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61Author    K. Arin Ruhlandt-Senge, AlfredDirk Bacher, G. Ertraude Koellner, Birgit Siewert, Ulrich MüllerRequires cookie*
 Title    Tetraphenylphosphonium-nonachlorodivanadat(III), (PPh4)3[V2Cl9l * 7 CH2C12 Tetraphenylphosphonium Nonachlorodivanadate(III), (PPh4)3[V2Cl9] * 7 C H 2C12  
  Reference    Z. Naturforsch. 47b, 814—818 (1992); eingegangen am 14. O ktober 1991 
  Published    1992 
  Keywords    N onachlorodivanadate, Synthesis, Crystal Structure 
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 Identifier    ZNB-1992-47b-0814 
 Volume    47 
62Author    G.Erhard Müller, Joachim Lachm, Jürgen RiedebRequires cookie*
 Title    Molekülstrukturen von (o-Brombenzyl)diphenylphosphan und l,3-Bis(diphenylphosphinomethyl)benzol M olecular Structures of (o-Bromobenzyl)diphenylphosphine and l,3-Bis(diphenylphosphinomethyl)benzene  
  Reference    Z. Naturforsch. 47b, 823—828 (1992); eingegangen am 3. Februar 1992 
  Published    1992 
  Keywords    Benzylphosphines, Conformation, Crystal Structure 
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 TEI-XML for    default:Reihe_B/47/ZNB-1992-47b-0823.pdf 
 Identifier    ZNB-1992-47b-0823 
 Volume    47 
63Author    Z. NaturforschRequires cookie*
 Title    Über Sulfide und Oxidsulfide des Samariums  
 Abstract    Stoichiometric oxidation o f SmCl2 with sulfur in the presence o f NaCl (evacuated silica ves­ sel, 850 °C, 7 d) results in the formation o f A -S m -,S 3 (orthorhombic, Pnma (no. 62), a = 737.64(5), b = 397.44(3), c = 1536.26(9) pm, Z = 4, /?w = 0.017). In contrast, C ~ S m 2S3 (cubic, I4 3 d (no. 220), a = 844.71(3) pm, Z = 5.333, Rw = 0.017) is obtained upon reaction o f the 
  Reference    Z. Naturforsch. 47b, 1614 (1992); eingegangen am 1. Juli 1992 
  Published    1992 
  Keywords    Samarium, Sulfides, Oxysulfides, Crystal Structure 
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 Identifier    ZNB-1992-47b-1614 
 Volume    47 
64Author    Gudrun Stieglitz, Bernhard Neumüller, K. Urt DehnickeRequires cookie*
 Title    Synthesen und Kristallstrukturen der Lithiumphosphide { Li(DME)[P(f-Bu)2]} 2 und [Li(DM E)PPh2l00 Syntheses and Crystal Structures of the Lithium Phosphides {Li(DME)[P(/-Bu)2]}2 and [Li(DM E)PPh2]0 0  
 Abstract    The title com pounds have been prepared by the reaction o f rc-butyllithium with the corre­ sponding diorganophosphanes H PR 2 (R = r-Bu, Ph) in D M E solutions. Both compounds were characterized by crystal structure determinations. {Li(DM E)[P(f-Bu)2]}2: Space group P 1, Z = 1, 2027 observed unique reflections, R = 0.055. Lattice dimensions at —80 °C: a = 879.9(3), b = 986.3(1), c = 1064.0(2) pm, a = 70.69(1)°, ß = 70.63(2)°, y -69.89(2)°. The com pound forms centrosymmetric dimers o f symmetry Q with L i-P bond lengths o f 260.0 and 257.3 pm for the Li2P2 four-membered ring. [Li(DM E)PPh2]0C : Space group P 2 ,/«, Z = 4. 3437 observed unique reflections, R = 0.055. Lattice dimensions at -8 0 °C: a = 1034.8(2), b = 812.48(9), c = 1978.4(3) pm, ß = 103.30(2)°. The com pound forms polymeric chains via LiP bridges with L i-P bond lengths o f 256.3 and 254.1 pm. 
