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301Author    Erwin Brechtel, Gerhard Cordier, Herbert SchäferRequires cookie*
 Title    Neue ternäre Erdalkaliverbindungen des Arsens mit Mangan New Ternary Alkaline Earth Compounds of Arsenic with Manganese  
 Abstract    The new compounds CaMn2As2, SrMn2As2 and BaMn2As2 have been prepared and their struc-tures determined. The crystallographic data are (pm): CaMn.2As2: P3ml, a = 423 ± 1, c = 703 ± 1, c/a = 1.66 SrMri2As2: P3m 1, a = 429±l,c = 732 ± 1, c/a = 1.70 BaMn2As2: I4/mmm, a = 415 ± 2, c = 1347 ± 2, c/a = 3.24 
  Reference    Z. Naturforsch. 33b, 820—822 (1978); eingegangen am 17. April 1978 
  Published    1978 
  Keywords    Intermetallic Compounds, Crystal Structure, Ternary Arsenides 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-0820_n.pdf 
 Identifier    ZNB-1978-33b-0820_n 
 Volume    33 
302Author    Johanna Von Unterrichter, Klaus-Jürgen RangeRequires cookie*
 Title    Ag8GeTe6, ein Vertreter der Argyroditfamilie AgsGeTe6, a Representative of the Argyrodite Family  
 Abstract    A single crystal of AgsGeTe6 was found to be rhombohedral, pseudocubic, space group R3m, with a— 817.6 pm, a — 60° and Z — 1. The anion lattice consists of three-dimen-sionally connected Frank-Kasper polyhedra with C. N. 12 and 16. The structure comprises isolated GeTe4-tetrahedra and silver ions, statistically distributed over a number of sites with distorted tetrahedral, trigonal and linear co-ordination. Structural data for some other compounds of the argyrodite family are given. 
  Reference    Z. Naturforsch. 33b, 866—872 (1978); eingegangen am 2. Mai 1978 
  Published    1978 
  Keywords    Silver Germanium Telluride, Crystal Structure, Argyrodite Family 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-0866.pdf 
 Identifier    ZNB-1978-33b-0866 
 Volume    33 
303Author    Wolfgang May, Hans Georg Von SchneringRequires cookie*
 Title    Darstellung und Struktur des Bicyclo-[4.4.0]-1.4.6.9-tetraazadecans C6H14N4  
 Abstract    By the weak acid interaction of polymeric phosphanes the condensation of ethylendi-amine yields in a small amount bicyclo-[4,4,0]-l,4,6,9-tetraazadecane C6H14N4. The compound crystallizes triclinic in the space group PI with a = 841.6 pm, b — 463.6 pm, c = 529.2 pm, a= 109.05°, ß= 108.35°, y = 84.13° and Z= 1 formula unit per unit cell. The two condensed six-membered rings have chair conformations. The mean N-C bond lengths are 146.0 pm, the bridging C-C bond is 150.3 pm, whereas the other C-C bonds are 155.1 pm. Structure and condensation reaction are discussed. 
  Reference    Z. Naturforsch. 33b, 881—883 (1978); eingegangen am 17. Mai 1978 
  Published    1978 
  Keywords    Tetraaza-bicyclo-decane, Preparation, Crystal Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-0881.pdf 
 Identifier    ZNB-1978-33b-0881 
 Volume    33 
304Author    A. Müller, N. Mohan, H. BöggeRequires cookie*
 Title    Molekül-und Elektronenstruktur des Thioheteroanions [S2 WS2CoS2WS2] 2 - Molecular and Electronic Structure of the Thiohetero Anion [S2WS2CoS2WS2] 2  
 Abstract    The crystal and molecular structure of [(C6H5)4P]2[Co(WS4)2] was determined from single crystal X-ray diffraction data (space group P2i/c with a = 18.542(4), b — 15.443(2), c= 18.713(2) A, /?= 108.73(1)°, Z = 4). In the complex anion Co is coordinated by two bidentate chelating WS4 2 -anions, with a nearly tetrahedral surrounding of Co. The bond lengths in the planar metal sulfur ring CoS2W are Co-S = 2.26 A and W-S = 2.22 A, while the terminal W-S bonds are 2.14 A. 
