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1Author    TalebH. Al-TelRequires cookie*
 Title    Carbohydrates to Pyrano-Furanoids: New and Regioselective Palladium-Catalyzed Syntheses of Tetrasubstituted Furanoids from Carbohydrate Scaffolds  
 Abstract    A new strategy for the asymmetric syntheses of polysubstituted pyrano-furanoids using allylic sulfates derived from carbohydrate precursors and the dianion of diethoxycarbonyl acetone, catalyzed by Pd(0), is described. 
  Reference    Z. Naturforsch. 55b, 657—660 (2000); received March 27 2000 
  Published    2000 
  Keywords    Dihydrofuran, Carbohydrates, Palladium 
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 TEI-XML for    default:Reihe_B/55/ZNB-2000-55b-0657.pdf 
 Identifier    ZNB-2000-55b-0657 
 Volume    55 
2Author    Norbert Kuhn, Martin Grathwohl, Christiane Nachtigal, Manfred SteimannRequires cookie*
 Title    2.3-Dihydro-2-methoxyethylimino-l,3-dimethylimidazol -ein neuer hemilabil koordinierender Chelatligand [1] 2.3-Dihydro-2-methoxyethylimino-\ ,3-dimethylimidazole -a Novel Hemilabile Coordinating Chelate Ligand [1]  
 Abstract    The bifunctional 2,3-dihydro-2-methoxyethylimino-l,3-dimethylimidazole (C8H 15N30 , 10) is obtained from the reaction of methoxyethyl tosylate (7) and 2,3-dihydro-2-imino-l,3-dimethylimidazole (8) followed by deprotonation in good yield. 10 reacts with {(COD)RhCl}2 (COD = 1,5-cyclooctadiene) to give the imine complex (C8H 15N30)Rh(C0D)Cl (11), which is converted into the chelate complex [(C8H 15N30)Rh(C0D)]BF4 (12) on treatment with AgBF4. The imine complex (C8H 15N30) 2PdCl2 (13) is formed through the reaction of 10 with (PhCN)2PdCl2. The X-ray structures of 11, 13 and 2 C8H 15N30 • H2PdCl4 (15) are reported. R R 1 Rv -■ 
  Reference    Z. Naturforsch. 56b, 704—710 (2001); eingegangen am 28. März 2001 
  Published    2001 
  Keywords    Imidazoles, Rhodium, Palladium 
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 TEI-XML for    default:Reihe_B/56/ZNB-2001-56b-0704.pdf 
 Identifier    ZNB-2001-56b-0704 
 Volume    56 
3Author    Sibbele Hietkamp, Reinhard SchmutzlerRequires cookie*
 Title    Eine neue Synthese von Fluorphosphonat-Komplexen des Palladiums und Platins A New Synthesis of Fluorophosphonato Complexes of Palladium and Platinum  
 Abstract    Addition of phosphorus(III) ligands, L (L = tertiary phosphine, phosphite) to the reaction mixture of allyldifluorophosphite (1) with (C 6 H5CN)2MCl2 (2) (M = Pd, Pt) was found to produce two types of products: after a shorter reaction period, monofluoro-phosphonate complexes of the previously known type £rans-L2MCl(POF2) (6) are obtained while over prolonged periods of time bis-fluorophosphonato complexes, Zrans-L2M(POF2)2 (7) are formed. By contrast, Bu"OPF2 (8) yields a mixture of «rans-L2PtCl(POF2) (6) and <rons-L2PtCl[(Bu"0)(F)P0] (10) (L = Ph3P), the latter originating from (Bu re O)2PF formed by ligand scrambling in Bu*OPF2; no products containing more than one fluorophos-phonate group are formed in this case. The new monofluorophosphite, (CH2 = CHCH20)2PF (10) was found to react rapidly with (C6H5CN)2PtCl2/L with formation of L2PtCl[(CH2==CHCH20)(F)P0] (11). Compound characterization was by IR, 19 F and 31 P NMR spectroscopy. 
