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Facet   Publication Year 1997  [X]
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1997[X]
1Author    Olaf Reckeweg, H.-Jürgen MeyerRequires cookie*
 Title    Unsymmetrische BN23'-Ionen in den Strukturen von Ca2ClBN2 und Sr2ClBN2. Unsymmetric BN23~-Ions in the Structures of Ca2ClBN2 and Sr2ClBN2  
 Abstract    The new compounds Ca2ClBN2 (1) and Sr2ClBN2 (2) were prepared from the respective metal, its dihalide and h-BN in sealed tantalum ampoules at 1200 °C. The crystals obtained were transparent yellow (1) and blue (2), respectively. The crystal structures were determined from single crystal X-ray data. Ca2ClBN2 and Sr2ClBN2 are isotypic and crystallize in the orthorhombic space group Pnma (No. 62), Z = 4 (Ca2ClBN 2: a = 1166.7(2), b = 390.26(4), c = 899.8(1) pm, R 1 = 0.043, wR2 = 0.115 for 554 independent reflections; Sr-,C1BNT: a = 1242.8(1), b = 416.75(4), c = 920.8(1) pm, R\ = 0.031, wR2 = 0.054 for 6 6 2 'independent reflections). The structures contain two different layers of M 2+, C P and BN23~ alternating along the [010] direction. The bond angles N-B-N are 177.2(4)° for (1) and 176,6(5)° for (2), the bond distances of the BN23_ ions are dB_ N] = 134.6(5) pm for (1), 136,3(7) pm for (2) and dg_N2 = 132.4(5) pm for (1) and 131,3(7) pm for (2). The unsymmetric structure of the BN23~ ion, as is manifested particularly in the Sr compound (2), is caused by the coordination of N 1 to four cations while N2 is coordinated only to three. 
  Reference    Z. Naturforsch. 52b, 340—344 (1997); eingegangen am 12. November 1996 
  Published    1997 
  Keywords    Boronitrides, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0340.pdf 
 Identifier    ZNB-1997-52b-0340 
 Volume    52 
2Author    K. Bluhm, C. H. ParkRequires cookie*
 Title    Die Synthese und Kristallstruktur des Borat-Phosphats: a -Zn3(B0 3)(P04) Synthesis and Crystal Structure of the Borate-Phosphate: Q-Zn3(B 0 3)( P 0 4)  
 Abstract    Single crystals of the compound a -Z n 3(B 0 3)(P 0 4) were obtained at 1050 °C by using B20 3, P20 5 and Z n C 0 3 as starting materials and subsequent cooling to 600°C with 20°C/h. X-ray investigations on single crystals yield a new crystal structure in the monoclinic space group Cm -(Nr. 8) with a = 972.5(2); b = 1272.0(3); c = 487.4(3) pm; 0 = 1 1 9 .8 0 (4)°; Z = 4. The structure contains isolated trigonally planar B 0 3 and tetrahedral P 0 4 units which are not joined together. Zinc occupies three crystallographically different point positions and is trigonal-bipyramidally, tetragonal-pyramidally or distorted tetrahedrally coordinated by oxygen. 