  Reference    Z. Naturforsch. 33b, 978—982 (1978); eingegangen am 8. Mai 1978 
  Published    1978 
  Keywords    Crystal Structure, Molecular Structure, Thiohetero Anion, Electronic Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-0978.pdf 
 Identifier    ZNB-1978-33b-0978 
 Volume    33 
305Author    Albrecht MewisRequires cookie*
 Title    ABX-Verbindungen mit Ni2In-Struktur Darstellung und Struktur der Verbindungen CaCuP  
 Abstract    (As), SrCuP(As), SrAgP(As) und EuCuAs ABX Compounds with the Structure Ni2In Preparation and Crystal Structure of CaCuP(As), SrCuP(As), SrAgP(As), and EuCuAs The compounds CaCuP(As), SrCuP(As), SrAgP(As) and EuCuAs were prepared and investigated by X-ray methods. They are isotypic and crystallize in a modified Ni2In structure (space group P 63/mmc-D^) with the lattice constants: CaCuP a = 405.5(1) pm, c = 780.3(3) pm, CaCuAs a = 418.4(1) pm, c = 786.8(2) pm, SrCuP a ' 414.6(1) pm, c = 837.6(3) pm, SrCuAs a = 427.3(2) pm, c = 845.2(3) pm, EuCuAs a = 425.4(2) pm, c = 827.4(3) pm, SrAgP a = 440.9(1) pm, c = 823.0(3) pm, SrAgAs a = 452.9(1) pm, c = 829.1(2) pm. 
  Reference    Z. Naturforsch. 33b, 983—986 (1978); eingegangen am 26. Juni 1978 
  Published    1978 
  Keywords    Intermetallic Compounds, Ternary Phosphides, Ternary Arsenides, Crystal Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-0983.pdf 
 Identifier    ZNB-1978-33b-0983 
 Volume    33 
306Author    Klaus Brodersen, Günter Liehr, Michael Rosenthal, Gerhard ThieleRequires cookie*
 Title    Stabile Quecksilber(I)-Selen  
 Abstract    Verbindungen, 2. Mitteilung [1] Die Struktur der roten Modifikation des Tetrakis(diphenylseleno)-diquecksilber(I)-bis(chlorat(VII)) Stable Mercury(I)-Selenium Compounds, 2 nd Communication [1] The Structure of the Red Modification of Tetrakis(diphenyl-seleno)-dimercury(I)-bis(chlorate(VII)) As shown by X-ray analysis the structure of the red modification of tetrakis(diphenyl-seleno)-dimercury(I)-bis(chlorate(VII)) contains cations [(C6H5)2Se]2Hg-Hg[Se(C6H5)2]2®® and C104~-anions. The twofold coordination of each mercury atom by 2 selenium atoms is remarkable for a mercury(I) compound. The relations between red and yellow modifica-tions are discussed. 
  Reference    Z. Naturforsch. 33b, 1227—1230 (1978); eingegangen am 5. Juni 1978 
  Published    1978 
  Keywords    Mercury(I)-Selenium Compounds, Crystal Structure, Mercury Compounds 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1227.pdf 
 Identifier    ZNB-1978-33b-1227 
 Volume    33 
307Author    H. J. Keller, R. Martin, U. TraegerRequires cookie*
 Title    Kristall-und Molekülstruktur eines  
 Abstract    "linearen 66 Festkörpers mit drei verschiedenen Metallsträngen: [Pt(dapn)2] [Pt(dapn)2Br2] [(Cu3Br5)2] (dapn = 1.2-Diaminopropan) Crystal and Molecular Structure of a Linear Chain Solid with Three Different Metal Chains: [Pt(dapn)2][Pt(dapn)2Br2][(Cu3Br5)2] (dapn = 1,2-diaminopropane) The compound {[Pt(dapn)2][Pt(dapn)2Br2]}(Cu3Br5)2, which was prepared by oxidation of Pt(dapn)2Br2 with CuBr2, crystallizes in the orthorhombic space group Bmmb (D^h), a = 5.617(4) A, b = 16.206(6) A, c = 22.00(1) A, Z = 2. The experimentally determined density is 3.22 g • cm -3 (calculated 3.40). The structure has been determined by Patterson and Fourier methods from single crystal diffractometer data and refined by least squares to R = 0.085 for 485 independent reflections. Crystals of the title compound contain halide-bridged copper and platinum chains. 
