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41	Author	G. Erhard, C. Ordier, H. Erbert Schäfer, Michael Stelter	Requires cookie*
	Title	CanInSb9, eine Zintlphase mit diskreten InSb49 -Anionen On C anInSb9, a New Zintlphase with Discrete InSb49-Anions
	Abstract	CauInSb9 crystallizes in the orthorhombic system, space group Iba2 (No. 45), with a = 1189.4(5) pm, b = 1259.4(5) pm, c = 1673.0(7) pm. In the structure there are different kinds o f anions, i.e. isolated Sb3~ anions, Sb24~ dumbbells and isolated InSb49* tetrahedra. The new compound belongs to the Zintlphases.
	Reference	Z. Naturforsch. 40b, 868—871 (1985); eingegangen am 3. April 1985
	Published	1985
	Keywords	Calciumantimonidoindate, Crystal Structure, Zintlphase
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	Identifier	ZNB-1985-40b-0868
	Volume	40

42	Author	H. Eribert, W. Adle, Kurt Dehnicke, D. Ieter Fenske	Requires cookie*
	Title	(AsPh4)4[CrCl4(/J-N2S2)]4 * 8 CH2C12; Synthese, IR-Spektrum und Kristallstruktur (A sPh4)4[CrCl4(w-N2S2)]4 -8 CH 2C12; Synthesis, IR Spectrum and Crystal Structure
	Abstract	Trithiazylchloride, (NSC1)3, reacts with metallic chrom ium, with chromium hexacarbonyl, with CrCl3-3 thf, as well as with chrom ium (VI) oxide to form mixtures, in which S4N 3®[CrCl4(N 2S2) ] 0 can be identified as the major product. This com pound reacts with tetraphenylarsonium chloride in dichlorom ethane to form the title com pound, which we have characterized by IR spectroscopy and an X-ray crystal structural analysis. (A sP h4)4[CrCl4(N 2S2)]4 -8 C H 2C12 crystallizes m onoclini-cally in the space group C 2 /c with four formula units per unit cell and with the follow ing lattice constants at —100 °C: a = 2146, b = 2033, c = 3137 pm; ß = 96.0° (9918 independent observed reflexions, R = 0.064). The com pound consists o f A sPh4® ions, tetrameric anions [CrCl4(N 2S2)]44e and included C H 2C12 m olecules. The chromium atom s of the anions occupy the corners o f a nearly ideal square; they are connected via the N -atom s o f planar N 2S2-rings, which are oriented perpendicularly to the Cr4-plane. The chromium atom s com plete their distorted octahedral coordination with four terminal chlorine atom s, the axial ones o f which form short Cl---S-contacts o f average 310 pm to the S-atom s o f the N 2S2-rings.
	Reference	Z. Naturforsch. 40b, 1314—1319 (1985); eingegangen am 2. Mai 1985
	Published	1985
	Keywords	Trithiazylchloride, IR Spectra, Crystal Structure
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	Identifier	ZNB-1985-40b-1314
	Volume	40

43	Author	Siegfried Pohl, Wolfgang Saak, Detlev Haase	Requires cookie*
	Title	Darstellung und Kristallstrukturen von (Ph4P)4Sb8I28 und (Ph4P)Sb3l 10 (Ph = C6H5) Synthesis and Crystal Structures of (Ph4P)4Sb8I28 and (Ph4P)Sb3 l 1 0 (Ph = C6H 5)
	Abstract	The compounds (Ph4P)4Sb8l 28 (1) and (Ph4P)Sb,Iio (2) were prepared by the reaction of Sbl3 and Ph4PI in acetonitrile (molar ratios 2:1 and 3:1 respectively). The structures of 1 and 2 were determined from single crystal X-ray diffraction data. 1 crystallizes in the triclinic space group P I with a = 1321.7(5), b = 1346.7(5), c = 2201.8(8) pm, a = 104.18(2), ß = 99.92(2), y = 100.33(2)°; 2: monoclinic, C2/c, a = 2371.1(2), b = 745.0(1), c = 2495.1(2) pm, ß = 100.75(1)°. Whereas 1 exhibits isolated SbsI284' ions, the anions of 2 are built up of polymeric chains [Sb3I 10_]x. In both compounds the distorted Sbl6 octahedra are linked by common edges. The Sb—I distances are in the range between 277.4 and 354.8 pm (1) and between 277.4 and 342.4 pm (2). The observed structures do not only depend on stoichiometry. the nature of the counter cations, and the possibility of oligomerisation but also on the wide variety of the Sb—I bond strengths and the different bridges formed by iodine. The lone pair of Sb(III) seems to be predominantly 5s: .
	Reference	Z. Naturforsch. 42b, 1493—1499 (1987); eingegangen am 30. Juni 1987
	Published	1987
	Keywords	Iodoantimonates, Synthesis, Crystal Structure
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	Identifier	ZNB-1987-42b-1493
	Volume	42

