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1982 (1)
1Author    Fritz Preuss, Lothar OggerRequires cookie*
 Title    Alkylvanadium( V) -Verbindungen Darstellung und NMR-spektroskopische Untersuchungen Alkylvanadium(V) Compounds S\ T nthesis and NMR Spectroscopic Studies  
 Abstract    The compounds Li["C4H9V0(0«C4H9)3], Me3SiCH2V(0<C4H9)3, (CH3)2V(OSiMe3)2 and V(0'C4Hg)4 have been prepared by reaction of esters VO(OR)3(R = J C4H9, SiMes) with lithium alkyls. RV0(0'C4H9)2 species are not formed by direct alkylation of VO(O f C4H 9)3 with LiR; albeit in small yields, these compounds (R = CH3, CH 2 SiMe3) can be synthesized however from V0(0«C4H9)2C1. The 51 V, and 13 C NMR spectra of the vanadium(V) and vanadium(IV) compounds are discussed; the constants of 51 V, iH and 51 V, 13 C coupling have been determined. 
  Reference    Z. Naturforsch. 37b, 957—964 (1982); eingegangen am 15. Februar 1982 
  Published    1982 
  Keywords    Alkylvanadium(V) Compounds, Preparation, NMR Spectra 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-0957.pdf 
 Identifier    ZNB-1982-37b-0957 
 Volume    37