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1998 (1)
1Author    Z. NaturforschRequires cookie*
 Title    Kristallstruktur  
 Abstract    von [Mo(CO)3(NCMe)(SrBu)]2 C ry stal S tru c tu re o f [M o (C O)3(N C M e)(S rB u)]2 M ike R. K opp, B e rn h a rd N eu m ü ller* Single crystals of [M o(CO)3(NCM e)(S'Bu)]2 (1) and [{Mo(CO)3}2{Mo(CO)2}{S'Bu}4] (2) were obtained by the reaction of [M o(CO)3(NCM e)3] with [(PhCH2)2GaS'Bu]2 in 1,4-dio-xane. The X-ray structure determination of 1 showed the presence of a Mo2S2 four-membe-red ring with a Mo-Mo bond length of 296,7(1) pm. Space group Pbca, Z = 4, lattice dim en­ sions at -80 °C: a = 1588,2(3), b = 905,8(1), c = 1676,0(1) pm, R y = 0,0555. 
  Reference    Z. Naturforsch. 53b, 378—380 (1998); eingegangen am 8. Dezember 1997 
  Published    1998 
  Keywords    Molybdenum Carbonyl Complex, Thiolato Complex, Crystal Structure 
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 TEI-XML for    default:Reihe_B/53/ZNB-1998-53b-0378.pdf 
 Identifier    ZNB-1998-53b-0378 
 Volume    53