  Reference    (Z. Naturforsch. 52b, 102—106 [1997]; eingegangen am 16. August 1996) 
  Published    1997 
  Keywords    Zinc, Borate, Phosphate, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0102.pdf 
 Identifier    ZNB-1997-52b-0102 
 Volume    52 
3Author    Z. NaturforschRequires cookie*
 Title      
 Abstract    Single crystals of (Me3Sn)3CCN were obtained by the reaction of tris(trimethylstannyl)amine with boiling acetonitrile in the presence of potas­ sium fluoride and trimethylarsane. The compound has been characterized by IR spectroscopy and by a crystal structure determination. Space group 
  Reference    Z. Naturforsch. 52b, 145—148 (1997); eingegangen am 7. Oktober 1996 
  Published    1997 
  Keywords    Tin Compound, Synthesis, IR Spectra, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0145_n.pdf 
 Identifier    ZNB-1997-52b-0145_n 
 Volume    52 
4Author    Borate Anion, A. Wiesch, K. BluhmRequires cookie*
 Title    AgSrfByO^]: Das erste wasserfreie quaternäre Silber(I)-Borat mit vierfach koordiniertem Silberion und einem neuartigen Boratanion AgSr[B70 12]: The First Anhydrous Quaternary Silver(I)-Borate with Fourfold Coordinated Silver Ion and a New  
 Abstract    Single crystals of AgSr[B70 , 2] were obtained by using a B20 3 flux-technique and Ag2C 0 3 and SrC 03 as starting materials in a silver ampoule at 800 °C. X-ray investigations on single crystals led to the space group C 2/c with a = 664.2(5); b = 1153.6(3); c = 2198.0(6) pm; ß = 92,52(3)°; Z = 8. Ag+ is fourfold coordinated by oxygen atoms and forms distorted A g04 tetrahedra while Sr2+ has nine nearest neighbours. The compound contains a hitherto unknown two dimensional borate anion [B70 i 2]3-which contains four trigonal planar B 0 3 groups and three B 0 4 tetrahedra per unit. 
  Reference    Z. Naturforsch. 52b, 227—230 (1997); eingegangen am 9. September 1996 
  Published    1997 
  Keywords    Silver, Strontium, Borate, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0227.pdf 
 Identifier    ZNB-1997-52b-0227 
 Volume    52 
5Author    Matthias Krieger3, Klaus Harms3, Jörg Magullb, Kurt Dehnicke3Requires cookie*
 Title    Phosphanimin-und Phosphaniminato-Komplexe des  
 Abstract    Zinks. Kristallstrukturen von [ZnCl2(Me3SiNP(CH2)4CMe3)]2, [ZnI2(Me3SiNPEt3)]2, [ZnI2{Me2Si(NPEt3)2 }] und [ZnBr(NPMe3)]4 CH2Cl2 Phosphaneimine and Phosphoraneiminato Complexes of Zinc. Crystal Structures of [ZnCl2(M e3SiNP(CH2)4CM e3)]2, [ZnI2(Me3SiNPEt3)]?, [Znl2{Me2Si(NPEt3)2}], and [ZnBr(NPMe3)]4 CH2Cl2 The donor-acceptor complexes [ZnCl2(Me3SiNP(CH2)4CMe3)]2 (l)and [ZnI2(Me3SiNPEt3)]2 (2) have been prepared from the zinc dihalides and the corresponding silylated phosphaneimi-nes in CH2C12. Thermolysis of 2 leads to the formation of [ZnI2(Me2Si(NPEt3)2)] (3). Znl2 and ZnBr2 react with the silylated phosphaneimines Me3SiNPR3 (R = Me, Et) in the presence 
  Reference    Z. Naturforsch. 52b, 243—250 (1997); eingegangen am 1. August 1996 
  Published    1997 
  Keywords    Zinc Compounds, Phosphoraneiminato Complexes, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0243.pdf 
 Identifier    ZNB-1997-52b-0243 
 Volume    52 
6Author    W. SchnickRequires cookie*
 Title    Synthesen, Kristallstrukturen und Eigenschaften von Trisilber-und Trikalium-tri-/x-imido-cyclotriphosphat, Ag3(P 0 2NH)3 und K3(P 0 2NH)3 Syntheses, Crystal Structures, and Properties of Trisilver and Tripotassium Tri-^-im ido Cyclotriphosphate, Ag3(P 0 2N H)3 and K3(P 0 2N H)3 N. Stock  
 Abstract    Coarse crystalline Ag3(P 0 2NH)3 (1) and K3(P 0 2NH)3 (2) are obtained by addition of an aqueous solution of A gN 03 to an acidified solution of Na3(P 0 2NH)3 • 4H20 and by diffusion controlled addition of ethanol to a solution of K3(P 0 2NH)3 in water, respectively. The crystal structures of 1 and 2 have been determined by single crystal X-ray methods (Ag3(P 0 2NH)3: P2,/c; a = 1166.6(1), b = 786.4(1), c = 997.8(1) pm, ß = 106.91(1)°; Z = 4. K3(P 0 2NH)3: R3; a = 1271.4(2), c = 1017.9(2) pm, Z = 6). In Ag3(P 0 2NH)3 the cyclic anion is markedly distorted because of interactions between Ag+ and one nitrogen atom of the anion. In K3(P 0 2NH)3 the trimetaphosphimate ring shows a chair conformation and two cyclic anions are connected to each other by hydrogen bonds. DTA/TG investigations show thermal decomposition above 275 and 250 °C for 1 and 2, respectively. 