44	Author	H.-Jürgen Meyer, Joachim Pickardt	Requires cookie*
	Title	Die Kristallstruktur von Calciumhexacyanoferrat(II)- Hexamethylentetramin-Wasser(l/l/6) Ca 2 [Fe(CN) 6 ] * C 6 H 12 N 4 * 6 H 2 0 The Crystal Structure of Calciumhexacyanoferrate(II)- Hexamethylenetetramine-Water(l/l/6) Ca 2 [Fe(CN) 6 ] * C 6 H 12 N 4 * 6 H : 0
	Abstract	Ca 2 [Fe(CN) 6 ] • C t ,H 1 2N 4 -6H 2 0 crystallizes in the monoclinic space group B2lb with a = 1130,2(4), b = 1373,5(4), c = 1353,0(4) pm and y = 97,17°. The X-ray single crystal structure determination converged at R -0.055 (2057 reflections). Each of the four Fe(CN) 6 octahedra (Z = 4) in the unit cell is coordinated by six Ca atoms with mean N CY AN — Ca distances of 253.5(3) pm. The Ca atoms are bridged by hexamethylenetetramine and water molecules.
	Reference	Z. Naturforsch. 43b, 135—137 (1988); eingegangen am 31. Juli 1987
	Published	1988
	Keywords	Crystal Structure, Hexacyanoferrate, Hexamethylenetetramine
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	Identifier	ZNB-1988-43b-0135
	Volume	43

45	Author	Walter Abriel, Hartmut Ehrhardt	Requires cookie*
	Title	Über hexakoordinierte gemischte Halogeno-Anionen des Te(IV): Kristallographische und Raman-spektroskopische Untersuchungen an Rb 2 TeBr 3 , 5 Cl 2 , 5 On Hexacoordinated Mixed Halogeno Anions of Te(IV): Crystallographic and Raman Spectroscopic Investigation of Rb 2 TeBr 3 5 C1 2 5
	Abstract	The title compound contains the anions [TeBr 3 Cl 3 ] 2_ and [TeBr 4 Cl 2 ] 2_ in a 1:1 ratio. The corresponding point symmetries, detected by Raman spectroscopic methods, are 3 m and 4/mmm, respectively. The crystal structure analysis exhibits a random distribution of these anions: K 2 PtCl 6 -type, space group Fm3m with a = 10.4602(5) Ä and Z = 4, final R = 0.036 from 178 F n (MoKa). Einführung
	Reference	Z. Naturforsch. 43b, 557—560 (1988); eingegangen am 7. Januar 1988
	Published	1988
	Keywords	Tellurates, Crystal Structure, Raman Spectra
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	Identifier	ZNB-1988-43b-0557
	Volume	43

46	Author	Gabi Reber, Jürgen Riede, Gerhard Müller	Requires cookie*
	Title	Molecular Structure of (o-Trimethylsilyl- benzyl)diphenylphosphine
	Abstract	(o-Trimethylsilylbenzyl)diphenylphosphine (1) crystallizes in the monoclinic space group P2 Jn with a = 14.088(2), b = 8.712(1), c = 16.481(2)Ä, ß = 101.63(1)°, V -1981.3Ä\ Z = 4. There is no P-Si interaction in the solid state which is also found for the solution (31 P NMR, l3 C NMR).
	Reference	Z. Naturforsch. 43b, 915—917 (1988); eingegangen am 18. März 1988
	Published	1988
	Keywords	Benzyl-phosphines, Conformation, Crystal Structure
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	Identifier	ZNB-1988-43b-0915_n
	Volume	43