  Reference    Z. Naturforsch. 35b, 548—553 (1980); eingegangen am 2. November 1979 
  Published    1980 
  Keywords    Palladium, Platinum, Fluorophosphonato Complexes 
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 TEI-XML for    default:Reihe_B/35/ZNB-1980-35b-0548.pdf 
 Identifier    ZNB-1980-35b-0548 
 Volume    35 
4Author    Ursula Eberz, Werner Seelentag, Hans-Uwe SchusterRequires cookie*
 Title    Zur Kenntnis farbiger ternärer und quaternärer Zintl-Phasen Coloured Ternary and Quaternary Zintl-Phases  
 Abstract    Ternary and quaternary, mostly coloured compounds of Au, Pd and Pt, resp., with Li, Mg, Sc and Sn were prepared and structurally investigated. They crystallize in a "filled" Zinkblende type structure (space group F?3m) and can be characterized as ternary or quaternary Zintl-phases. Colours seem to depend on unfilled d-orbitals of Au, Pd or Pt. 
  Reference    Z. Naturforsch. 35b, 1341—1343 (1980); eingegangen am 5. August 1980 
  Published    1980 
  Keywords    Lithium, Magnesium, Scandium, Gold, Palladium 
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 TEI-XML for    default:Reihe_B/35/ZNB-1980-35b-1341.pdf 
 Identifier    ZNB-1980-35b-1341 
 Volume    35 
5Author    Andreas Lenz, Christoph Schmidt, AnnetteBarbara Lehmann, Wagner, Wolfgang BeckRequires cookie*
 Title    Ein-und zweikernige Palladium-und Platin(II)-Chelat-Komplexe mit dem Mono-und Dianion von Indigo und Indigoderivaten Metal Complexes o f D yes, VIII [1 ] Mono-and Dinuclear Palladium and Platinum (II) Chelate Complexes of the Mono-and Dianion o f Indigo and Derivatives thereof  
 Abstract    A series of mono and bis N,O-chelate complexes 1-32 with the mono and dianion of indigo and indigo derivatives (R3P)(C1)M(L-H+) (M = Pd.Pt), (r/3-allyl)Pd(L-H+), (PhiC=NCH->CO->Et-H+)Pd(L-H+), (PhN=NPh-H+)Pd(L-H+), (Q H 5)Fe(C5H3CH2NMe2)Pd(L-H+), [(R3P)(Cl)Pt]2(L-2H+), [(//3-allyl)Pd]2(L-2H+), [(C6H4CH2N M e2)Pd]2(L-2H+) with L = indigo, 4,4'-dichloro-, 6,6'-dichloro-, 6,6'-dibromo-, 6,6'-di-»Bu-, 4,4'-dichloro-, 5.5'dibromo-, 5,5', 6,6'-tetramethoxy-, 4.4'-di-S]2H25-, 5,5'-di-SO?Na-indigo, indigo malonic ester and tetrahydro indigo have been prepared from chloro bridged metal complexes. In comparison to the free neutral indigo ligands the complexes show a high bathochromic shift in the VIS spectra (150-300 nm) which is mainly due to the anionic character of the coordinated indigo ligands. The structure of [(Et3P)(Cl)Pt]2(indigo-2H+) has been determined by X-ray diffraction. Metallkomplexe von Farbstoffen, VIII [1] 
  Reference    Z. Naturforsch. 52b, 474—484 (1997); eingegangen am 8. November 1996 
  Published    1997 
  Keywords    Indigo, Indigo Derivatives, Palladium, Platinum 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0474.pdf 
 Identifier    ZNB-1997-52b-0474 
 Volume    52 
6Author    Roland Hubei2, Tomas Jelinekb, Wolfgang Beck3Requires cookie*
 Title    Metal Complexes of Biologically Important Ligands, CXXV [1]. Palladium(II) and Platinum(II) Complexes of Quinine Derivatives and in vitro Tests  
 Abstract    Several quinine substituted derivatives at the C(9)-0 position (1 -7) have been obtained from quinine and N-protected glycine chloride, chlorocarbonyl ferrocene, phenylisocyanate, dicarboxylic acid dichlorides or trimesinic trichloride. From these only the glycine derivative 1 showed significant antimalarial activity in in vitro tests against Plasmodium falciparum 
  Reference    Z. Naturforsch. 55b, 821—833 (2000); received March 13 2000 
  Published    2000 
  Keywords    Quinine Derivatives, Palladium, Platinum 
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 TEI-XML for    default:Reihe_B/55/ZNB-2000-55b-0821.pdf 
 Identifier    ZNB-2000-55b-0821 
 Volume    55 
7Author    Vincenzo Calò, Angelo NacciRequires cookie*
 Title    Influence of Ionic Liquids on Pd-Catalyzed Carbon-Carbon Bond Formation  
 Abstract    Rates of Heck-type reactions, catalysed by a Pd-catalyst with benzothiazole carbene as ligands, are strongly influenced by tetrabutylammonium bromide utilized as solvent. 