  Reference    Z. Naturforsch. 33b, 1263—1266 (1978); eingegangen am 14. Juli 1978 
  Published    1978 
  Keywords    Linear Chain Transition Metal Complexes, Crystal Structure, Molecular Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1263.pdf 
 Identifier    ZNB-1978-33b-1263 
 Volume    33 
308Author    Joachim Strähle, Ulrich Weiher, Kurt DehnickeRequires cookie*
 Title    Darstellung, Kristallstruktur und Infrarotspektrum von [MONC13 * P0C13]4 Preparation, Crystal Structure and Infrared Spectrum of [MONC13 * P0C13]4  
 Abstract    [MoNCl3 • P0C13]4 is prepared both by the reaction of MoNCl3 with POCl3 as well as by the reaction of M0CI5 with NC13 in the presence of P0C13. [MONC13 • P0C13]4 crystallizes in the monoclinic space group P2i/c with 2 tetrameric molecules in the unit cell. The crystal structure was solved by X-ray diffraction methods (R — 0.033, 1821 observed reflections). The structure consists of planar and almost square Mo4N4-eight-membered rings with alternating Mo-N bond lengths. The distorted octahedral environment of the molybdenum atoms is completed by three terminal Cl-ligands and by the oxygen atom of a POCl3 molecule, which is coordinated trans to the Mo = N triple bond. The IR spectrum is discussed with respect to the vibrational spectra of the isoelectronic niobium complex [NbOCl3 • P0C13]4. 
  Reference    Z. Naturforsch. 33b, 1347—1351 (1978); eingegangen am 12. Juni 1978 
  Published    1978 
  Keywords    Preparation, Crystal Structure, IR, Molybdenum Nitridochloride-POCl3 Solvate 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1347.pdf 
 Identifier    ZNB-1978-33b-1347 
 Volume    33 
309Author    R. D. Fischer, E. Klähne, J. KopfRequires cookie*
 Title    Halogeno-und Pseudohalogeno-tris(pentahaptocyclopentadienyl)uran(IV)- Komplexe als Lewis-Säuren: Darstellung und Struktur trigonal-bipyramidaler Uran-Organyle des Typs [(rj 5 -C5H5)3UXL] Tris(pentahaptocyclopentadienyl)uranium(IV) Halides and Pseudohalides as Lewis-Acids: Preparation and Structure of Uranium Organyls [(^-C5H5)3UXL] with Trigonal-Bipyramidal Coordination  
 Abstract    The first two examples of a novel series of organo-actinide complexes, [CpsUXL] (Cp = r/ 5 -CoH5, X = halide or pseudohalide anion, L = uncharged Lewis base), are described. The X-ray structure analysis of the system with X = NCS and L = CH3CN confirms an almost linear alignment (H3)CCNUNCS along with the coplanarity of the three Cp ring normals. The remarkable Lewis acidity of certain CpsUX-compounds appears to be essential for the formation of oligomeric species [Cp3UX]oo as well as for specific reactions of monomeric CP3UX. 
  Reference    Z. Naturforsch. 33b, 1393—1397 (1978); eingegangen am 17. Juli 1978 
  Published    1978 
  Keywords    Uranium Organyls, Cyclopentadienyl Ligand, Crystal Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1393.pdf 
 Identifier    ZNB-1978-33b-1393 
 Volume    33 
310Author    Bernd Schmidt, Walter JungRequires cookie*
 Title    Darstellung und Kristallstruktur von CaRh2B2 und CaIr2B2 Preparation and Crystal Structure of CaRh2B2 and CaIr2B2  
 Abstract    The isotypie compounds CaRh2B2 and CaIr2B2 were prepared and investigated by X-ray methods. They crystallize orthorhombic in space group Fddd-Dgft with lattice constants CaRh2B2: a = 1060.6 ± 0.4 pm, b = 924.0 ± 0.4 pm, c = 583.2 ± 0.2 pm. CaIr2B2: a = 1072.7 ± 0.4 pm, 6 = 925.7 ± 0.4 pm, c = 587.7 ± 0.2 pm. 
  Reference    Z. Naturforsch. 33b, 1430—1433 (1978); eingegangen am 21. Juli 1978 
  Published    1978 
  Keywords    Calcium Rhodium Boride, Calcium Iridium Boride, Crystal Structure 
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 TEI-XML for    default:Reihe_B/33/ZNB-1978-33b-1430.pdf 
 Identifier    ZNB-1978-33b-1430 
 Volume    33 
311Author    Albrecht MeRequires cookie*
 Title    CaAgP und CaAgAs -Zwei Verbindungen mit Fe2P-Struktur CaAgP and CaAgAs -Two Compounds with the Fe2P-Structure  
 Abstract    The compounds CaAgP and CaAgAs have been prepared and their structures have been determined. They are isotypic and crystallize in a modified Fe2P-structure (space group P62m-Dj|h) with the lattice constants: CaAgP ' a = 704,5(1) pm, c = 417,4(1) pm, CaAgAs a = 720,4(1) pm, c = 427,0(1) pm. 
