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1985 (1)
1Author    H. Erbert, W. Roesky, Mathias Noltem, GeorgeM. SheldrickRequires cookie*
 Title    Synthese und Struktur des Trifluoracetyldicyanomethanids Synthesis and Structure of Trifluoroacetyldicyanom ethanide  
 Abstract    A suspension of NaCN in CH3CN was treated with excess of C2F4. The resulting red solution was evaporated to dryness and a red amorphous solid remained. One part of this solid was dissolved in water and a solution of Ph4AsCl was added. During the work-up procedure two salts were isolated, yellow [Ph4A s'][C F 3C (0)C (C N)2~] l a and red [Ph4A s+][(NC)2CC(CN)C(F)NC(CN)2_] 2a. The products were characterized on the basis of field desorption mass spectroscopy for positive and negative ions, l a was further characterized by an X-ray single crystal investigation. 
  Reference    Z. Naturforsch. 40b, 883 (1985); eingegangen am 7. März 1985 
  Published    1985 
  Keywords    X-Ray, Carbanion, Fluorine, Nitrile 
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 TEI-XML for    default:Reihe_B/40/ZNB-1985-40b-0883.pdf 
 Identifier    ZNB-1985-40b-0883 
 Volume    40