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'Fluorophosphorylcyclosilazanes' in keywords Facet   Publication Year 1997  [X]
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1997[X]
1Author    Uwe Klingebiel, Mathias Noltemeyer, Hans-Jörg RakebrandtRequires cookie*
 Title    Difluorphosphorylcyclosilazane -Synthese und Kristallstruktur Difluorophosphorylcyclosilazanes -Syntheses and Crystal Structure  
 Abstract    The reaction of lithiated l,3-bis(fluorodimethyl)cyclotrisilazane with PF3 leads to the formation of a PF2-substituted six-membered Si-N ring (1). 1,5-Bis(difluorophosphanyl)-2,2,4,4,6,6,8,8-octamethyl-cyclotetrasilazane (2) is obtained in the reaction of the dilithium derivative of the cyclic tetrasilazane with trifluorophosphane in a molar ratio 1:2. The crystal structure of (F2P-N-SiMe2-NH-SiMe2)2 (2) has been determined. 
  Reference    Z. Naturforsch. 52b, 775—777 (1997); eingegangen am 14. April 1997 
  Published    1997 
  Keywords    Fluorophosphorylcyclosilazanes, Silicon, Crystal Structure 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0775.pdf 
 Identifier    ZNB-1997-52b-0775 
 Volume    52