  Reference    Z. Naturforsch. 48b, 156 (1993); eingegangen am 8. Oktober 1992 
  Published    1993 
  Keywords    Lithium Phosphides, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/48/ZNB-1993-48b-0156.pdf 
 Identifier    ZNB-1993-48b-0156 
 Volume    48 
65Author    Jorge Blanco, Eduardo Gayoso, JoseManuel Vila, Miguel Gayoso, CäciliaM. Aichle, -. M. Össmer, Joachim SträhleRequires cookie*
 Title    Synthesis and Structure of Di-I/i-acetato(0,0')-ferrocenylmethyliden- 2,4,6-trimethylaniline(N,C)-palladium(II)l  
 Abstract    Di-[//-acetato(0,0')-ferrocenylmethylidene-2,4,6-trimethylaniline(N,C)-palladium(II)], 
  Reference    Z. Naturforsch. 48b, 906—910 (1993); received M arch 8 1993 
  Published    1993 
  Keywords    Cyclometallation, Synthesis, Crystal Structure 
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 Identifier    ZNB-1993-48b-0906 
 Volume    48 
66Author    Enno Lork, Ulrich Behrens, G. Ünter Steinke, Rüdiger MewsRequires cookie*
 Title    Die Kristallstruktur von trans-l,3?5-Trichloro-l,3>5-trioxo  
 Abstract    1 A6, 3 A6, 5 A6,2,4,6-trithiatriazin (/?-Sulfanurchlorid) The Crystal Structure o f /raws-1,3,5-Trichloro-1,3,5-trioxo-1 X6, 3/i6, 516, 2,4,6-trithiatriazine (/?-Sulfanuric Chloride) The crystal structure o f /?-(N S(0)C l)3 is reported. 
  Reference    Z. Naturforsch. 49b, 437 (1994); eingegangen am 22. November 1993 
  Published    1994 
  Keywords    Trichlorotrioxotrithiatriazines, Sulfanuric Chlorides, Crystal Structure 
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 TEI-XML for    default:Reihe_B/49/ZNB-1994-49b-0437.pdf 
 Identifier    ZNB-1994-49b-0437 
 Volume    49 
67Author    Müller-BuschbaumRequires cookie*
 Title    Zur Kristallchemie der Oxoplatinate. Eine neue Phase der Zusammensetzung Sr4_j.Naj.PtO6 (jt = 0,33)  
 Abstract    On the Crystal Chemistry of Oxoplatinates. A New Phase of the Composition Sr4 _xN avP t0 6 (x -0.33) G. Tams, Hk. Single crystals of Sr3 67Na() 33PtO fi were prepared by heating oxide mixtures in closed silver tubes and investigated by X-ray single crystal techniques. It crystallizes with trigonal symme­ try, space group Dfd-R 3 c (Nr. 167) with a = 9.6617, c = 11.6580 Ä, Z = 6. Sr367Na()33P t0 6 belongs to the Sr4P t0 6 type and is isotypic to K4CdCl6. One point position characterized by a trigonal prismatic O 2-coordination is occupied by N a+ and Sr2+ statistically. The crystal structure is discussed with respect to the related compounds Sr3C u P t0 6 and Ca3 5Cu() 5P t0 6. 
  Reference    Z. Naturforsch. 49b, 581—584 (1994); eingegangen am 12. Januar 1994 
  Published    1994 
  Keywords    Strontium, Sodium, Platinum Oxide Crystal Structure 
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 Identifier    ZNB-1994-49b-0581 
 Volume    49 
68Author    Siegfried Pohl, Michael Peters, Detlev Haase, Wolfgang SaakRequires cookie*
 Title    Bildung von Iodoantimonaten und -bismutaten. Kristallstrukturen von (PhCH2NEt3)4 [Sb6l 2 2 L (PhCH2NEt3)4 [Bi6l 2 2 ] und (Ph4P)3[Bi5I18] Form ation of Iodoantim onates and Bismutates. Crystal Structures of (PhCH 2N E t3)4[Sb6I22], (PhC H 2N Et3)4[Bi6l22] and (Ph4P)3[Bi5I 18]  
 Abstract    The formation and the crystal structures of the title compounds are reported. (PhCH2N E t3)4[Sb6l 22] and (PhCH 2N E t3)4[Bi6l 22] are isotypic and contain a novel [E6I22]4~ anion (E = Sb, Bi). The anion of (Ph4P)3[Bi5I18] consists of a linear chain of five face-sharing [B il6] octahedra. 
