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1987 (1)
1Author    Michel Mégnamisi-Bélombé, Helmut EndresRequires cookie*
 Title    Two Modifications of Tetraethylammonium tranis-Diiodobis(ethanedialdioximato)cobaltate(III) with and without Intermolecular 1--I Interactions  
 Abstract    The structures of two modifications of [C 8 H 2 nN][C4H 6 Col2N 4 04], M r -617.11, have been deter-mined by X-rav investigations. Form 1 is orthorhombic, Pben, a = 8.417(2), b — 12.923(3), c = 18.444(3) A, V = 2006 Ä 3 , Z = 4, d c = 2.04 gem" 3 , final R w = 0.037 for 1989 reflections and 124 parameters. There are no unusual intermolecular interactions in this modification. From 2 is tetragonal, \A x md, a = 8.886(3), c = 25.841(6) Ä, V = 2040 Ä 3 , Z = 4, d c = 2.01 gem" 3 , final R w = 0.027 for 1629 reflections and 80 parameters. In this modification the metal complexes form strictly linear chains via short intermolecular I -I contacts, 3.722(1) Ä. 
  Reference    (Z. Naturforsch. 42b, 1—4 [1987]; received August 21 1986) 
  Published    1987 
  Keywords    Structure, Dioxime Complex, Iodine Interactions, Linear Chain Compounds 
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 TEI-XML for    default:Reihe_B/42/ZNB-1987-42b-0001.pdf 
 Identifier    ZNB-1987-42b-0001 
 Volume    42