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1990 (1)
1Author    Rolf Minkwitz, Volker Gerhard, Hans PreutRequires cookie*
 Title    Halogen-Pseudohalogen-Austausch an Bromsulfoniumsalzen. Dimethylthiocyansulfonium-und Dimethylselenocyansulfonium- Hexafluoroarsenat [1] Halide-Pseudohalide Exchange with Bromosulfonium Salts. Dimethylthiocyanosulfonium-and Dim ethylselenocyanosulfonium-Hexafluoroarsenate [1]  
 Abstract    The preparation and spectroscopic characterization o f the sulfonium salts (C H 3)-,SSCN+A sF 6~, (C H 3)2SSeCN + A sF 6~ and (C H 3),S N C O +A sF ^ is reported. The com ­ pounds are obtained via halide-pseudohalide exchange reactions with (C H 3)2SBr+A sF 6~ and the corresponding silver pseudohalide. In addition the crystal structure o f (C H 3)2SS C N +A sF 6~ was determined. The salt crystallizes in the orthorhombic space group Pbca with a = 1048.4(9) pm, b -1290.2(6) pm, c = 1405.1(12) pm and Z = 8. 
  Reference    Z. Naturforsch. 45b, 1625—1631 (1990); eingegangen am 19. März 1990 
  Published    1990 
  Keywords    Raman Spectra, N M R Spectra, Crystal Structure, Bromosulfonium Salts, Hexafluoroarsenate 
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 TEI-XML for    default:Reihe_B/45/ZNB-1990-45b-1625.pdf 
 Identifier    ZNB-1990-45b-1625 
 Volume    45