  Reference    Z. Naturforsch. 56a, 702—706 (2001) 
  Published    2001 
  Keywords    Ionic Liquids, Heck Reaction, Palladium, Carbenes, Aryl Acrylates 
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 TEI-XML for    default:Reihe_A/56/ZNA-2001-56a-0702.pdf 
 Identifier    ZNA-2001-56a-0702 
 Volume    56 
8Author    Max Schmidt, GerhardG. HoffmannRequires cookie*
 Title    Darstellung und Eigenschaften von Dihydrogensulfido-, Dihydrogenselenido-und Dinatriumsulfido-Komplexen von Palladium(II) und Platin(II) Synthesis and Properties of Di-hydrogensulfido, Di-hydrogenselenido and Di-sodiumsulfido Complexes of Palladium(II) and Platinum(II)  
 Abstract    Dichloro-bis(triphenylphosphine)platinum(II) (2) and Dichloro-l,2-bis(diphenylphos-phine)ethane-palladium(II) (3) do react with hydrogensulfide and sodiumsulfide under formation of the corresponding compounds Di-hydrogensulfido-l,2-bis(diphenylphos-phine)ethane-palladium(II) (4), Disodiumsulfido-l,2-bis(diphenylphosphine)ethane-palla-dium(II) (7), Di-hydrogensulfido-bis(triphenylphosphine)platinum(II) (1) and Di-sodium-sulfido-bis(triphenylphosphine)platinum(II) (8). 2 and 3 react with sodiumhydrogen-selenide under formation of Di-hydrogenselenido-l,2-bis(diphenylphosphine)ethane-palladium(II) (5) and Di-hydrogenselenido-bis(triphenylphosphine)platinum(II) (6). IR and *H NMR spectra are reported. 
  Reference    Z. Naturforsch. 33b, 1334—1337 (1978); eingegangen am 23. Mai 1978 
  Published    1978 
  Keywords    Platinum, Palladium, Dihydrogensulfido Complexes, Dihydrogenoselenido Complexes, Synthesis 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1334.pdf 
 Identifier    ZNB-1978-33b-1334 
 Volume    33 
9Author    Hans-Uwe Schuster, Sandör RozsaRequires cookie*
 Title    Darstellung und Struktur von K2PdAs2 Preparation and Structure of K2PdAs2  
 Abstract    K2PdAs2 was prepared from the elements. It crystallizes orthorhombically, space group Cmcm, a = 653.6 pm, 6= 1412.1pm, c = 602.5 pm, forming infinite Pd-As2-zig-zag-ribbons and conforming to a filament. 