47	Author	HerbertW. Roesky, Michael Zimmer, Regine Herbst, GeorgeM. Sheldrick, Prof Heinz, G. Wagner	Requires cookie*
	Title	N,N'-Bis(diphenyIphosphino)-S,S-dimethylsulfodiimin — ein Ligand für cyclische Übergangsmetallkomplexe N,N'-Bis(diphenylphosphino)-S,S-dimethylsulfodiimine — a Ligand for Cyclic Transition Metal Complexes
	Abstract	Me 2 SN 2 P 2 Ph 4 M(CO) 4 complexes (1) (M: la Cr, lb Mo, lc W) have been synthesized from Me 2 S(NPPh 2) 2 and C 7 H s M(CO) 4 . la—lc are stable at room temperature, lb crystallizes in the space group P2,2,2 with cell constants a = 2486.3(2); b = 1488.8(1); c = 882.0(1) pm.
	Reference	Z. Naturforsch. 43b, 933—936 (1988); eingegangen am 26. Februar 1988
	Published	1988
	Keywords	Crystal Structure, Chromium, Molybdenum, Tungsten
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	Identifier	ZNB-1988-43b-0933
	Volume	43

48	Author	Siegfried Pohl, Rainer Lötz, Detlev Haase, Wolfgang Saak	Requires cookie*
	Title	Iodoantimonate der Zusammensetzung A + Sb 2 I 7 : Diskrete Anionen in (Me 4 N) 4 Sb 8 I 2 8 und (Me 3 S) 4 Sb 8 I 28 , polymere Ketten in (Me 3 NCH 2 Ph)Sb 2 I 7 (Me = CH 3 , Ph = C 6 H 5 ) Iodoantimonates of Composition A~Sb 2 I 7 ~: Discrete Anions in (Me 4 N) 4 Sb 8 I 28 and (Me 3 S) 4 Sb s I 28 , Polymerie Chains in (Me 3 NCH 2 Ph)Sb 2 I 7 (Me = CH 3 , Ph -C 6 H 5 )
	Abstract	The reaction of Sbl 3 with Me 4 NI, Me ? SI, and Me^NCH^Phl in acetonitrile (molar ratios 2:1) yields (Me 4 N) 4 Sb 8 I 28 (1). (Me,S) 4 Sb K I 28 (2). and (Me,NCH 2 Ph)Sb : I 7 (3), respectively. The struc-tures of 1—3 were determined from single crystal X-ray diffraction data. 1—3 crystallize in the monoclinic space group P2,/«. 2: a -1434.2(3). b -1484.1(4). c = 2102.6(4) pm. ß = 105.4(1)°, Z = 2. 1: a = 1441.7(1), b = 1545.1(1). c = 2117.3(1) pm. ß = 106.4(1)°, Z = 2. 3: a = 1004.4(1). b = 1378.8(1). c = 1899.3(2) pm. ß = 94.2(1)°. Z = 4. The structures of 1 and 2 are very similar and consist of isolated cations and anions. The Sb s I 28
	Reference	Z. Naturforsch. 43b, 1144—1150 (1988); eingegangen am 24. Mai 1988
	Published	1988
	Keywords	Iodoantimonates, Synthesis, Crystal Structure
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	Identifier	ZNB-1988-43b-1144
	Volume	43

49	Author	CarlD. Habben, Mathias Noltemeyer	Requires cookie*
	Title	Molekül-und Kristallstruktur
	Abstract	des l,l-Diethyl-3,5-dimethyl-lA 6 ,4,2,6,3,5-dithiadiazadiborins Molecular and Crystal Structure of l,l-Diethyl-3,5-dimethyl-H 6 ,4,2,6,3,5-dithiadiazadiborine The title compound, isolated from the reaction of SS-diethyl-N,N'-bistrimethylsilylsulfodiimide and 3.5-dimethyl-l,2,4-trithiadiborolane, crystallizes in space group Pbca with cell constants a — 1218.7(6), b = 1295.8(6), c = 1455.7(9) pm, V = 2.2987 nm 3 , Z = 8, Q — 1.167 MgirT 3 . The X-ray structure was refined to R = 0.053.
	Reference	Z. Naturforsch. 43b, 1683—1684 (1988); eingegangen am 11. August 1988
	Published	1988
	Keywords	Crystal Structure, Synthesis, Dithiadiazadiborines
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	Identifier	ZNB-1988-43b-1683_n
	Volume	43

