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'Electrochemical Synthesis' in keywords Facet   Publication Year 1990  [X]
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1Author    R. Castro, M.L D Urán, J.A G Arcía-Vázquez, J. Romero, A. Sousa, A. Castiñeiras, W. Hiller, J. SträhleRequires cookie*
 Title    Electrochemical Syntheses of Pyrimidine-2-thiolato Complexes of Nickel(II) Crystal and Molecular Structure of 2,2 -Bipyridine-bis(pyrimidine-2-thiolato)nickel(II) Monohydrate+  
 Abstract    The electrochemical oxidation o f nickel in pyrimidine-2-thione (pym tH) solution yields a com pound o f formula [Ni(pymt)-,]. When pyridine (py), 2,2'-bipyridine (bipy) or 1,10-phenan­ throline (phen) are added to the solution phase, the product obtained is a complex [Ni(pym t)2py2] or [Ni(pym t)2L] (L = bipy or phen). The crystal structure o f [Ni(pym t)2bipy] • H 20 is monoclinic, space group P 2,/c, with a = 726.6(2), b = 1586.2(2), c = 
  Reference    Z. Naturforsch. 45b, 1632—2 (1990); received May 14 1990 
  Published    1990 
  Keywords    Crystal Structure, Nickel(II) Complexes, Pyrimidine-2-thione, Electrochemical Syntheses 
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 TEI-XML for    default:Reihe_B/45/ZNB-1990-45b-1632.pdf 
 Identifier    ZNB-1990-45b-1632 
 Volume    45