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1	Author	J. Feldmann, Hk Miiller-Buschbaum	Requires cookie*
	Title	Kristallstrukturuntersuchung an einem Strontium-Vanadyl-Vanadat: Sr2(V 0 )V 20 8 Crystal Structure Investigation of the Strontium Vanadyl-Vanadate: Sr2( V 0 ) V 20 8
	Abstract	Single crystals of Sr2(V 0)V 20 8 have been prepared by quenching melts from higher tem peratures. This compound represents a new structure type and crystallizes with monoclinic symmetry, space group C \|h-I 2 la, a = 6.929, b = 16.246, c = 7.260 A, ß = 115.82°, Z = 4. The point positions occupied by V5+ show tetrahedral coordination. The refinement of the V4+ position led to split positions with acentric orientations of V4+ in the octahedral O2-surrounding. It results in a square pyramidal coordination with one short V -O distance typically for vanadyl groups.
	Reference	(Z. Naturforsch. 50b, 43—46 [1995]; eingegangen am 8. Juli 1994)
	Published	1995
	Keywords	Strontium, Vanadium Oxide, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0043.pdf
	Identifier	ZNB-1995-50b-0043
	Volume	50

2	Author	H., M. Üller-Buschbaum, L. Walz	Requires cookie*
	Title	Einkristallröntgenstrukturanalyse an Quecksilberchromat(VI)
	Abstract	g 3 0 2 C r 0 4 Single C rystal X -Ray S tructure D eterm ination of a M ercury C hrom ate(V I): H g30 2C r 0 4 Th. H an sen , H k. Single crystals of Hg3C r0 6 have been prepared by high pressure techniques (3600 bar oxygen, 600 °C). Hg3C r06 crystallizes with trigonal symmetry, space group D \|-P 3 212, a = 7.137(1), c = 10.017(2)Ä, Z -3. Nearly linear O -H g -O dumb-bells are connected in planes, forming strongly puckered nets of six-membered rings. Each Hg60 6 ring is centered by a C r04 tetrahedron; the C r04 tetrahedra are arranged in two equally occupied split positions.
	Reference	(Z. Naturforsch. 50b, 47—5 [1995]; eingegangen am 2. August 1994)
	Published	1995
	Keywords	Mercury, Chromium, Oxide, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0047.pdf
	Identifier	ZNB-1995-50b-0047
	Volume	50

3	Author	E. Peters, Hk Müller-Buschbaum	Requires cookie*
	Title	Ein Titan-Tantaloxid mit Ti11: Ti0 ,3 3 Ta0 ,6 7O2 (TiTa20 6)
	Abstract	Black single crystals o f Tio^Tao 670 2 have been prepared by C 0 2-LA SER techniques heating a mixture of TiO and Ta20 5 to T > 2000 °C. The titanium tantalum oxide crystallizes with tetragonaj symmetry, space group D 4 h -P 4 2/mnm, lattice constants a = 4.7344(6) A, c = 3.0504(2) A , Z = 2. Ti().33Ta0.67O 2 represents the compound TiTa20 6 with rutile structure because of the statistical distribution of Ti2+ and Ta5+. The composition of rutile-type com pounds is discussed in more general terms.
	Reference	Z. Naturforsch. 50b, 1167—1170 (1995); eingegangen am 16. Januar 1995
	Published	1995
	Keywords	Titanium, Tantalum, Oxide, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-1167.pdf
	Identifier	ZNB-1995-50b-1167
	Volume	50

4	Author	V. Ikto, R. Keimes, A. Lb Rech, M. Ewis	Requires cookie*
	Title	M g6N i16A s7 -a N ew G Phase
	Abstract	Mg6N i16A s7 (F m 3m ; a = 11.479(1) Ä; Z = 4) was prepared by heating a mixture of the ele ments and investigated by m eans of single crystal X-ray methods. The arsenide crystallizes in a m o dified Th6Mn23 type structure, similar to many ternary com pounds of the com position A 6M 16X 7, called G phases.
	Reference	Z. Naturforsch. 50b, 1275—1276 (1995); eingegangen am 6. März 1995
	Published	1995
	Keywords	Ternary Nickelarsenide, Magnesium, Crystal Structure
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	Identifier	ZNB-1995-50b-1275_n
	Volume	50