50	Author	Petra Krieger-Beck, A. Ndreas Brodbeck, Joachim Strähle	Requires cookie*
	Title	Synthesis and Structure of K2A u3, a New Phase in the System Potassium —Gold
	Abstract	K2A u 3 is obtained from the elem ents in a sealed Ta am poule as air-sensitive needles with a golden lustre. It crystallizes in the orthorhom bic space
	Reference	Z. Naturforsch. 44b, 237—239 (1989); eingegangen am 18. O ktober 1988
	Published	1989
	Keywords	Dipotassium Triauride, Synthesis, Crystal Structure
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	Identifier	ZNB-1989-44b-0237_n
	Volume	44

51	Author	Brigitte Eisenmann, Roland Zagler	Requires cookie*
	Title	Selenoantimonate
	Abstract	(V): Darstellung und Struktur von Na3SbSe4, K3SbSe4 und [Ba(en)4]2[Ba(en)3](SbSe4)2 Selenoantim onates(V): Preparation and Crystal Structure of N a3SbSe4, K3SbSe4 and [Ba(en)4]2[Ba(en)3](SbSe4) 2 The crystal structures of N a 3SbSe4, K3SbSe4 and [B a(en)4]2[B a(en)3](SbSe4)2 contain isolated tetrahedral anions SbSe43 -, which are the first exam ples o f selenoantim onates(V). Na3SbSe4
	Reference	Z. Naturforsch. 44b, 249 (1989); eingegangen am 24. Oktober 1988
	Published	1989
	Keywords	Selenoantim onates, Preparation, Crystal Structure
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	Identifier	ZNB-1989-44b-0249
	Volume	44

52	Author	HansG. Eorg Stammler, Johannes Weiss	Requires cookie*
	Title	Synthese
	Abstract	und Kristallstruktur von (S4N3)2Se2Cl10, (S4N3)2Se2CI6 und [(S4N3)SeCl5]n Synthesis and Crystal Structure of (S4N3)2Se2C l10, (S4N3)2Se2Cl6, and [(S4N 3)SeCl5]" (S4N 3)2S e2C l10, (S4N 3)2Se2Clft and [(S4N 3)SeC l5]" are formed by the reaction o f S4N 4, Se2Cl2, and SO C l2. The structures o f the three com pounds where determ ined by X-ray diffraction. The yellow crystals o f (S4N 3)2Se2C l10 are monoclinic, space group P 2,/a, a = 817.5(2) pm , b = 1790.4(5) pm, c = 843.1(6) pm, ß = 104.31(4)°, Z = 2. The Se2C l102~ anion consists o f 2 Cl-bridged distorted octahedra. (S4N 3)2Se2Cl6 forms red m onoclinic crystals, space group P2,/c, a = 1036.5(3) pm , b = 1376.5(5) pm , c = 1400.4(4) pm ,/3 = 100.65(2)°, Z = 4. In the Se2Cl62" anion the Se atoms have a square planar environm ent. The yellow crystals o f (S4N 3)SeC l5 are orthorhom bic, space group P 2 12 12 1, a = 734.2(3) pm , b — 989.4(4) pm , c = 1627.4(6) pm , Z = 4. In the SeC l5_ anion the Se atom has an octahedral environm ent o f chlorine atom s, thus forming a polym eric structure.
	Reference	Z. Naturforsch. 44b, 1483 (1989); eingegangen am 5. Mai 1989
	Published	1989
	Keywords	Thiotrithiazyl-chloroselenates, Synthesis, Crystal Structure
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	Identifier	ZNB-1989-44b-1483
	Volume	44