  Reference    Z. Naturforsch. 52b, 251—255 (1997); eingegangen am 14. November 1996 
  Published    1997 
  Keywords    Trimetaphosphimate, Synthesis, Crystal Structure, Thermal Property 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0251.pdf 
 Identifier    ZNB-1997-52b-0251 
 Volume    52 
7Author    SvitlanaR. Petrusenkoa, Joachim Sielerb, VladimirN. Kokozay3 'Requires cookie*
 Title    Direct Synthesis of Zinc and Nickel(II) Complexes with l,4-Diazabicyclo[2.2.2]octane  
 Abstract    The peculiarities of the formation of zinc and nickel(II) complexes by interaction of metal powder or metal oxide with ammonium salts (halides, nitrate, thiocyanate) were investigated in non-aqueous solutions (methanol, acetonitrile, N,N-dimethylformamide=DMF, dimethylsulf-oxide=DMSO) in presence of l,4-diazabicyclo[2.2.2]octane. The stoichiometry of the com ­ plexes was found to depend on the initial reagent ratio Ni/ZnOiNfLX and Ni/ZnO:Ten. The compounds of compositions Z n(H Ten)(H 20)(N 03)3 and Ni(HTen)(Ten)Cb were character­ ized by X-ray crystallography. Both complexes contain five-coordinate metal atoms. The zinc compound possesses monomeric molecular structure whilst the nickel complex is polymeric. 
  Reference    Z. Naturforsch. 52b, 331—336 (1997); received July 30 1996 
  Published    1997 
  Keywords    Synthesis, Zinc, Nickel(II), Triethylenediamine, X-Ray 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0331.pdf 
 Identifier    ZNB-1997-52b-0331 
 Volume    52 
8Author    Stefan Horstmann, Wolfgang SchnickRequires cookie*
 Title    Synthese, Kristallstruktur und Eigenschaften von 1,1,3,3,3-Pentaamino- l-th io -l A \3 A 5-diphosphaz-2-en (NH2)2P(S)N=P(NH2)3 Synthesis, Crystal Structure, and Properties of 1,1,3,3,3-Pentaam ino-l-thio-l A5,3A5-diphosphaz-2-ene (N H 2)2P(S)N =P(NH 2)3  
 Abstract    (NH2)2P(S)N=P(NH2)3 has been prepared by a two step synthesis. Suitable single crystals were obtained from an acetonitrile solution in a temperature gradient between 60 °C and room temperature. The crystal structure of (NH->)tP(S)N=P(NH->)3 has been determined by single cry­ stal X-ray methods (P2,/c, a = 9 9 8 .2 7 (9)> '= 762.78(8), c = 1007.70(15) pm, ß = 107.340(7)°, Z = 4). In the crystal structure each hydrogen atom is subject to a hydrogen bond. Four N-H -N hydrogen bonding interactions per molecule build up a framework connecting two molecules in eight-membered rings. Each sulfur atom shows six distances N -H -S in the range of weak hydrogen bonding interactions. 