  Reference    Z. Naturforsch. 34b, 1167—1168 (1979); eingegangen am 15. Mai 1979 
  Published    1979 
  Keywords    Ternary Compound, Potassium, Palladium, Arsenic, Crystal Data 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-1167_n.pdf 
 Identifier    ZNB-1979-34b-1167_n 
 Volume    34 
10Author    Z. NaturforschRequires cookie*
 Title    Der ThCr2Si2-Typ und verwandte Strukturen bei AFd2X2-Verbindungen (A = Ca, Sr, Ba; X = P, As)  
 Abstract    The T hC r2Si2-Type and Related Structures of /IPd^XVCompounds (A — Ca, Sr, Ba; X = P, As) A lbrecht Mewis The com pounds APd2X 2 (A = Ca, Sr; X = P, A s) have been prepared and their structures have 
  Reference    Z. Naturforsch. 39b, 713 (1984); eingegangen am 7. Februar 1984 
  Published    1984 
  Keywords    Ternary Pnictides, Alkaline Earth M etals, Palladium, Crystal Structure 
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 TEI-XML for    default:Reihe_B/39/ZNB-1984-39b-0713.pdf 
 Identifier    ZNB-1984-39b-0713 
 Volume    39 
11Author    Dirk Johrendt, Albrecht MewisRequires cookie*
 Title    Darstellung und Kristallstruktur der Verbindungen SEPdP (SE = Seltenerdelement) Preparation and Crystal Structure of SEPdP C om pounds (SE = Rare Earth Element)  
 Abstract    The new compounds SEPdP (SE = L a -G d), which were prepared by heating the elements, crystallize with a modified N i2In-type structure. The phosphides o f SE = D y -L u attain the orthorhombic TiNiSi-type structure. A comparison o f the cell volumes suggests that europium has intermediate valence in EuPdP. 
  Reference    Z. Naturforsch. 45b, 1262—1266 (1990); eingegangen am 19. März 1990 
  Published    1990 
  Keywords    Rare Earth Elements, Palladium, Phosphides, Crystal Structure 
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 TEI-XML for    default:Reihe_B/45/ZNB-1990-45b-1262.pdf 
 Identifier    ZNB-1990-45b-1262 
 Volume    45 
12Author    Hans-Uwe Schuster, Axel Czybulka, Detlef LastRequires cookie*
 Title    Preparation and Structure of LiPd2Tl  
 Abstract    A new ternary phase LiPd2Tl has been synthe­ sized. It crystallizes in a modified tetragonal A l3Ti-type-structure with the lattice constants a = 
  Reference    Z. Naturforsch. 45b, 1451—1452 (1990); eingegangen am 26. Januar 1990 
  Published    1990 
  Keywords    Ternary Compound, Lithium, Palladium, Thallium, Crystal Data 
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 TEI-XML for    default:Reihe_B/45/ZNB-1990-45b-1451_n.pdf 
 Identifier    ZNB-1990-45b-1451_n 
 Volume    45 
13Author    Thomas Pill, Wolfgang BeckRequires cookie*
 Title    Metallkomplexe mit biologisch wichtigen Liganden, LXVI [1). Rhodium(III)-, Iridium(III)-, Palladium(II)-, Platin(II)-und Gold(I)-Komplexe von N-(2,3,4,6-Tetra-0-acetyl-/?-D-glucopyranosyl)-thiocarbamatestern und /?-D-Glucopyranosylthioharnstoff Metal Complexes o f Biologically Im portant Ligands, LXVI [1], Rhodium(III), Iridium (III), Palladium(II), Platinum (II), Gold(I) Complexes of N-(2,3,4,6-Tetra-0-acetyl-/?-D-glucopyranosyl)-thiocarbamate Esters and /?-D-Glucopyranosylthiourea  
 Abstract    From N-(2,3,4,6-tetra-0-acetyl-/?-D-glucopyranosyl)-thiocarbamate esters (L 1) the complexes (75-C5M e5)(Cl2)M (L') (M = Rh, Ir), C l(M e,N C H 7C6H4)Pd(LI), trans-(«-Bu3P)(Cl)2M (L') (M = Pd, Pt), /ra«5-Cl2P t(L 1)2, [(Ph3P)2(C l)Pt(L')]+, Cl2Pt(//-L')PtCl2 and C lA uL1 have been obtained. /?-D-glucopyranosylthiourea (L2) forms the complexes (>75-C5M e5)(Cl)-,M(L2) (M = Rh, Ir), (C l)M e2N C H 2C6H 4)Pd(L2), (Et3P)Cl,Pd(L2) and C12M (L2)2 (M = Pd, Pt). 
