| 1 | Author | IhsanA M Jasim | Requires cookie* |
| Title | Zur Reaktion von Hexamethyldistannoxan und Hexamethyldistannthian mit Phosphor-oxo-bzw. -thio-halogeniden. Schwingungsspektren von (Me2PS)20 und (Me2PS)2S A bdel-Fattah Shihada  | ||
| Abstract | M e3S n 0 2PCl2 and (M e2PS)20 are prepared from the reactions o f (M e3Sn)20 with PO C l3 (1:1) and with M e2PSCl (1 :2), respectively. The reactions of (M e3Sn)2S with M e2PSCl and with PSBr3 lead to the formation o f (M e2PS)2S and P4S9, respectively. PO C l3 reacts with (M e3Sn)2S to give unidentified products as a result o f O/S exchange. The i.r. and Raman spectra o f the solids (M e2P S)20 and (M e2PS)2S and the Raman spectra of the m olten com pounds are reported and the frequencies assigned. | ||
| Reference | Z. Naturforsch. 39b, 783—787 (1984); eingegangen am 16. Januar 1984 | ||
| Published | 1984 | ||
| Keywords | R eactions, Preparations, Vibrational Spectra | ||
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