53	Author	SylviaM. Agull, Bernhard Neumüller, K. Urt Dehnicke	Requires cookie*
	Title	Synthese und Kristallstrukturen der Polyselenido-Mercurate (PPh4)2\|H g(Se4)2\| und \|Cs(18-Krone-6)\|2\|H g2(Se4)3l Syntheses and Crystal Structures of the Polyselenido M ercurates (PPh4)2[Hg(Se4)2] and [Cs(18-Crown-6)]2[Hg2(Se4)3]
	Abstract	(PPh4)2[Hg(Se4)J has been prepared by the reaction o f (PPh4)2[Sn(Se4)3] with H g(C H 3COO)2 in dimethylformamide (D M F) solution. [Cs(18-crown-6)]2[Hg2(Se4)3] has been prepared by the reaction o f a lithium polyselenide solution in D M F with H g(C H 3COO)2 in the presence o f CsBr and 18-crown-6. Both com pounds are obtained as dark red crystals and characterized by X-ray structure determinations. (PPh4) 2[H g(Se4) 2]: Space group P 2,/c, Z = 4, 3021 observed unique reflexions, R = 0.082. Lattice dim ensions at 20 °C: a = 1046.0(3), b = 2129.4(2), c = 2213.1(3) pm,/? = 97.62(2)°. The com pound consists o f PPh4+ ions and anions [Hg(Se4)2]2", in which the mercury atom is a spi-rocenter o f puckered HgSe4 rings. [ Cs(18-crown-6) J2[H g2(Se4)3J: Space group la, Z = 4, 2859 observed unique reflexions, R = 0.074. Lattice dimensions at 20 °C: a = 2018(1), b = 1097.0(2), c = 2317.1(5) pm, ß = 99.40(3)°. The compound forms an ion triple which originates from Cs-Se contacts o f 382 to 390 pm with the [Hg2(Se4)3]2~ ion. The latter can be described as a [FlgtSe^JJ2-ion, which has contacts with a HgSe4 fragment.
	Reference	Z. Naturforsch. 46b, 985—9 (1991); eingegangen am 12. Dezember 1990
	Published	1991
	Keywords	Polyselenido Mercurates, Synthesis, Crystal Structure
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	Identifier	ZNB-1991-46b-0985
	Volume	46

54	Author	Bernhard Neumüller	Requires cookie*
	Title	Darstellung und Kristallstruktur von [(Me3Si)2CH(7-Pr)InCll2 Synthesis and Crystal Structure o f [(Me3Si)2CH(/-Pr)InCl]2
	Abstract	The title com pound 1 has been prepared by the reaction o f z-PrlnCl, with LiC H (SiM e3)2 in diethylether at -3 0 °C. The colorless substance 1 was characterized by N M R , IR, and RE spectroscopy, as well as by mass spectrometry. 1 is dimer in solution and the solid state and crystallizes in the space group P 2 ,/c with the cell parameters a = 1206.4(3) pm, b = 905.7(2) pm, c = 1591.2(5) pm, and ß = 101.18(2)°. The unit cell contains two centrosymmetri-cal dimeric molecules.
	Reference	Z. Naturforsch. 46b, 1539—1543 (1991); eingegangen am 12. April 1991
	Published	1991
	Keywords	Diorganoindiumchloride, Synthesis, Crystal Structure
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	Identifier	ZNB-1991-46b-1539
	Volume	46

55	Author	K. Arin Ruhlandt-Senge, AlfredDirk Bacher, G. Ertraude Koellner, Birgit Siewert, Ulrich Müller	Requires cookie*
	Title	Tetraphenylphosphonium-nonachlorodivanadat(III), (PPh4)3[V2Cl9l * 7 CH2C12 Tetraphenylphosphonium Nonachlorodivanadate(III), (PPh4)3[V2Cl9] * 7 C H 2C12
	Reference	Z. Naturforsch. 47b, 814—818 (1992); eingegangen am 14. O ktober 1991
	Published	1992
	Keywords	N onachlorodivanadate, Synthesis, Crystal Structure
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	Identifier	ZNB-1992-47b-0814
	Volume	47

56	Author	G.Erhard Müller, Joachim Lachm, Jürgen Riedeb	Requires cookie*
	Title	Molekülstrukturen von (o-Brombenzyl)diphenylphosphan und l,3-Bis(diphenylphosphinomethyl)benzol M olecular Structures of (o-Bromobenzyl)diphenylphosphine and l,3-Bis(diphenylphosphinomethyl)benzene
	Reference	Z. Naturforsch. 47b, 823—828 (1992); eingegangen am 3. Februar 1992
	Published	1992
	Keywords	Benzylphosphines, Conformation, Crystal Structure
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	Identifier	ZNB-1992-47b-0823
	Volume	47

