| | 1 | Author
| CarlD H, A. Ndreas, H. Eineb, D. Ietm, S. Talkeb, G. Eorge, M. Sheldrickb | Requires cookie* | | | Title
| Synthese und Eigenschaften von l  | | | | Abstract
| Sulfurdiimides, 2,7,3,6-Tetrahydrobenzo[b]-l,2,7,3,6-thiadiazadiborepines, 1,2,4-Trithia-3,5-diborolanes, 2,5-D ihydrobenzo[b]-1,2,5-thiadiboroles 2,5-Bisdim ethylam ino-2,5-dihydrobenzo[b]-l,2,5-thiadiborole (2) has been obtained from the diiodine-derivative by reaction with dimethyl-aminotrimethylsilane. Reaction o f 2 or 2,5-bisdim ethylam ino-r,2'-dim ethyl-2,5-dihydrobenzo[b]-thiadiborole with di-rer/-butyl-, tert-butyl-trimethylsilyl-and bistrimethylsilyl-sulfurdiimide yields the 2,7,3,6-tetrahydrobenzo[b]-1,2,7,3,6-thiadiazadiborepines (3a-3e). 'H, "B, l3C N M R , MS and analytical data and results o f analysis are given. For 3 a the X-ray structure is reported. | | | |
Reference
| Z. Naturforsch. 47b, 697—7 (1992); eingegangen am 24. Juni 1991 | | | |
Published
| 1992 | | | |
Keywords
| 2, 7, 3?6-Thiadiazadiborepinen, Kristallstruktur des 2, 7-Di-terf-butyl-3, 6-dimethyl-3, 6-dihydrobenzo-1, 2, 7, 3, 6-thiadiazadiborepins Syntheses and Properties o f 1, 2, 7, 3, 6-T hiadiazadiborepines, C rystal Structure o f 2, 7-D i-teT /-butyl-3, 6-dim ethyl-3, 6-dihydrobenzo-l, 2, 7, 3, 6-thiadiazadiborepin | | | |
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| default:Reihe_B/47/ZNB-1992-47b-0697.pdf | | | | Identifier
| ZNB-1992-47b-0697 | | | | Volume
| 47 | |
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