  Reference    Z. Naturforsch. 49b, 741—7 (1994); eingegangen am 27. Januar 1994 
  Published    1994 
  Keywords    Iodoantimonates, Iodobismutates, Crystal Structure 
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 Identifier    ZNB-1994-49b-0741 
 Volume    49 
69Author    Viktor Keimes, Albrecht MewisRequires cookie*
 Title    MgNi2P -das erste ternäre Phosphid mit geordneter Fe3C-Struktur MgNi2P -The First Ternary Phosphide with an O rdered Fe3C Type Structure  
 Abstract    MgNi2P was prepared by heating a mixture of the elements and investigated by means of single crystal X-ray methods. The compound crystallizes in an ordered Fe3C-type structure 
  Reference    Z. Naturforsch. 49b, 1071—1073 (1994); eingegangen am 00. 00. 0000 
  Published    1994 
  Keywords    Ternary Nickelphosphide, Magnesium, Crystal Structure 
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 Identifier    ZNB-1994-49b-1071 
 Volume    49 
70Author    Holger Szillat, Hanskarl Müller-BuschbaumRequires cookie*
 Title    Synthesis and Crystal Structure of Cuq^sH oj 25w 2o 8  
 Abstract    Single crystals of Cu(l.2sHO|.2sW20 8 were prepared by recrystallization from melts and investigated by X-ray diffractometer technique. Cuo^sHoj 25W 2Os crystallizes with m ono­ clinic symmetry, space group C2/c, o -19.123, b -5.613, c = 11.479 Ä , ß = 111.44°. Z = 8. It represents a new structure type characterized by W40 18 groups and Cu+/H o3+ at one point position in statistical distribution. Cu+/H o3+ show an octahedral coordination. A nother point position is occupied by Ho3+ with C. N. = 7. 
  Reference    Z. Naturforsch. 49b, 1145—1149 (1994); eingegangen am 25. März 1994 
  Published    1994 
  Keywords    Crystal Structure Copper Holmium, Tungsten, Oxide 
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 Identifier    ZNB-1994-49b-1145 
 Volume    49 
71Author    J. Feldmann, Hk Miiller-BuschbaumRequires cookie*
 Title    Kristallstrukturuntersuchung an einem Strontium-Vanadyl-Vanadat: Sr2(V 0 )V 20 8 Crystal Structure Investigation of the Strontium Vanadyl-Vanadate: Sr2( V 0 ) V 20 8  
 Abstract    Single crystals of Sr2(V 0)V 20 8 have been prepared by quenching melts from higher tem­ peratures. This compound represents a new structure type and crystallizes with monoclinic symmetry, space group C |h-I 2 la, a = 6.929, b = 16.246, c = 7.260 A, ß = 115.82°, Z = 4. The point positions occupied by V5+ show tetrahedral coordination. The refinement of the V4+ position led to split positions with acentric orientations of V4+ in the octahedral O2-surrounding. It results in a square pyramidal coordination with one short V -O distance typically for vanadyl groups. 
  Reference    (Z. Naturforsch. 50b, 43—46 [1995]; eingegangen am 8. Juli 1994) 
  Published    1995 
  Keywords    Strontium, Vanadium Oxide, Crystal Structure 
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 Identifier    ZNB-1995-50b-0043 
 Volume    50 
72Author    H., M. Üller-Buschbaum, L. WalzRequires cookie*
 Title    Einkristallröntgenstrukturanalyse an Quecksilberchromat(VI)  
 Abstract    g 3 0 2 C r 0 4 Single C rystal X -Ray S tructure D eterm ination of a M ercury C hrom ate(V I): H g30 2C r 0 4 Th. H an sen , H k. Single crystals of Hg3C r0 6 have been prepared by high pressure techniques (3600 bar oxygen, 600 °C). Hg3C r06 crystallizes with trigonal symmetry, space group D |-P 3 212, a = 7.137(1), c = 10.017(2)Ä, Z -3. Nearly linear O -H g -O dumb-bells are connected in planes, forming strongly puckered nets of six-membered rings. Each Hg60 6 ring is centered by a C r04 tetrahedron; the C r04 tetrahedra are arranged in two equally occupied split positions. 