5	Author	T. Gressling, Hk Müller-Buschbaum	Requires cookie*
	Title	Zur Kristallstruktur von Ce2(W 0 4)3 On the Crystal Structure of Ce2(W 0 4)3
	Abstract	Single crystals of Ce2(W 0 4)3 have been prepared by crystallisation from molten mixtures of W 0 3 and C e 0 2. The compound shows m onoclinic symmetry, a = 7.813(4), b = 11.720(2), c = 11.586(3), ß = 109.36(3)°, Z = 4, and is isotypic to Eu2(W 0 4)3, but shows large differences of the atomic coordinates especially of oxygen. The crystal structure of Ce2(W 0 4)3 is charac terized by W (1)0 4 tetrahedra, square W (2)0 5 pyramids and a distorted capped trigonal prism of oxygen around cerium. The decrease o f the oxidation states of C e4+ or W6+ was proved by thermogravimetric and magnetic measurements as well as by calculations of the Coulomb terms of lattice energy.
	Reference	Z. Naturforsch. 50b, 1513—1516 (1995); eingegangen am 25. Mai 1995
	Published	1995
	Keywords	Cerium, Tungsten, Oxygen, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-1513.pdf
	Identifier	ZNB-1995-50b-1513
	Volume	50

6	Author	Z. Naturforsch	Requires cookie*
	Title	K34[Zn2oIn85]: Eine ternäre Auffüllungsvariante des /?-rhomboedrischen Bors
	Abstract	In the crystal structure of K34[Zn2()In85] (a = 1827.7(5) pm, c = 3980.5(8) pm, R3m , Nr. 166, Z = 3, R1 = 0.056, wR2 = 0.124) the In and Zn atoms form the /3-rhombohedral boron structure. The structure contains In84 Samson polyhedra, and clusters of 18 In and 10 Zn atoms, forming three In12 icosahedra sharing two common triangular faces. The potassium atoms occupy the centres of truncated tetrahedra -forming the Samson polyhedra -and Kasper polyhedra.
	Reference	(Z. Naturforsch. 50b, 23 [1995]; eingegangen am 16. Juni 1994)
	Published	1995
	Keywords	Crystal Structure, Intermetallic Compound, Potassium, Zinc, Indium
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0023.pdf
	Identifier	ZNB-1995-50b-0023
	Volume	50

7	Author	F.-DM. Artin, H.K M Üller-B, Uschbaum	Requires cookie*
	Title	Eine synthetische Spezies zum Mineral Howardevansit mit Eisen anstelle von Kupfer: NaFe3V 30 12
	Abstract	Single crystals of NaFe3V30 12 have been prepared by solid state reaction below the melt ing point of the reaction mixture. This compound is isotypic to the mineral Howardevansite but shows lower triclinic symmetry, space group C }-P 1 , a = 6.757(2), b = 8.155(2), c = 9.816(3) Ä, a = 106.05(2), ß = 104.401(9), y = 102.09(2)°, Z = 2. The acentric space group is caused by the sodium positions, all other atoms comply with the space group PI of Howarde vansite. The different ions are coordinated by O2-forming V 0 4 tetrahedra, FeOfi octahedra, trigonal FeOs bipyramids and irregular NaOs and NaOy polyhedra, respectively. The crystal chemistry is discussed with respect to Howardevansite.
	Reference	(Z. Naturforsch. 50b, 51—55 [1995]; eingegangen am 5. August 1994)
	Published	1995
	Keywords	Sodium, Iron, Vanadium, Oxide, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0051.pdf
	Identifier	ZNB-1995-50b-0051
	Volume	50