  Reference    Z. Naturforsch. 48b, 1461—1469 (1993); eingegangen am 27. April 1993 
  Published    1993 
  Keywords    Rhodium, Iridium, Palladium, Platinum, G old 
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 TEI-XML for    default:Reihe_B/48/ZNB-1993-48b-1461.pdf 
 Identifier    ZNB-1993-48b-1461 
 Volume    48 
14Author    =. Eu, Hk Müller-Buschbaum, L. W. LffRequires cookie*
 Title    Weitere Verbindungen mit isolierten quadratischen P d 0 4-Polygonen: Compounds Containing Isolated Square Planar P d 0 4 Polygons: B aPd Ln 20 5 (L  
 Abstract    New compounds o f the composition BaPdLn2O s (Ln = Eu, Gd, Dy, H o) have been prepa­ red by crystallization from flux. They crystallize isotypic to BaPtLn7Ö 5, space group D-4h-P4/ mbm. Eu: a = 6.6359(6), c = 5.885(3) A ; Gd: a = 6.608(3), c = 5.873(3) A ; Dy: a = 6.5431(7), c = 5.8574(8) A ; Ho: a = 6.522(4), c = 5.855(5) A , Z = 2. The crystal structure is characterized by isolated planar P d 0 4 polygons incorporated into a framework o f edge-and corner-sharing doubly capped BaO s cubes and edge-and face-sharing L n 0 6 prisms. 
  Reference    Z. Naturforsch. 51b, 461—464 (1996); eingegangen am 16. Oktober 1995 
  Published    1996 
  Keywords    Barium, Palladium, Rare Earth Oxide, Crystal Structure 
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 TEI-XML for    default:Reihe_B/51/ZNB-1996-51b-0461.pdf 
 Identifier    ZNB-1996-51b-0461 
 Volume    51 
15Author    Norbert Kuhn, Martin Grathwohl3, Manfred Steimann3, Gerald Henkelb, HerrnRequires cookie*
 Title    .2-Bis( 1' ,31 -dimethy limidazolin-21 -iminato)ethan - ein neuer Chelatligand [1]  
 Abstract    The reaction of 2-imino-l,3-dimethylimidazoline (10, ImNH) with X-CH2CH2-X (11, X = p-CH3C6 H4 S 0 3) gives the diimine adduct ImN-CH2CH2-NIm • 2 HX (12) from which the diimine ImN-CH2CH2-NIm (13) is obtained on treatment with KH. 13 reacts with (C6H5CN)2PdCl2 (15) to give the chelate complex (ImN-CH2CH2-NIm)PdCl2 (16). The X-ray structures of 12 and 16 are reported. 
  Reference    Z. Naturforsch. 53b, 997—1003 (1998); eingegangen am 2. Juni 1998 
  Published    1998 
  Keywords    Imines, Palladium, Chelates, Ligand Effects, X-Ray Data 
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 TEI-XML for    default:Reihe_B/53/ZNB-1998-53b-0997.pdf 
 Identifier    ZNB-1998-53b-0997 
 Volume    53 
16Author    Beate Dannecker, Gerhard ThieleRequires cookie*
 Title    Darstellung und Kristallstruktur von Palladiumoxidchlorid Pd2OCl2 Preparation and Crystal Structure of Palladium Oxide Chloride Pd:OCl2  
 Abstract    Pd2O C l2 was obtained by reaction o f y-PdCl2 and PdO • rcH20 in a K N 0 3/N a N 0 3 melt at 450 °C. Single crystals were grown from a T1C1 flux. The crystal structure o f the tetragonal com pound (a = 631.3(2) pm, c -987.2(2) pm, space group R ^ am d) is built up from bands of edge shared square planar PdO :Cl2 groups connected by com m on O -atom s to a framework. The relationship betw een the structures o f Pd2O Cl2 and PdO is discussed. 
