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'Triketohydrinden' in keywords Facet   Publication Year 1993  [X]
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1993[X]
1Author    Hans-Jörg Hemmerling, Margarete Janoschka, Hartmut WunderlichRequires cookie*
 Title    Amidinadditionsprodukte des 1,2,3-Indantrionhydrats: Synthese und Strukturzuordnung durch Kristallstrukturanalyse, spektrale Daten und Blei(IV)acetatoxidation Products o f Am idinaddition to 1,2,3-Triketohydrindenhydrat: Synthesis and Determination by Crystal Structure, Spectral Data and Oxidation with Lead(IV)acetate  
 Abstract    The addition o f amidines to 1,2,3-triketohydrindenhydrat gives cyclic dihydroxyindenoimi-dazoles. From N-substituted amidines mixtures o f regioisomeric derivatives were obtained. Analysis o f crystals revealed the major product o f 2 k to be 4 k. They belong to the monoclinic space group P 2 ,/c (a = 889.1(2); b = 1186.6(3); c = 2783.5(7) pm; ß = 91.26(2)°) with Z = 8 molecules including four molecules o f ethanole per unit cell. These results were confirmed by oxidation with lead(IV)acetate, which lead to derivatives o f isoindols. 
  Reference    Z. Naturforsch. 48b, 1094—1104 (1993); eingegangen am 26. März 1993 
  Published    1993 
  Keywords    Indeno[l, 2-d]im idazoles, Triketohydrinden, Crystal Structure, Amidines, Isoindoles 
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 TEI-XML for    default:Reihe_B/48/ZNB-1993-48b-1094.pdf 
 Identifier    ZNB-1993-48b-1094 
 Volume    48