| | 1 | Author
| Tristram Chivers, Xiaorong Li, Masood Parvez | Requires cookie* | | | Title
| Preparation and X-Ray Structure of 3,5-Dimethyl-1,4-dichloro-1,2,6- thiadiazine-1 -oxide  | | | | Abstract
| The title compound was obtained by the reaction of 3,5-dimethyl-2//-l,2,6-thiadiazine-l,l-dioxide with PCI5 in chloroform. It crystallizes in the monoclinic system, space group P2\/c, a = 7.521(7) A, b = 8.400(4) A, c = 13.908(4) Ä, ß = 100.35(4)°, V = 864.4(8) A3, and Z = 4. The S(VI) atom lies 0.43 A out of the plane of the 7r-delocalized NCCCN unit. The mean S-N bond distance is 1.569(3) A. | | | |
Reference
| Z. Naturforsch. 53b, 532—534 (1998); received December 18 1997 | | | |
Published
| 1998 | | | |
Keywords
| Crystal Structure, 1, 2, 6-Thiadiazines, Sulfanuric Chloride | | | |
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| default:Reihe_B/53/ZNB-1998-53b-0532.pdf | | | | Identifier
| ZNB-1998-53b-0532 | | | | Volume
| 53 | |
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