8	Author	G. Tams, HkM. Üller-Buschbaum	Requires cookie*
	Title	Synthese und Röntgenstrukturanalyse von Ba4LiCu0 4(C03)2 Synthesis and X -R ay Analysis of B a4L iC u 0 4( C 0 3) 2
	Abstract	Single crystals of Ba4LiCu0 4 (C0 3)2 have been prepared by C 0 2-L A SE R technique and investigated by single crystal X-ray diffraction. The compound crystallizes in the tetragonal space group D7d-I42m (No. 121), a = 5.767(1), c = 15.2614(7) A, Z = 2. It is isotypic with Ba4NaCu0 4(C03)2 and shows Li+ with octahedral and Cu3+ with square planar coordina tion by O2-. The crystal structure are discussed with respect to the related compounds Ba4N aA u 04(0 2)2 and Ba4K A u04(
	Reference	(Z. Naturforsch. 50b, 56—6 [1995]; eingegangen am 2. August 1994)
	Published	1995
	Keywords	Barium, Lithium Copper, Oxide Carbonate, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0056.pdf
	Identifier	ZNB-1995-50b-0056
	Volume	50

9	Author	E. Klüver, Hk Müller-Buschbaum	Requires cookie*
	Title	Uber einen Lanthanoid-Mangan-Apatit: Nd4M n(Si04)30 On a Lanthanoid Manganese Apatite: Nd4M n(S i04)30
	Abstract	Single crystals of Nd4M n (S i0 4)30 have been prepared by a Bi20 3 flux in closed copper tubes. The colourless crystals show hexagonal symmetry, space group C \|h-P 6 3/m, a -9,4986(9), c = 6,944(2) A, Z = 2. Nd4M n (S i0 4)30 crystallizes in the A patite structure and shows Nd3+ and Mn2+ with partly statistical distribution. A s a consequence of this, 0 (2) and 0 (4) are occupying split positions.
	Reference	(Z. Naturforsch. 50b, 61 [1995]; eingegangen am 25. Juli 1994)
	Published	1995
	Keywords	Neodymium, Manganese, Silicon, Apatite, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0061.pdf
	Identifier	ZNB-1995-50b-0061
	Volume	50

10	Author	FrankW. Heinemann, Helm Ut, Hartung, NadjaM. Aier	Requires cookie*
	Title	Kristall-und Molekülstruktur von 2-[3-(N,N-Diethylammonium)propylimino]-2-phenyl-dithioacetat Crystal and Molecular Structure of 2-[3-(N,N-Diethylammonium)propylimino]-2-phenyl-dithioacetate
	Abstract	The title compound, formed by the reaction o f acetophenone with 3-diethylamino-1-propylamine and sulfur, crystallizes in the orthorhombic space group P 2 12 12 1 (Z = 4) with lattice constants a = 818.1(2) pm, b -1225.1(2) pm and c = 1622.4(4) pm. The characterization of the molecule as a zwitterion is established by the observed bond parameters. Both spec troscopic investigations and the results of the X-ray structure determination show that a hydrogen atom is bonded to the amino nitrogen rather than to the imino nitrogen.
	Reference	(Z. Naturforsch. 50b, 81—8 [1995]; eingegangen am 9. August 1994)
	Published	1995
	Keywords	Dithioacetates, A cetophenone, Crystal Structure, Zwitterion, Betaine
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0081.pdf
	Identifier	ZNB-1995-50b-0081
	Volume	50

11	Author	Shan-Jia, C. Hena, Klaus Brychcy3, Ulrich Behrens3, Wolf-Dieter Stohrerb, Rüdiger Mews3	Requires cookie*
	Title	Strukturuntersuchungen an Perchlortriazaphosphininen (CICN)"(C12PN)3_"
	Abstract	The crystal structures of (C1CN)2(C12PN) (1) and (C1CN)(C12PN)2 (2) are reported. A
	Reference	(Z. Naturforsch. 50b, 86—9 [1995]; eingegangen am 1. Juli 1994)
	Published	1995
	Keywords	Triazaphosphinines, Crystal Structure, Bond Properties, M NDO-Calculations
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0086.pdf
	Identifier	ZNB-1995-50b-0086
	Volume	50

