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1999 (1)
1Author    Barbara Wenzel, Peter StrauchRequires cookie*
 Title    Synthesis, Structural and EPR Investigations on Bis(tetraphenylphosphonium)- bis(l,2-dithiosquarato)oxovanadate(IV), (Ph4P)2[VO(dtsq)2]  
 Abstract    The molecular structure and EPR studies of bis(tetraphenylphosphonium)bis(1,2-dithiosquarato)oxovanadate(IV) are reported. (Ph4P)2[VO(dtsq)2] crystallizes in the mono­ clinic spaceogroup P2,/n with the unit cell parameters a = 10,9820(2), b = 15,4620(3), c = 14,5050(3) Ä, ß = 95,700(8)°, Z = 2. The g and hyperfine coupling tensors Av obtained from the EPR spectra in liquid and frozen solution are used to characterize the properties of the molecular orbital containing the unpaired electron and are compared to those obtained from EHT-MO calculations. 
  Reference    Z. Naturforsch. 54b, 165—170 (1999); eingegangen am 18. September 1998 
  Published    1999 
  Keywords    Sulfur, Oxovanadate(IV), Synthesis, EPR Data, Crystal Structure 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0165.pdf 
 Identifier    ZNB-1999-54b-0165 
 Volume    54