| | 1 | Author
| Tristram Chivers, Masood Parvez, Peter Zoricak | Requires cookie* | | | Title
| Preparation and X-Ray Structure of 4-BrC6H4CNSC(Cl)N  | | | | Abstract
| The title compound was obtained in 82% yield by the intramolecular cyclization of 4-BrC6H4C(NSCCl3)[N(SiMe3)2] in CH2CI2 at 23°C. It crystallizes in the triclinic system, space group PI, a = 7.957(3) Ä, b = 10.864(5) A, c = 5.625(1) A, a = 95.94(3)°, ß = 97.79(2)°, 7 = 100.72(3)°, V = 469.2(3) A3, and Z -2. The bond lengths of the planar C2N2S ring indicate partial 7r-delocalization. | | | |
Reference
| Z. Naturforsch. 52b, 557—559 (1997); received September 5 1996 | | | |
Published
| 1997 | | | |
Keywords
| Crystal Structure, 1, 2, 4-Thiadiazole, Intramolecular Cyclization | | | |
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| default:Reihe_B/52/ZNB-1997-52b-0557.pdf | | | | Identifier
| ZNB-1997-52b-0557 | | | | Volume
| 52 | |
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