12	Author	Andreas Puder3, Joachim Fuchs3, D. Ieter Lentz3, KlausR. Othb	Requires cookie*
	Title	Das erste cyclische Isopolyoxoanion aus Oktaederbausteinen
	Abstract	Synthese und Strukturbestimmung von Kaliumhexatellurat(VI) K8Te6O17(OH)10.1/2 KOH • 16 H20 The First Cyclic Isopolyoxo Anion Built from Octahedra. The Structure of the Potassium hexatellurate(VI) K8Te6O 1 7 (O H) 10 • 1/2 KOH • 16 H 20 The crystal structure of the potassium hexatellurate(VI) K8Te6O 17(O H)10-1/2K O H -16H 20 features a cyclic polyoxotellurate anion with six octahedral T e 0 6 units condensed through alternate sharing of edges and vertices.
	Reference	(Z. Naturforsch. 50b, 91—9 [1995]; eingegangen am 13. April 1994)
	Published	1995
	Keywords	Polyoxo Anions, Tellurates(VI), Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0091.pdf
	Identifier	ZNB-1995-50b-0091
	Volume	50

13	Author	Klaus Diem, Thomas Hahn, Wilhelm Kuchen+, DietrichM. Ootz+, WolfgangPeter Poll, Tommes	Requires cookie*
	Title	Kristallstruktur von (CO)5CrPH2COOH und ab m/r/ö-Berechnung des hypothetischen freien Liganden [H2PCOOH]2 -ein Vergleich Crystal Structure of (C O )5CrPH2CO O H and ab initio Calculation of the Hypothetical Free Ligand [H2PC O O H ] 2 -a Comparison
	Abstract	Crystal structure analysis of (C O)5CrPH2COOH (a = 1338.2, b = 622.6, c = 1161.5 pm, ß = 96,77°, P 2 1/c, Z = 4, R -0.0330) has shown the complex to be dimerized via hydrogen-bonds of the COOH group. Geom etrical parameters of the hypothetical free ligand [H2PCO O H ]2 were calculated using the HF/3-21 G, HF/6-31G* and MP2-FU/6-31 G** basis sets. Bond lengths and bond angles o f the calculated free ligand are similar to those derived from the crystal structure analysis of the coordinated ligand and are not significantly influenced by coordination and/or intermolecular interactions.
	Reference	Z. Naturforsch. 50b, 209 (1995); eingegangen am 7. September 1994
	Published	1995
	Keywords	Crystal Structure, Chromium Complex, Phosphinoformic Acid, Hydroxycarbonylphosphine
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0209.pdf
	Identifier	ZNB-1995-50b-0209
	Volume	50

14	Author	U. Berger, V. Schultz-Coulon, W. Schnick	Requires cookie*
	Title	Ca2Sr[WN4], das erste gemischte Erdalkalimetall-nitridowolframat C a2Sr[WN4], the First Mixed Alkaline-Earth Nitridotungstate
	Abstract	The title com pound has been prepared by the reaction of Sr2N and Ca3N 2 or SrCN2 and Ca3N 2 with tungsten powder under nitrogen atmosphere at 1200 °C. The structure has been determined from single crystal X-ray data (Pbca (No. 61); Z = 8; a = 1017.7(2), b = 934.4(2), c = 1131.8(2) pm; wR = 5.56% (1150 observed reflections, 73 refined parameters)) and has been found to be isotypic to the low-temperature modification of Ba3[WN4], In contrast to the yellow or orange colour of other nitridometallates, Ca2Sr[WN4] is obtained as colourless crystals.
	Reference	Z. Naturforsch. 50b, 213 (1995); eingegangen am 8. September 1994
	Published	1995
	Keywords	Alkaline-Earth Nitridotungstate, Crystal Structure, Colour
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0213.pdf
	Identifier	ZNB-1995-50b-0213
	Volume	50

