| | 1 | Author
| Jens Anhaus, ZafarA. Siddiqi, HerbertW. Roesky, JanW. Bats, Yalcin Elerman | Requires cookie* | | | Title
| Reaktion von Tetraschwefeltetranitrid mit Rhenium(VII)-chloronitrid Die Kristallstruktur von [Ph 4 As + ] 2 [Cl 4 Re(NS)(NSCl) 2_ ] * CH 2 C1 2 Reaction of Tetrasulfurtetranitride with Rhenium(VII)-chloronitride The Crystal Structure of [Ph 4 As + ] 2 [Cl 4 Re(NS)(NSCl) 2_ ] * CH 2 C1 2  | | | | Abstract
| The synthesis of [Ph 4 As + ] 2 [Cl 4 Re(NS)(NSCl) 2 ~] • CH 2 C1 2 (4) from the reaction of S 4 N 4 , Cl 4 ReN, and Ph 4 AsCl is reported. CH 2 C1 2 is used as solvent. The reaction of S 4 N 4 with Re 2 Cl 10 similarly leads to the salt [Ph 4 As + ][Cl 5 ReNS~] (5) in a smaller yield. 4 crystallizes in the triclinic space group PI with Z -2, a = 10.434(2), b = 12.1454(6), c -21.125(2) Ä, a = 81.210(6), ß = 86.70(1), Y = 76.624(8)°. | | | |
Reference
| Z. Naturforsch. 40b, 740—744 (1985); eingegangen am 6. Februar 1985 | | | |
Published
| 1985 | | | |
Keywords
| Thionitrosyl Complexes, Rhenium(VII), Crystal Structure | | | |
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| default:Reihe_B/40/ZNB-1985-40b-0740.pdf | | | | Identifier
| ZNB-1985-40b-0740 | | | | Volume
| 40 | |
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