| | 1 | Author
| FathyA. Amer, El-Sayed Afsah, MohamedA. Metwally, MohamedT. El-Zimaity | Requires cookie* | | | Title
| Related Compounds from l,4-Bis(ethoxycarbonyl)-2,5-diamino-l,4-cyclohexadiene  | | | | Abstract
| Interaction of o-phenylenediamine with l,4-Bis-(ethoxycarbonyl)-2,5-diamino-l,4-cyclo-hexadiene (1) gave 2, which cyclised to the hexahydrobenzodiazepinone (3). On the other hand, interaction of 1 with o-aminophenol, gave compound 4 which on treatment with polyphosphoric acid gave the tetrahydrobis-benzooxazepinone (11). Treatment of 1 with phenylisothiocyanate and formamide afforded the dithiopyrimidoquinazolinone (8) and the tetrahydropyrimidoquinazolinone (9), while the interaction of 1 with benzenesulphonyl-chloride gave dibenzenesulphonamido-cyclohexadiene dicarboxylate (10). The structure of these compounds was established by chemical and spectroscopic methods. | | | |
Reference
| Z. Naturforsch. 35b, 1395—1397 (1980); received July 13/October 11 1979/May 2 1980 | | | |
Published
| 1980 | | | |
Keywords
| Diazepinones, Oxazepinones, Pyrimidoquinazolinones, Synthesis | | | |
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| default:Reihe_B/35/ZNB-1980-35b-1395.pdf | | | | Identifier
| ZNB-1980-35b-1395 | | | | Volume
| 35 | |
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