15	Author	H. Vogt, C. Frauendorf, A. Fischer, P. G. Jones	Requires cookie*
	Title	Synthese und Kristallstruktur von Tribrommethyltriphenylphosphonium-bromid und Bis(tribrommethyltriphenylphosphonium)-tribroniid-bromid Synthesis and Crystal Structure of Tribrom om ethyltriphenylphosphonium Bromide and Bis(tribrom omethyltriphenylphosphonium ) Tribromide Bromide
	Abstract	Tribromotriphenylphosphonium bromide 1 has been prepared by the reaction o f triphenyl-phosphine with tetrabromomethane in dichloromethane. Colourless crystals were obtained by recrystallization from the same solvent. The^ light-sensitive crystals change colour to yel
	Reference	Z. Naturforsch. 50b, 223 (1995); eingegangen am 28. Septem ber 1994
	Published	1995
	Keywords	Tribromomethyltriphenylphosphonium Bromide, Bis(tribromomethyltriphenylphosphonium) Tribromide Bromide, Synthesis, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0223.pdf
	Identifier	ZNB-1995-50b-0223
	Volume	50

16	Author	F.-D Martin, Hk Miiller-Buschbaum	Requires cookie*
	Title	Ein Beitrag zur Kristallchemie der Alkali-Erdalkalimetall-Oxovanadate: Synthese und Struktur von K3CaV50 15 A Contribution to the Crystal Chemistry of A lkaline-Alkaline-Earth Oxovanadates: Synthesis and Structure of K3CaV50 15
	Abstract	Single crystals of K3CaV50 15 have been prepared by crystallization from melts. The com pound shows a new structure type with orthorhombic symmetry, space group D ^-C m m a, a = 25.953(5), b = 15.688(3), c = 7.804(4) Ä , Z = 8. Typical features of K3CaV50 15 are isolated cyclic V40 12 and V60 18 groups o f corner sharing V 0 4 tetrahedra.
	Reference	Z. Naturforsch. 50b, 243 (1995); eingegangen am 13. Septem ber 1994
	Published	1995
	Keywords	Potassium, Calcium, Vanadium Oxide, Crystal Structure
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0243.pdf
	Identifier	ZNB-1995-50b-0243
	Volume	50

17	Author	H. Szillat, Hk Müller-Buschbaum	Requires cookie*
	Title	Synthesis and Crystal Structure of (Cu,Zn)3 7 5 Mo30 12
	Abstract	Single crystals of (Cu,Zn)3 75Mo30 12 have been prepared by crystallization from melts and investigated by X-ray diffractometer techniques. (Cu,Zn)3 75Mo3Oi2 crystallizes orthorhom-bically, space group D^-P212,21, Z = 4, a = 17.947(9), b = 5.092(3), c = 10.685(5) A. It is isotypic to Cu385Mo30 12. All molybdenum atoms are tetrahedrally coordinated by oxygen atoms. There are layers of C u 0 6 and Z n 0 6 octahedra, while other metal sites are occupied by copper in a deformed prismatic coordination with one oxygen atom at a remarkably greater distance from copper than the other five. Some of the zinc atoms occupy positions in chains of face-sharing octahedra with an occupancy factor of 0.75. The crystal structure is discussed with respect to the isotypic compound Cu385Mo30 12 and compounds of the type CuLnMo20 8.
	Reference	Z. Naturforsch. 50b, 247—251 (1995); eingegangen am 13. September 1994
	Published	1995
	Keywords	Crystal Structure, Copper, Molybdenum, Zinc, Oxide
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0247.pdf
	Identifier	ZNB-1995-50b-0247
	Volume	50