  Reference    Z. Naturforsch. 52b, 490—95 (1997); eingegangen am 18. Dezember 1996 
  Published    1997 
  Keywords    Aminophosphazenes, Synthesis, Crystal Structure, Hydrogen Bonding 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0490.pdf 
 Identifier    ZNB-1997-52b-0490 
 Volume    52 
9Author    A. M. Orgenstern, H. OppermannRequires cookie*
 Title    Untersuchungen zur thermischen Zersetzung von Ammoniumlanthanhalogeniden Investigation on the Thermal D ecom p osition o f A m m onium H alides  
 Abstract    The decomposition equilibria of Ammonium Lanthanum Halides (NH4)2LaX5 were determined by total pressure measurements in a membrane zero manometer. The phases (NH4j2LaX5 decompose in one step to give solid LaX3 and gaseous NH3 and HX. From the decomposition functions the enthalpies of formation and the standard entropies of the phases are derived. ^H £(N H 4)2LaCl5,f,298) = -4 1 1 ,7 ± 2,2 kcal/mol; S°((NH4)2LaCl5,f,298) = 86,7 ± 2,3cal/Kmol; ^H^(NH4)2LaBr5,f,298) = -351,6 ± 3,8 kcal/mol; S°((NH4)2LaBr5,f,298) = 101,1 ± 1,8 cal/Kmol; _}H£(NH4)2LaI"f,298) = -2 6 8 ,9 ± 3,9 kcal/mol; S°((NH4)2LaI5,f,298) = 115,5 ± 4,3 cal/Kmol. 
  Reference    Z. Naturforsch. 52b, 696—706 (1997); eingegangen am 17. Februar 1997 
  Published    1997 
  Keywords    Synthesis, Ammonium Lanthanum Halides, Thermal Decomposition, Thermochemical Data 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0696.pdf 
 Identifier    ZNB-1997-52b-0696 
 Volume    52 
10Author    Hans Hartl, Michael HoyerRequires cookie*
 Title    Synthese und Strukturuntersuchungen von Iodocupraten(I), X V III. Darstellung und Kristallstruktur von PbCu2I4 * 2C H 3CN [1] Synthesis and Structure Investigations of Iodocuprates(I), X V III. Preparation and Crystal Structure of PbCu2I4 * 2C H 3CN [1]  
 Abstract    Single crystals of PbCu2I4-2(CH3CN) are formed by reaction of Pbl2 with Cul in ace-tonitril. The compound crystallizes in the mono­ clinic space group C2/m; a = 1625.8(3), b = 436.6(1), c = 1025.8(2)pm; ß = 94.77(3)°; V = 725.7 pm3 TO6; Z = 2. The crystal structure is built up by chains of trans-edge sharing ^[PbI6/3] octahe-dra and corner sharing ^[CuI-y^CH^CN)] tetra­ hedra connected by common I-I edges. 
  Reference    Z. Naturforsch. 52b, 766—768 (1997); eingegangen am 14. März 1997 
  Published    1997 
  Keywords    Iodometallates, Lead-Copper-Iodide, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0766_n.pdf 
 Identifier    ZNB-1997-52b-0766_n 
 Volume    52 
11Author    P. Schm, O. Bosholm, H. O. Pperm, AnnRequires cookie*
 Title    Untersuchungen zum ternären System Bi/Te/O, II. Thermisches Verhalten und Koexistenzbeziehungen von Bi20 2Te  
 Abstract    Investigations o f the Ternary System Bi/Te/O, II. The Therm al Behaviour and the R elations o f Phase C oexistences o f B i20 2Te The phase Bi20 2Te exists in the pseudobinary system Bi203/Bi2Te3. The thermal behaviour of Bi2Ö2Te was determined by DTA and X-ray analysis: The phase exists up to 620 °C and decomposes into the solid phases Bi12TeO20, Bi10Te2O 19 [1] and liquid BiTe. The relations of the phase coexistences in the pseudobinary system and in the ternary area Bi20 3/Te02/Bi2Te3/Te were investigated by solid state reactions, chemical transport reactions, and by total pressure measurements. 
