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'Halogeno Complexes of N Iodosuccinimide' in keywords
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1994 (1)
1Author    Mitra Ghassemzadeh, Kurt Dehnicke, Helmut Goesmann, Dieter FenskeRequires cookie*
 Title    //2-Halogenokomplexe von N-Iodsuccinimid. Die Kristallstrukturen von PPh4[X(N-Iodsuccinimid)2] * CH3CN mit X = Cl, Br, I /^2-Halogeno Complexes of N-Iodosuccinimide. The Crystal Structures of PPh4 [X(N-Iodosuccinimide)2] * CH 3CN with X = Cl, Br, I  
 Abstract    The ,a2-halogeno complexes PPh4[X(N-Iodosuccinimide)2] • CH 3CN with X = Cl. Br, I have been prepared by reactions of N-Iodosuccinimide with the corresponding tetraphenylphos-phonium halides PPh4X in acetonitrile solutions. The compounds form pale yellow crystal needles, which were characterized by IR spectroscopy and by crystal structure determina­ tions. PPh4[Cl(N-Iodosuccinimide)2] C H 3CN (1): Space group Pna2!, Z = 4, 4461 observed unique reflections, R -0.027. Lattice dimensions at -6 0 °C: a = 1840.5(9), b = 2589(1), c = 728.2(4) pm. 
  Reference    Z. Naturforsch. 49b, 602—608 (1994); eingegangen am 22. Dezember 1993 
  Published    1994 
  Keywords    Halogeno Complexes of N-Iodosuccinimide, Synthesis, IR Spectra, Crystal Structure 
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 TEI-XML for    default:Reihe_B/49/ZNB-1994-49b-0602.pdf 
 Identifier    ZNB-1994-49b-0602 
 Volume    49