR and DSC as well as the crystal structure at room temperature of the title compound were determined. This compound shows a first-order phase transition of an order-disorder type at 245 K. Eight 127 I(i^i: m = ±5 <-+ ±\|) NQR lines of 79. corresponding eight 127 I(^ 2 : m = ±\| <-» • ±\|) NQR lines were observed at liquid nitrogen temperature. Three 127 I(^i) NQR lines wfth an intensity ratio of 1:1:2 in the order of decreasing frequency were observed just above the transition point and two NQR lines except for the middle-frequency line disappeared around room temperature. This temperature behavior of NQR lines is very similar to that observed in [N(CH 3)4] 2 Hgl4. Another first-order phase transition takes place at 527 K. The structure of the room-temperature phase was redetermined: orthorhombic, Pnma, Z = 4, a = 1342.8(3), b = 975.7(2), c = 1696.5(3) pm. The NQR result of three lines with an intensity ratio of 1:1:2 is in agreement with this structure. The thermal displacement parameters of atoms in both cations and anions are large.
	Reference	Z. Naturforsch. 55a, 225—229 (2000); received October 13 1999
	Published	2000
	Keywords	NQR, DSC, Crystal Structure, Phase Transition
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	TEI-XML for	default:Reihe_A/55/ZNA-2000-55a-0225.pdf
	Identifier	ZNA-2000-55a-0225
	Volume	55

114	Author	W. Haase, R. Mergehenn, W. Krell	Requires cookie*
	Title	Die Kristallstruktur von Thiocyanato(2-dimethylaminoäthanolato)kupfer(II) The Crystal Structure of Thiocyanato(2-dimethylaminoethanalato)copper(II)
	Abstract	The crystal structure of the title compound has been determined from three-dimensional X-ray diffractometer data. Crystals are monoclinic, space group P2i/c with 8 CU(C4HIONO)SCN units in a cell of dimensions a = 11.951(4), b = 8.954(3), c = 16.805(6) Ä, and ß = 107.5(1)°. The structure was refined by least squares techniques to a final discrepancy factor of 0.041 based on 2234 observed independent reflexions. The compound is polymeric with copper atoms alternately bridged by two oxygen atoms and two thiocyanato groups. The coordination geometry around each copper atom is distorted square pyramidal. The basal plane consists of the two bridging oxygen atoms (mean value Cu-O: 1.914(3) A), the amino nitrogen atom (mean value Cu—N: 2.035(3) A) and the nitrogen atom from the thiocyanato group (mean value Cu-N: 1.908(3) A) while the axial coordination site is occupied by a sulfur atom from a thiocyanato group (mean value Cu-S: 2.979(2) A) centrosymmetric to the first. The magnetic susceptibility of the compound shows a broad maximum at 200 K.
	Reference	(Z. Naturforsch. 31b, 85—89 [1976]; eingegangen am 25. September 1975)
	Published	1976
	Keywords	Crystal Structure, Copper Compound, Thiocyanato Bridging, Spin Coupling
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-0085.pdf
	Identifier	ZNB-1976-31b-0085
	Volume	31

115	Author	Klaus-Jürgen Range, Richard Leeb	Requires cookie*
	Title	Preparation and Crystal Structure of the High Pressure Phase Tm 2 S3-II
	Abstract	Single crystals of the quenchable high pressure phase Trri2S3-II were grown from a TmJ3-flux at 10 kbar, 1600 °C. The crystals are monoclinic, space group P2i/m, with a = 11.110(5) A, 6 = 3.874(3) A, c = 10.872(5) A, ß = 108.88(2) ° and Z = 4. In Tm2S3-II, which is isotypic with Er3ScS6, the four independent thulium atoms are coordinated by six (2 x), seven and eight sulfur atoms.
	Reference	(Z. Naturforsch. 31b, 311—314 [1976]; eingegangen am 7. November 1975)
	Published	1976
	Keywords	Thulium Sesquisulfide, High Pressure Phase, Crystal Structure
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-0311.pdf
	Identifier	ZNB-1976-31b-0311
	Volume	31

116	Author	Bernd Grande, Hanskarl Müller-Buschbaum	Requires cookie*
	Title	Über Oxocuprate, XIV Zur Kristallchemie von Sr2Cu304Cl2 On Oxocuprate, XIV On the Crystal Chemistry of Sr2Cu304Cl2
	Abstract	The new compound Sr2Cu304Cl2 was prepared in melts of SrCl2. A single crystal X-ray examination (a = 546.2, c= 1259.1 pm, space group D^-14/mmm) shows that the octahedral distortion of the [Cu304Cl2] 4 ~-network cannot be explained only by the JAHN-TELLER effect.
	Reference	(Z. Naturforsch. 31b, 405—407 [1976]; eingegangen am 24. November 1975)
	Published	1976
	Keywords	Strontium, Copper, Oxide Chloride, Crystal Structure, Coordination
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-0405.pdf
	Identifier	ZNB-1976-31b-0405
	Volume	31