  Reference    Z. Naturforsch. 52b, 1461—1466 (1997); eingegangen am 2. Oktober 1997 
  Published    1997 
  Keywords    Synthesis, Thermal Properties, Phase Diagram, Chemical Transport Reactions 
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 Identifier    ZNB-1997-52b-1461 
 Volume    52 
12Author    U. Steiner, W. ReicheltRequires cookie*
 Title    Zum System Ca/Mo/O: Phasendiagramm, Synthese und Charakterisierung der ternären Verbindungen On the System Ca/Mo/O: Phase Diagram, Synthesis and Characterization of Ternary Compounds  
 Abstract    The phase diagram of the ternary system Ca/Mo/O has been determined. Powder samples of the ternary compounds CaM o04, CaM o03, CaMo50 8, Ca16 5Mo,3 5O40 and Ca5 45Moi80 32 were prepared by solid state reactions. Rietveld analysis based on powder X-ray diffraction data shows that the compound CaMo50 8 has monoclinic structure (P2,/c) with a = 7.549, b = 9.064, c = 9.974 A, 3 = 110.04°. CaMo.O*, Ca I*. <Moit sOjo and Ca« 4sMoieO-i9 are semiconductors over the temperature range 75 to 300 K. 
  Reference    Z. Naturforsch. 52b, 1169—1174 (1997); eingegangen am 14. August 1997 
  Published    1997 
  Keywords    Calcium Molybdate, Phase Diagram, Synthesis, Crystal Structure, Electric Properties 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-1169.pdf 
 Identifier    ZNB-1997-52b-1169 
 Volume    52 
13Author    JuliaA. Manskaya, VolodimirN. Kokozay, KonstantinV. DomasevitchRequires cookie*
 Title    Crystal Structure of an Ammonium Dithiocyanatocuprate(I) Complex with 18-Crown-6, [NH4(18-Crown-6){Cu(NCS)2}] Obtained from Zero Valent Metal  
 Abstract    The new macrocyclic dithiocyanatocuprate(I) complex [NH4(18-crown-6){Cu(NCS)2}] has been prepared using a direct method of interaction and characterized by X-ray crystallogra­ phy (orthorhombic, space group Cmc2i, with a = 12.453(2), b = 21.650(4), c = 8.151(2) A, V = 2197.6(8) Ä3, Z = 4 , 1 (F) = 0.054; wR2(F2) = 0.141 for 972 unique reflections with I > 2<r(I) and /?1(F) = 0.082; w/?2(F2) = 0.210 for all 1098 unique reflections). The lattice comprises complex cations [NH4(18-crown-6)]+ and infinite polymeric anions [Cu(NCS)2]-of a one-dimensional zig-zag structure. The copper atoms adopt three-fold coordination [CuN^S] (Cu-N 1,89(1), 1,90(1) A; Cu-S 2.278(4) A). 
  Reference    Z. Naturforsch. 52b, 1311—1314 (1997); received 
  Published    1997 
  Keywords    18-Crown-6, Copper(I), Thiocyanate, Synthesis, X-Ray 
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 Identifier    ZNB-1997-52b-1311 
 Volume    52 
14Author    C. H. Ennig, H. O. Pperm, AnnRequires cookie*
 Title    Thermische Zersetzung und Lösungskalorimetrie von Ammoniumsamariumchloriden Therm al D ecom position and Solution C alorim etry of A m m onium Sam arium Chlorides  
 Abstract    We determined the decomposition equilibria of ammonium samarium chlorides (NH4)2SmCl5 and NH4Sm2Cl7 by total pressure measurements and derived their thermody­ namical data from the decomposition functions. The enthalpies of formation were compared with the results of the solution calorimetry. The heats of solution of all solid phases in the system SmCl3-NH4Cl and of Sm20 3 were measured in 4n HC1. The enthalpies of formation of ammonium samarium chlorides were derived from the enthalpies of formation of SmCl3 and of NH4C1 and their heats of solution. Data by total pressure measurement ZlHB((NH4)2SmCl5f298) =-407,7±2,9 kcal/mol; S0((NH4)2SmCl5x298) = 84,0 ±4,5 cal/K-mol; ZlHß((NH4)Srn2Ci7x298) = -576,8 ±3,4 kcal/mol; S0(NH4Sm2Cl7x298) = 98,l ±5,5 cal/K-mol. Data by solution calorimetry ZlH°B(SmCl3 f298) = -248,1 ±0,8 kcal/mol; zJHo B((NH4),Sm Cl,f298) = -40 4 ,3 ± l,l kcal/mol; ZlH°B(NH4Sm9Cl7 f 298)= -572,3± 1,8 kcal/mol. 
