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'Mass Spectrum' in keywords Facet   Publication Year 1995  [X]
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1Author    Abdel-Fattah Shihada, Frank WellerbRequires cookie*
 Title    Synthesis, Vibrational Spectra, Mass Spectrum and Crystal Structure of Tri-n-butyltin Diphenylphosphinate (n-Bu)3S n 0 2PPh2  
 Abstract    Tri-/?-butyltin diphenylphosphinate (/?-Bu)3S n 0 2PPh2 has been synthesized by the reaction o f («-B u 3Sn)20 with Ph2POCl in toluene. An X-ray diffraction study of (/?-Bu3) S n 0 2PPh2 shows that the structure is polymeric and consists of helical chains in which (/7-Bu)3Sn groups are linked by O-P-O bridges. The geometry about tin is trigonal bipyramidal, with «-butyl groups in equatorial positions and an axial O -S n -O angle of 176.2 (2)°. IR and Raman spectra of («-B u)3SnÖ2PPh2 are given and assigned. The mass spectrum is reported and discussed. 
  Reference    Z. Naturforsch. 50b, 1343—1347 (1995); received D ecem ber 12 1994 
  Published    1995 
  Keywords    Crystal Structure, Vibrational Spectra, Mass Spectrum, Tri-n-butyltin Diphenylphosphinate 
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 TEI-XML for    default:Reihe_B/50/ZNB-1995-50b-1343.pdf 
 Identifier    ZNB-1995-50b-1343 
 Volume    50