  Reference    (Z. Naturforsch. 34b, 14—17 [1979]; eingegangen am 28. September 1978) 
  Published    1979 
  Keywords    Ternary Phosphide, Ternary Arsenide, Calcium, Silver, Crystal Structure 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0014.pdf 
 Identifier    ZNB-1979-34b-0014 
 Volume    34 
312Author    Volker Küllmer, Erika Röttinger, Heinrich VahrenkampRequires cookie*
 Title    Oxidation von Mercapto-Carbonyl-Mangankomplexen Oxidation of Mercapto Carbonyl Manganese Complexes  
 Abstract    Chemical oxidation of the mercapto carbonyl manganese complexes (Me3P)2(CO)3Mn-SX (1), (Me3P)2(CO)5Mn2(SX)2 (2), and (CO)8Mn2(SX)2 (3) (X = H, SnMe3) were investigated. From the SH complexes no identifiable products could be obtained. For X = SnMe3, the iodine oxidation of 2 yielded (Me3P)2(CO)5Mn2S2 (5), that of 3 gave (CO)i5Mn4S4 (7), both containing bridging disulfide ligands. The crystal structure of 7 was determined. 
  Reference    Z. Naturforsch. 34b, 224—229 (1979); eingegangen am 29. September 1978 
  Published    1979 
  Keywords    Chemical Oxidation, Mercapto Ligands, Disulfide Ligands, Crystal Structure 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0224.pdf 
 Identifier    ZNB-1979-34b-0224 
 Volume    34 
313Author    Manfred Zabel, Sigrid Wandinger, Klaus-Jürgen RangeRequires cookie*
 Title    Ternäre Chalkogenide M3M2'X2 mit Shandit-Struktur Ternary Chalcogenides M3M2'X2 with Shandite-Type Structure  
 Abstract    Metal-rich ternary chalcogenides M3M2'X2 (M = Ni, Co, Pd, Rh; M' = In, Tl, Pb, Sn; X = S, Se) with Shandite-type structure were synthesized from mixtures of the elements and/or binary components. A single-crystal investigation on Co3ln2S2 verifies the rhombo-hedral unit cell of Shandite-type compounds, originally postulated by Peacock and McAndrew (Crystal data for Co3ln2S2: Rhombohedral, space group R3m; a = 549,31 (6) pm, a = 57.89°, Z= 1; 3 Co in 3d, 1 In(l) in la, 1 In(2) in lb, 2 S in 2c with x = 0.2790). 
  Reference    Z. Naturforsch. 34b, 238—241 (1979); eingegangen am 20. Oktober 1978 
  Published    1979 
  Keywords    Metal-rich Ternary Chalcogenides, Shandite-type, Synthesis, Crystal Structure 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0238.pdf 
 Identifier    ZNB-1979-34b-0238 
 Volume    34 
314Author    Erwin Brechtel, Gerhard Cordier, Herbert SchäferRequires cookie*
 Title    Zur Darstellung und Kristallstruktur des SrZnSb2 On the Preparation and Crystal Structure of SrZnSb2  
 Abstract    SrZnSb2 has been prepared and characterized analytically and structurally. The compound crystallizes in the orthorhombic system with a = 2305 ± 5 pm, b = 437 ± 1 pm, c = 446 i 1 pm, Pnma-D|j>. Zn-and Sb-atoms form distorted fourfold pyramids, con-nected by common edges in the basis to two-dimensional sheets. These sheets are sepa-rated by double layers of Sr-atoms in which further Sb-atoms are located building four-cornered networks. 
  Reference    Z. Naturforsch. 34b, 251—255 (1979); eingegangen am 5. Oktober 1978 
  Published    1979 
  Keywords    Intermetallic Compound, Crystal Structure, Ternary Antimonide 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0251.pdf 
 Identifier    ZNB-1979-34b-0251 
 Volume    34 
315Author    Siegfried PohlRequires cookie*
 Title    von Diazadiphosphetidin-Derivaten: Fünf Kristall-und Molekülstrukturen Cis-trans Isomers of Diazadiphosphetidine Derivatives: Five Crystal and Molecular Structures  
 Abstract    The crystal structures of the compounds [R3CP(X)NR]2 (R = CH3; X = S, Te for eis 
  Reference    Z. Naturforsch. 34b, 256—261 (1979); eingegangen am 11. Oktober 1978 
  Published    1979 
  Keywords    Cis-trans Isomerism, Diazaphosphetidine Derivatives, Crystal Structures 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0256.pdf 
 Identifier    ZNB-1979-34b-0256 
 Volume    34 
316Author    Hans-Uwe Schuster, Cornelia Mues, Walter JungRequires cookie*
 Title    Darstellung und Kristallstruktur des Na2AgSb Preparation and Crystal Structure of Na2AgSb  
 Abstract    Na2AgSb crystallizes orthorhombically, space group Cmcm, with a = 929.2 pm, b = 790.3 pm, c = 577.3 pm. The structure contains Ag-Sb-zigzag-chains with -^Ag-Sb-Ag = 180° and Sb-Ag-Sb = 64.9°. 