  Reference    (Z. Naturforsch. 50b, 47—5 [1995]; eingegangen am 2. August 1994) 
  Published    1995 
  Keywords    Mercury, Chromium, Oxide, Crystal Structure 
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 Identifier    ZNB-1995-50b-0047 
 Volume    50 
73Author    E. Peters, Hk Müller-BuschbaumRequires cookie*
 Title    Ein Titan-Tantaloxid mit Ti11: Ti0 ,3 3 Ta0 ,6 7O2 (TiTa20 6)  
 Abstract    Black single crystals o f Tio^Tao 670 2 have been prepared by C 0 2-LA SER techniques heating a mixture of TiO and Ta20 5 to T > 2000 °C. The titanium tantalum oxide crystallizes with tetragonaj symmetry, space group D 4 h -P 4 2/mnm, lattice constants a = 4.7344(6) A, c = 3.0504(2) A , Z = 2. Ti().33Ta0.67O 2 represents the compound TiTa20 6 with rutile structure because of the statistical distribution of Ti2+ and Ta5+. The composition of rutile-type com ­ pounds is discussed in more general terms. 
  Reference    Z. Naturforsch. 50b, 1167—1170 (1995); eingegangen am 16. Januar 1995 
  Published    1995 
  Keywords    Titanium, Tantalum, Oxide, Crystal Structure 
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 Identifier    ZNB-1995-50b-1167 
 Volume    50 
74Author    V. Ikto, R. Keimes, A. Lb Rech, M. EwisRequires cookie*
 Title    M g6N i16A s7 -a N ew G Phase  
 Abstract    Mg6N i16A s7 (F m 3m ; a = 11.479(1) Ä; Z = 4) was prepared by heating a mixture of the ele ­ ments and investigated by m eans of single crystal X-ray methods. The arsenide crystallizes in a m o­ dified Th6Mn23 type structure, similar to many ternary com pounds of the com position A 6M 16X 7, called G phases. 
  Reference    Z. Naturforsch. 50b, 1275—1276 (1995); eingegangen am 6. März 1995 
  Published    1995 
  Keywords    Ternary Nickelarsenide, Magnesium, Crystal Structure 
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 Identifier    ZNB-1995-50b-1275_n 
 Volume    50 
75Author    T. Gressling, Hk Müller-BuschbaumRequires cookie*
 Title    Zur Kristallstruktur von Ce2(W 0 4)3 On the Crystal Structure of Ce2(W 0 4)3  
 Abstract    Single crystals of Ce2(W 0 4)3 have been prepared by crystallisation from molten mixtures of W 0 3 and C e 0 2. The compound shows m onoclinic symmetry, a = 7.813(4), b = 11.720(2), c = 11.586(3), ß = 109.36(3)°, Z = 4, and is isotypic to Eu2(W 0 4)3, but shows large differences of the atomic coordinates especially of oxygen. The crystal structure of Ce2(W 0 4)3 is charac­ terized by W (1)0 4 tetrahedra, square W (2)0 5 pyramids and a distorted capped trigonal prism of oxygen around cerium. The decrease o f the oxidation states of C e4+ or W6+ was proved by thermogravimetric and magnetic measurements as well as by calculations of the Coulomb terms of lattice energy. 
  Reference    Z. Naturforsch. 50b, 1513—1516 (1995); eingegangen am 25. Mai 1995 
  Published    1995 
  Keywords    Cerium, Tungsten, Oxygen, Crystal Structure 
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 Identifier    ZNB-1995-50b-1513 
 Volume    50 
76Author    Karl Peters3, Eva-Maria Peters3, Gerhard Bringmannb, Sven HarmsenbRequires cookie*
 Title    l,4-Dibromonaphthalene-2,3-diyI- bis(l'-bromo-2'-naphthoate) * CHC13, a Potential Precursor to Lactone-Bridged Teraryls  
 Abstract    The title compound was prepared from 1,4-di-bromo-2,3-dihydroxynaphthalene by two-fold es-terification with l-bromo-2-naphthoic acid. It crystallizes from chloroform in the triclinic sys­ 
  Reference    Z. Naturforsch. 51b, 144—146 (1996); received June 20 1995 
  Published    1996 
  Keywords    Crystal Structure, Biaryl Coupling, Teraryls 
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 TEI-XML for    default:Reihe_B/51/ZNB-1996-51b-0144_n.pdf 
 Identifier    ZNB-1996-51b-0144_n 
 Volume    51 
77Author    D. Frerichs, C. H. Park, HkM. Üller-B, UschbaumRequires cookie*
 Title    Zur Kenntnis zweier Formen des Zinkorthoarsenates: a-Z n 3(A s04)2 und /3-Zn3(A s0 4)2 On Two Forms o f Zinc O rthoarsenate: a -Z n 3(A s 0 4)2 and /3-Zn3(A s 0 4)2  
 Abstract    Single crystals of two forms of zinc orthoarsenate (a-Z n3(A s04)2 (I) and /3-Zn3(A s04)2 (II)) have been prepared by flux techniques. Both compounds crystallize monoclinically, space groups (I): Cih-P2l/c, (II): Cih-P21/n, with the lattice parameters (I): a = 6.306(2), b = 8.652(2), c = 'ol 1.321(4) A, ß = 92.25(5) °, Z = 4 and (II): a = 5.281(1), b = 8.494(2), c = 7.726(3) A, ß = 96.39(3)°, Z = 2. ct-Zn3(A s04)2 is isotypic to I-Cu3(A s04)2 and ß-Zn3(A s04)2 to 7-Zn3(P 0 4)2. Similarities and differences of the crystal structures are discussed. 