117	Author	K. Diehl, D. Khodadadeh, J. Kummer, Strähle	Requires cookie*
	Title	L
	Abstract	Upon use of a synthetic method reported earlier by us respective alloys of Na/Sn, Na/Ge and Na/Sb are dissolved in ethylene-diamine and the title compounds precipitated from the solutions in high yield. By recrystal-lisation well shaped, stable crystals are obtain-ed. The crystal structure of [Na4 • 7 en]Sn9 confirms the presence of a Sn9 4 ~-polyhedron which had been suggested by us on the basis of other investigations. The Sn9 4_ -polyhedron may be described as a distorted tricapped trigonal prism. Ethylenediamine is coordi-nated to Na+-ions exclusively.
	Reference	(Z. Naturforsch. 31b, 522—524 [1976]; eingegangen am 16. Februar 1976)
	Published	1976
	Keywords	Polyanionic Compounds, Germanium, Tin, Antimony, Crystal Structure
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	TEI-XML for	default:Reihe_B/31/ZNB-1976-31b-0522_n.pdf
	Identifier	ZNB-1976-31b-0522_n
	Volume	31

118	Author		Requires cookie*
	Title	Röntgenographische Strukturuntersuchung von Cäsiumhexaoxo-tetrahydroxo-pentaborat-2-dimethylsulfoxid X-ray Study of the Structure of Cesiumhexaoxo-tetrahydroxo-pentaborate-2-dimethyl Sulfoxide
	Abstract	The compound Cs[Bs0 6 (OH)4 ] • 2 DMSO was prepared by hydrolysis of tris(methoxy)-borane in organic solvents with small amounts of water in presence of cesium ierf-butylate and recrystallized in DMSO (dimethyl sulfoxide). Cs[Bs0 6 (0 H)4 ] • 2 DMSO crystallizes in the monoclinic space group P2i/a with a = 9.593(2), 6 = 19.179(4), c = 11.585(2) Ä, ß = 119.99(2)° and Z — 4. The crystal structure was determined by single-crystal diffracto meter data and refined to a conventional R value of 9.9%. The crystal structure consists of chains of pentaborate anions [Bs0 6 (OH)4 ]-linked by hydrogen bonds. The cesium cation and the DMSO molecules join the chains to sheets by coordination and hydrogen bonds respectively.
	Reference	(Z. Naturforsch. 32b, 268—274 [1977]; eingegangen am 4. November/7. Dezember 1976)
	Published	1977
	Keywords	X-ray, Crystal Structure, Isopolyanions, Polyborates
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	TEI-XML for	default:Reihe_B/32/ZNB-1977-32b-0268.pdf
	Identifier	ZNB-1977-32b-0268
	Volume	32

119	Author	W.	Requires cookie*
	Title	Preparation and Crystal Structure of Li2Sb
	Reference	(Z. Naturforsch. 32b, 357—359 [1977]; eingegangen am 3. Dezember 1976)
	Published	1977
	Keywords	Lithium Antimonide, Intermetallic Compound, Crystal Structure
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	Identifier	ZNB-1977-32b-0357_n
	Volume	32

120	Author		Requires cookie*
	Title
	Abstract	G e r h a r d C o r d i e r u n d H e r b e r t S c h ä f e r BaMnSb2, SrMnBi2 and BaMnBi2 have been prepared and structurally characterized. The new compounds are isotypic and crystallize tetragonal in the SrZnBi2 structure with the following constants: BaMnSb2: a = 4.53 ± 0.01 A, c = 24.34 ± 0.03 A, c/a = 5.37. SrMnBi2: a = 4.58 ± 0.01 A , c = 23.13 ± 0.03 A, c/a = 5.05. BaMnBi2: a — 4.63 ± 0.02 A, c = 24.22 i 0.05 A, c/a = 5.23. The transition metal atoms form together with the semimetal atoms sheets of tetragonal pyramids separated by double layers of alkali earth atoms. In these double layers there are inserted Bi/Sb-square nets.
	Reference	(Z. Naturforsch. 32b, 383—386 [1977]; eingegangen am 29. Dezember 1976)
	Published	1977
	Keywords	Intermetallic Compounds, Crystal Structure, Ternary Antimonides, Ternary Bismutides
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	TEI-XML for	default:Reihe_B/32/ZNB-1977-32b-0383.pdf
	Identifier	ZNB-1977-32b-0383
	Volume	32

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