18	Author	H. Szillat, Hk Müller-Buschbaum	Requires cookie*
	Title	Uber das Oxomolybdat AgKCu3Mo4Oi6 mit Silber in siebenfacher Koordination About the Oxomolybdate AgKCu3Mo4O i6 with Silver in Seven-Fold Coordination
	Abstract	Single crystals of AgKCu3Mo40 16 have been prepared by crystallization from melts and investigated by X-ray diffractometer techniques. This compound crystallizes with monoclinic symmetry, space group C \|h-P 2 Je, a = 5.056(1), b = 14.546(4), c = 19.858(9) Ä, ß = 86.64(5)°, Z = 4. The crystal structure of AgKCu3Mo40 16 is closely related to K2Cu3Mo40 16 showing ribbons of edge-sharing C u 0 6 and AgÖ7 polyhedra. The ribbons are linked by tetrahedrally coordinated molybdenum and K2O 10 groups. Another kind of M o 0 4 tetrahedra occupies the cavities inside the ribbons. The crystal structure and the coordination of silver, copper, potas sium and molybdenum by oxygen are discussed with respect to K2Cu3Mo40 16.
	Reference	Z. Naturforsch. 50b, 252—256 (1995); eingegangen am 19. September 1994
	Published	1995
	Keywords	Crystal Structure, Copper, Silver, Molybdenum, Potassium
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0252.pdf
	Identifier	ZNB-1995-50b-0252
	Volume	50

19	Author	H. Szillat, Hk Müller-Buschbaum	Requires cookie*
	Title	Zur Kristallchemie eines neuen Oxomolybdats: Cu2YbMo30 12 On the Crystal Chemistry of a New Molybdenum Oxide: Cu2YbM o30 12
	Abstract	Single crystals of Cu2YbMo30 12 have been prepared by crystallization from melts and investigated by X-ray diffractometer techniques. Cu2YbMo30 12 crystallizes with monoclinic symmetry (space group C 2h -P 12i/m l, a = 5.162(2), b = 10.885(4), c = 8.699(4) A. ß -95.73(7)°, Z = 2), forming a new structure type. Typical features are layers of C u 0 6 octahedra, connected via corners and edges. These layers are linked by molybdenum and ytterbium ions along [001]. The crystal structure as well as the coordination of copper, ytterbium and molybdenum and the oxidation states of copper and molybdenum are discussed with respect to the related but not isotypic compound (Cu,Zn)3 75Mo30 12.
	Reference	Z. Naturforsch. 50b, 257—260 (1995); eingegangen am 19. September 1994
	Published	1995
	Keywords	Crystal Structure, Copper, Molybdenum, Ytterbium, Oxide
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	Identifier	ZNB-1995-50b-0257
	Volume	50

20	Author	H. Szillat, Hk Müller-Buschbaum	Requires cookie*
	Title	Synthese und Kristallstruktur eines Oxoantimonats mit Verwandtschaft zum Delafossit-Typ: Cu3MgSbl940 6 Synthesis and Crystal Structure of an Oxoantimonate with Relationship to the Delafossite Type: Cu3MgSbi 40 6
	Abstract	Single crystals of Cu3MgSb140 6 have been prepared by crystallization from melts and investigated by X-ray diffractometer techniques. Cu^MgSb] 40 6 crystallizes trigonally, space group C 3v — R3/c, a = 5.348(1), c = 34.482(8) A, Z = 6, with a Delafossite related new structure, characterized by layers containing S b 0 6 and M g06 octahedra. These layers are connected by O -C u -O dumb-bells. The crystal structure is discussed with respect to the Delafossite type.
	Reference	Z. Naturforsch. 50b, 261—264 (1995); eingegangen am 26. September 1994
	Published	1995
	Keywords	Crystal Structure, Copper, Magnesium, Antimony, Oxide
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	TEI-XML for	default:Reihe_B/50/ZNB-1995-50b-0261.pdf
	Identifier	ZNB-1995-50b-0261
	Volume	50

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