57	Author	Z. Naturforsch	Requires cookie*
	Title	Über Sulfide und Oxidsulfide des Samariums
	Abstract	Stoichiometric oxidation o f SmCl2 with sulfur in the presence o f NaCl (evacuated silica ves sel, 850 °C, 7 d) results in the formation o f A -S m -,S 3 (orthorhombic, Pnma (no. 62), a = 737.64(5), b = 397.44(3), c = 1536.26(9) pm, Z = 4, /?w = 0.017). In contrast, C ~ S m 2S3 (cubic, I4 3 d (no. 220), a = 844.71(3) pm, Z = 5.333, Rw = 0.017) is obtained upon reaction o f the
	Reference	Z. Naturforsch. 47b, 1614 (1992); eingegangen am 1. Juli 1992
	Published	1992
	Keywords	Samarium, Sulfides, Oxysulfides, Crystal Structure
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	Identifier	ZNB-1992-47b-1614
	Volume	47

58	Author	Gudrun Stieglitz, Bernhard Neumüller, K. Urt Dehnicke	Requires cookie*
	Title	Synthesen und Kristallstrukturen der Lithiumphosphide { Li(DME)[P(f-Bu)2]} 2 und [Li(DM E)PPh2l00 Syntheses and Crystal Structures of the Lithium Phosphides {Li(DME)[P(/-Bu)2]}2 and [Li(DM E)PPh2]0 0
	Abstract	The title com pounds have been prepared by the reaction o f rc-butyllithium with the corre sponding diorganophosphanes H PR 2 (R = r-Bu, Ph) in D M E solutions. Both compounds were characterized by crystal structure determinations. {Li(DM E)[P(f-Bu)2]}2: Space group P 1, Z = 1, 2027 observed unique reflections, R = 0.055. Lattice dimensions at —80 °C: a = 879.9(3), b = 986.3(1), c = 1064.0(2) pm, a = 70.69(1)°, ß = 70.63(2)°, y -69.89(2)°. The com pound forms centrosymmetric dimers o f symmetry Q with L i-P bond lengths o f 260.0 and 257.3 pm for the Li2P2 four-membered ring. [Li(DM E)PPh2]0C : Space group P 2 ,/«, Z = 4. 3437 observed unique reflections, R = 0.055. Lattice dimensions at -8 0 °C: a = 1034.8(2), b = 812.48(9), c = 1978.4(3) pm, ß = 103.30(2)°. The com pound forms polymeric chains via LiP bridges with L i-P bond lengths o f 256.3 and 254.1 pm.
	Reference	Z. Naturforsch. 48b, 156 (1993); eingegangen am 8. Oktober 1992
	Published	1993
	Keywords	Lithium Phosphides, Synthesis, Crystal Structure
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	Identifier	ZNB-1993-48b-0156
	Volume	48

59	Author	Jorge Blanco, Eduardo Gayoso, JoseManuel Vila, Miguel Gayoso, CäciliaM. Aichle, -. M. Össmer, Joachim Strähle	Requires cookie*
	Title	Synthesis and Structure of Di-I/i-acetato(0,0')-ferrocenylmethyliden- 2,4,6-trimethylaniline(N,C)-palladium(II)l
	Abstract	Di-[//-acetato(0,0')-ferrocenylmethylidene-2,4,6-trimethylaniline(N,C)-palladium(II)],
	Reference	Z. Naturforsch. 48b, 906—910 (1993); received M arch 8 1993
	Published	1993
	Keywords	Cyclometallation, Synthesis, Crystal Structure
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	Identifier	ZNB-1993-48b-0906
	Volume	48

60	Author	Enno Lork, Ulrich Behrens, G. Ünter Steinke, Rüdiger Mews	Requires cookie*
	Title	Die Kristallstruktur von trans-l,3?5-Trichloro-l,3>5-trioxo
	Abstract	1 A6, 3 A6, 5 A6,2,4,6-trithiatriazin (/?-Sulfanurchlorid) The Crystal Structure o f /raws-1,3,5-Trichloro-1,3,5-trioxo-1 X6, 3/i6, 516, 2,4,6-trithiatriazine (/?-Sulfanuric Chloride) The crystal structure o f /?-(N S(0)C l)3 is reported.
	Reference	Z. Naturforsch. 49b, 437 (1994); eingegangen am 22. November 1993
	Published	1994
	Keywords	Trichlorotrioxotrithiatriazines, Sulfanuric Chlorides, Crystal Structure
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	Identifier	ZNB-1994-49b-0437
	Volume	49

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