| | 1 | Author
| HerbertW. Roesky, Pierre Schäfer, Mathias Noltemeyer, GeorgeM. Sheldrick | Requires cookie* | | | Title
| Zur Darstellung und Struktur des 1.3-Dichloro-5-N.N-dimethylamino-1.3-dithia-2.4.6-triazins Synthesis and Structure of l,3-Dichloro-5-N,N-dimethylamino-l,3-dithia-2,4,6-triazine  | | | | Abstract
| The six membered ring of composition (CH3)2NCN3S2Cl2 8 a was prepared from N,N-dimethylguanidinhydrochloride and trithiadiazindichloride. 3 a was characterized on the basis of mass, 1 H, 13 C NMR spectra and X-ray structure analysis. Crystals of 3 a are monoclinic, space group P2i/c, with a — 660.3(6), b = 834.5(7), c = 1774.7(15) pm, ß = 112.83(6)° and Z = 4. The C2N unit lies approximately in the plane of the [-CNSNSN-] ring, with both Cl atoms on the same side of the ring. | | | |
Reference
| Z. Naturforsch. 38b, 347—349 (1983); eingegangen am 16. September 1982 | | | |
Published
| 1983 | | | |
Keywords
| Six Membered Ring, Carbon, Sulfur, Nitrogen, X-Ray Structure | | | |
Similar Items
| Find | | | DEBUG INFO
| | | | | TEI-XML for
| default:Reihe_B/38/ZNB-1983-38b-0347.pdf | | | | Identifier
| ZNB-1983-38b-0347 | | | | Volume
| 38 | |
|
