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'NMR Spectra' in keywords Facet   section ZfN Section B  [X]
Facet   Publication Year 1995  [X]
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1Author    Peter Dierkes, Gerlinde Frenzen, Sigrid Wocadlo, W. Erner Massa, Stefan Berger, Jürgen Pebler, Kurt DehnickeRequires cookie*
 Title    Komplexe des Typs [MCl4(SEt2)2] mit M = Mo und W. Kristallstrukturen, NMR-Spektren und magnetisches Verhalten [MCl4(SE t2)2] Complexes with M = Mo and W. Crystal Structures, NMR Spectra, and Magnetic Behaviour  
 Abstract    The crystal structures of the thioether complexes [MCl4(SEt2)2] with M = Mo and W have been solved by X-ray methods. Both compounds crystallize isotypically in the triclinic space group P I with two formula units per cell unit. The metal atoms are octahedrally coordinated by four chlorine atoms and by the two sulfur atoms of the thioether molecules in trans­ position (symmetry Q) with bond lengths (average): M o -C l 233.1, M o -S 253.4, W -C l 233.1, and W -S 251.7 pm. Both complexes were also characterized by !H and 13C NM R spectro­ scopy as well as by measurement of the magnetic susceptibilities in the tem perature range from 1.8 to 350 K. 
  Reference    Z. Naturforsch. 50b, 159—167 (1995); eingegangen am 23. August 1994 
  Published    1995 
  Keywords    D iethylthioethers of Molybdenum and Tungsten, Crystal Structure, NMR Spectra, Magnetic Susceptibility 
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 TEI-XML for    default:Reihe_B/50/ZNB-1995-50b-0159.pdf 
 Identifier    ZNB-1995-50b-0159 
 Volume    50