  Reference    Z. Naturforsch. 34b, 354—355 (1979); eingegangen am 6. November 1978 
  Published    1979 
  Keywords    Intermetallic Compound, Crystal Structure, Ternary Antimonide 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0354_n.pdf 
 Identifier    ZNB-1979-34b-0354_n 
 Volume    34 
317Author    Alois Nagel, Klaus-Jürgen RangeRequires cookie*
 Title    Die Kristallstruktur von Ag7GeS5I The Crystal Structure of Ag7GeS5I  
 Abstract    The unit cell of Ag7GeSsI, a member of the argyrodite family, is cubic face-centered with a = 1072.2(7) pm and Z = 4. The anion lattice consists of three-dimensionally connected Frank-Kasper polyhedra with C. N. 12 and 16. The silver ions are statistically distributed over a number of sites with C. N. 4, 3 and 2, formed by isolated GeS4-tetrahedra, as well as isolated S 2 ~-and I~-ions. 
  Reference    Z. Naturforsch. 34b, 360—362 (1979); eingegangen am 26. Oktober 1978 
  Published    1979 
  Keywords    Silver Germanium Sulfide Iodide, Crystal Structure, Argyrodite Family 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0360_n.pdf 
 Identifier    ZNB-1979-34b-0360_n 
 Volume    34 
318Author    ChrL. TeskeRequires cookie*
 Title    Über die Darstellung und röntgenographische Untersuchung von Cu2SrGeS4 und Cu2BaGeS4 On the Preparation and X-ray Investigation of Cu2SrGeS4 and Cu2BaGeS4  
 Abstract    Single crystals of Cu2SrGeS4 and Cu2BaGeS4 were prepared by using molten bromides as solvents. The compounds crystallize isotypically to their homologous thiostannates(IV) [1, 2], (Cu2SrGeS4: Space group P32, a = 614,3, b = 614,3 and c = 1528,2 pm; Cu2BaGeS4: Space group P3i, a = 621,5, b — 621,5 and c = 1553,4 pm). The atomic parameters and interatomic distances are reported. 
  Reference    Z. Naturforsch. 34b, 386—389 (1979); eingegangen am 6. Oktober 1978 
  Published    1979 
  Keywords    Quaternary Thiogermanates(IV), Salt Melts, Crystal Structure 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0386.pdf 
 Identifier    ZNB-1979-34b-0386 
 Volume    34 
319Author    Natriumperchlorats Nac104, HansJoachim Berthold, BrigitteGabriele Kruska, Rudolf WartchowRequires cookie*
 Title    der orientierungsfehlgeordneten kubischen Hochtemperaturphase des The Crystal Structure of the Orientationally Disordered, Cubic High-temperature Phase of Sodium Perchlorate NaC104  
 Abstract    The crystal structure of the orientationally disordered, cubic high-temperature phase of NaC104 has been investigated using single crystal X-ray diffraction data. Space group Fm3m-Oj>, Z = 4, sodium and chlorine as in NaCl, oxygen in position 96 j (occupation factor 1/6). 
  Reference    Z. Naturforsch. 34b, 522—523 (1979); eingegangen am 22. Dezember 1978 
  Published    1979 
  Keywords    Sodium Perchlorate, Crystal Structure, Orientationally Disordered High-temperature Phase 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0522_n.pdf 
 Identifier    ZNB-1979-34b-0522_n 
 Volume    34 
320Author    ChrL. TeskeRequires cookie*
 Title    Darstellung und Kristallstruktur von Silber-Barium-Thiogermanat(IV). Ag2BaGeS4 Preparation and Crystal Structure of Silver-Barium-Thiogermanate(IV). Ag2BaGeS4  
 Abstract    Ag2BaGeS4 was prepared for the first time and the crystal structure determined using X-ray methods, a — b = 682,g; c = 801,7 pm, Space group I 4 2 m (No. 121) tetragonal. The atomic parameters and interatomic distances are reported and the structure is discussed. 
  Reference    Z. Naturforsch. 34b, 544—547 (1979); eingegangen am 16. Januar 1979 
  Published    1979 
  Keywords    Quaternary Thiogermanates(IV), Silver, Crystal Structure 
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 TEI-XML for    default:Reihe_B/34/ZNB-1979-34b-0544.pdf 
 Identifier    ZNB-1979-34b-0544 
 Volume    34 
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