  Reference    Z. Naturforsch. 51b, 333—337 (1996); eingegangen am 31. August 1995 
  Published    1996 
  Keywords    Zinc, Arsenic, Oxide, Crystal Structure 
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 Identifier    ZNB-1996-51b-0333 
 Volume    51 
78Author    Karl Peters3, Eva-M Aria Peters3, G.Erhard Bringmannb, O. La, F. SchuppbRequires cookie*
 Title    l,3-Dimethoxy-677- benzo[b]naphtho[l,2-d]pyran-6-thione, a Thionolactone-Bridged Axially Prostereogenic Biaryl  
 Abstract    The title compound was prepared from the cor­ responding " ordinary" oxolactone bridged biaryl using Lawesson's reagent. It crystallizes from di-chloromethane / petroleum ether in the mono­ clinic system, space group P2xla; a = 1115.7(2), 
  Reference    Z. Naturforsch. 51b, 431—432 (1996); received September 9 1995 
  Published    1996 
  Keywords    Crystal Structure, Stereochemistry, Biaryl Coupling 
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 Identifier    ZNB-1996-51b-0431_n 
 Volume    51 
79Author    J. Feldmann, Hk Müller-BuschbaumRequires cookie*
 Title    Kristallstrukturuntersuchung am Barium-Yanadyl-Vanadat: Ba2(V 0)V 20 8 Crystal Structure Investigation of the Barium Vanadyl-Vanadate: Ba2(V 0 )V 20 8  
 Abstract    Single crystals of Ba2(V 0)V 20 8 have been prepared by solid state reactions of Ba2V 20 7, V 9O 1 and V ^ 05 in sealed silica tubes. This compound crystallizes with monoclinic symmetry, space group C 1 -P 2 ,, a = 8.1174(9), b = 5.9699(9), c = 9.2903(9) A , ß = 113.94(1)°, Z = 2. V 5+ shows tetrahedral coordination. V 4+ inside ^ [V (3)0 4] chains is characterized by a square pyramidal coordination with a short apical V-O distance of 1.6 A typically for vanadyl groups. Ba2(V 0)V 20 8 represents a new structure type and is not isotypic to Sr2(V 0)V 20 8. 
  Reference    Z. Naturforsch. 51b, 489—4 (1996); eingegangen am 22. August 1995 
  Published    1996 
  Keywords    Barium, Vanadium, Oxide, Crystal Structure 
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 Identifier    ZNB-1996-51b-0489 
 Volume    51 
80Author    Rolf Minkwitz, RaimUnd Bröchler, Hans PreutRequires cookie*
 Title    Low-Temperature Crystal Structure of the Inclusion Compound {[N(CH3)4+C1]2] * CH 3CN * h 2o  
 Abstract    The crystal structure of {[N(CH3)4+C1]2}-CFI3C N H 20 is reported. Cry-stalls are orthorhombic, space group Pnma, with a = 1622.9(15), b = 671.3(6), c = 1511.2(11) pm, V = 1646(2) 106 pm3 and Z = 4. 
  Reference    Z. Naturforsch. 51b, 599—601 (1996); eingegangen am 3. August 1995 
  Published    1996 
  Keywords    Preparation, Crystal Structure, Inclusion Compound 
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 Identifier    ZNB-1996-51b-0599_n 
 Volume    51 
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