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'Phosphinoethers' in keywords Facet   section ZfN Section B  [X]
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1995 (1)
1Author    W. Erner Wolfsberger, WolfgangB. Urkart, Helmut WernerRequires cookie*
 Title    Darstellung und Charakterisierung substituierter Phosphinoether und -thioether Preparation and Characterization of Substituted Phosphinoethers and -thioethers  
 Abstract    The (diorganophosphinopropyl)alkyl ethers 1 -7 are prepared by hydrophosphination of allylalkyl ethers with secondary phosphines. The corresponding thioethers cannot be ob­ tained in a pure state by the same route. The nucleophilic ring opening of thiirane with lithium dialkyl phosphides, followed by the reaction with ClSi(CH3)3 or C1(CH2)20C H 3 pro­ duces the thioethers 8 -1 2 and 16. The silylated thioethers 8, 10 and 12 react with CH3OH/ H20 to give the phosphinoethyl thiols 13-15. All new compounds have been identified and characterized by elemental analyses, IR and NM R spectra. 
  Reference    Z. Naturforsch. 50b, 168—174 (1995); eingegangen am 13. September 1994 
  Published    1995 
  Keywords    Phosphinoethers, Phosphinothioethers, Phosphinothioles, NM R Spectra 
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 TEI-XML for    default:Reihe_B/50/ZNB-1995-50b-0168.pdf 
 Identifier    ZNB-1995-50b-0168 
 Volume    50