  Reference    Z. Naturforsch. 41b, 1363—1366 (1986); eingegangen am 17. Juli 1986 
  Published    1986 
  Keywords    Palladium O xide Chloride, O xide Chloride, Crystal Structure, Palladium 
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 TEI-XML for    default:Reihe_B/41/ZNB-1986-41b-1363.pdf 
 Identifier    ZNB-1986-41b-1363 
 Volume    41 
17Author    Yuanlin Zhou, Barbara Wagner, Kurt Polborn, Karlheinz Sünkel, Wolfgang BeckRequires cookie*
 Title    Metallkomplexe mit biologisch wichtigen Liganden, LXXIII [1] Komplexe von Palladium(II), Platin(II), Rhodium(III) und Iridium(III) mit N-6-Deoxy-galactopyranosyl-«-Aminosäuren Metal Complexes with Biologically Im portant Ligands, LXXIII [1] Organometallic Compounds of Palladium(II), Platinum (II), R hodium (III) and Iridium (III) with N-6-Deoxy-galactopyranosyl-a-amino Acids  
 Abstract    A series of complexes with anions of N -[l,2:3,4-di-0-isopropylidene-6-deoxy-a-D -galacto-pvranos-6-vl]-a-aminoacids has been obtained and characterized by spectroscopic data: 
  Reference    Z. Naturforsch. 49b, 1193—1202 (1994); eingegangen am 24. Januar 1994 
  Published    1994 
  Keywords    Palladium, Platinum, Rhodium, Iridium Complexes, N-6-Deoxy-galactopyranosyl-a-aminoacidates 
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 TEI-XML for    default:Reihe_B/49/ZNB-1994-49b-1193.pdf 
 Identifier    ZNB-1994-49b-1193 
 Volume    49 
18Author    D. Irk Johrendt, R. Einer, M. Iericke, A.Lbrecht MewisRequires cookie*
 Title    Neue Pnictide mit modifizierten A1B2-Strukturen New Pnictides with M odified A1B2-Type Structures  
 Abstract    Nine new compounds A M X with A: Ca, Sr, Ba, M: Pd, Au and X : P, As were prepared by heating mixtures of the elements and investigated by X-ray methods. They crystallize in modified A1B2-type structures, for the present examples in the ZrBeSi-and SrPtSb-types, with an ordered distri­ bution of the atoms. 
  Reference    Z. Naturforsch. 51b, 905—906 (1996); eingegangen am 6. November 1995 
  Published    1996 
  Keywords    Ternary Pnictides, Alkaline Earth Metals, Palladium, Gold, Crystal Structure 
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 TEI-XML for    default:Reihe_B/51/ZNB-1996-51b-0905_n.pdf 
 Identifier    ZNB-1996-51b-0905_n 
 Volume    51 
19Author    H. W. ErnerRequires cookie*
 Title    M ax-Planck-Institut für K ohlenforschung, D-4330 M ülheim a.d . Ruhr  
  Reference    Z. Naturforsch. 39b, 990—9 (1984); received February 17 1984 
  Published    1984 
  Keywords    Palladium, ^3-A llyl, ?75 -Cyclopentadienyl, ?7 2-Fulvene 
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 TEI-XML for    default:Reihe_B/39/ZNB-1984-39b-0990_n.pdf 
 Identifier    ZNB-1984-39b-0990_n 
 Volume    39 
20Author    Akinori ShiotaniRequires cookie*
 Title    Die Pd-katalysierte oxidative Kupplungsreaktion von Methylbenzoesäuremethylester The Pd-Catalyzed Oxidative Coupling Reaction of Methyl Methylbenzoates  
 Abstract    The Pd-catalyzed oxidative coupling reaction of methyl o-toluate gives, in the presence of a Pd/l,10-phenanthroline(phen)/Cu catalyst, exclusively, the para-linked biphenyldicarboxy-lates 1, 2, and 3. On the other hand, the meta-linked biphenyldicarboxylates 4 and 5, were predominantly formed in a catalyst system of Pd/2,4-pentanedione(acacH)/Cu, and under similar conditions 6 and 7 were also obtained from the coupling reaction of methyl m-toluate and methyl p-toluate, respectively. A reaction scheme has been proposed. 
  Reference    Z. Naturforsch. 49b, 1731—1736 (1994); eingegangen am 21. April 1994 
  Published    1994 
  Keywords    Coupling Reaction, Steric Influence, Palladium, 1, 10-Phenanthroline, 2, 4-Pentanedione 
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 TEI-XML for    default:Reihe_B/49/ZNB-1994-49b-1731.pdf 
 Identifier    ZNB-1994-49b-1731 
 Volume    49 
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