  Reference    Z. Naturforsch. 52b, 1517—1525 (1997); eingegangen am 29. September 1997 
  Published    1997 
  Keywords    Ammonium Samarium Chlorides, Samarium Chloride, Synthesis, Thermodynamical Data, Solution Calorimetry 
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 Identifier    ZNB-1997-52b-1517 
 Volume    52 
15Author    H. Oppermann, S. Ehrlich, C. HennigRequires cookie*
 Title    Calorimetrie an Yttriumtrihalogeniden und Yttriumoxidhalogemden Calorimetry of Yttrium Trihalides and Yttrium Oxyhalides  
 Abstract    The heats of solution of Yttrium, YOC1, YOBr, YOI, YC13, YBr3, YI3 and Y20 3 were determined in 4n HX. From those the enthalpies of formation of Yttrium Trihalides YX3 and Yttrium Oxyhalides YOX at 298 K were derived: Z\Hb(YC13j 298) = -2 4 0 .4 ± 0.6 kcal/mol, Z\H^(YBr3,f,298) = -2 0 2 .1 ± 1.5 kcal/mol, _\H £(YI3,f '298) = -147.0 ± 1.7 kcal/mol, ^ H ^ (Y O c if,298) = -2 4 0 .2 ± 1.0 kcal/mol. _AHß(YOBrf 298) = -229.7 ± 2.0 kcal/mol, AH 
  Reference    Z. Naturforsch. 52b, 305—310 (1997); eingegangen am 28. November 1996 
  Published    1997 
  Keywords    Synthesis, Yttrium Oxyhalides, Yttrium Halides, Heat of Solution, Enthalpy of Formation 
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 Identifier    ZNB-1997-52b-0305 
 Volume    52 
16Author    S. Ehrlich, H. Oppermann, C. HennigRequires cookie*
 Title    Calorimetrie an Ammoniumyttriumhalogeniden Calorimetry of Ammonium Yttrium Halides  
 Abstract    The heat o f solution of all solid phases in the system YX3-NH4X with X = Cl, Br, I in 4 n HX was investigated. The enthalpies of formation of the ammonium yttrium halides are derived from the enthalpies of formation of Y X 3 and of NH4X and their heats of solution in An HX: Z\H^(NH4 Y 2Cl7,f,298) = — 561,5 ± 1,7 kcal/mol, Z\H^((NH4)3 YCl6,f,298) = -474,5 ± 1,3 kcal/mol, ziH ß((N H 4)3YBr6 f 298) = -400,8 ± 2,6 kcal/mol, _AH£((NH4)3 YI6,t-298) = -291,9 ± 3,0 kcal/mol. 
  Reference    Z. Naturforsch. 52b, 311—314 (1997); eingegangen am 24. Januar 1997 
  Published    1997 
  Keywords    Synthesis, Ammonium Yttrium Halides, Ammonium Halides, Heat of Solution, Enthalpy of Formation 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0311.pdf 
 Identifier    ZNB-1997-52b-0311 
 Volume    52 
17Author    Lothar BeyerRequires cookie*
 Title    Substituierte l,2,4-Thiadiazolium-dichloroaurate(I) und -tetra- chloroaurate(III) als Reaktionsprodukte von N-Thiocarbamoyl- benzamidinen mit TetrachIorogold(III)-Verbindungen  
 Abstract    Substituted 1,2,4-T hiadiazolium dichloroaurates(I) and -tetrachloroaurates(III) as Products o f the R eaction o f N -T hiocarbam oyl-benzam idines w ith Tetrachlorogold(III) Com pounds U w e Schröder3, R ainer R ichter3, Jürgen H artung3, U lrich A bram b, 
  Reference    Z. Naturforsch. 52b, 620—628 (1997); eingegangen am 12. März 1997 
  Published    1997 
  Keywords    1, 2, 4-Thiadiazoliumchloroaurates(I/III), Synthesis, X-Ray, EM Spectra, N-Thiocarbamoylbenzamidines 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0620.pdf 
 Identifier    ZNB-1997-52b-0620 
 Volume    52