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1995 (1)
1Author    E. K. Yudin, K. V. Domasevitch, E. B. RusanovRequires cookie*
 Title    Crystal and Molecular Structure of Isonitrosomalonodiamido- (2,2-dipyridyl)copper(II), Chloride Monohydrate [Cu(Dipy){ONC(CONH2)2}Cl] H20  
 Abstract    The crystal and molecular structure of the complex [Cu(Dipy){NDA}Cl] • H 20 , where (NDA) = {ONC(CONH2)2}~ anion (space group P I, triclinic, with a = 7.834(1), b = 9.923(1), c = 9.952(1)A, a = 93.60(1), ß = 93.65(1), y = 92.72(1)°, Z = 2) has been determined from X-ray diffraction data. The structure was refined to R -0.029 for 2243 reflections with I>3ct(I). The coordination polyhedron of Cu2+ can be described as a distorted square pyra­ mid with a chlorine atom in the apex, and with the central atom situated 0.258(3) A above the base of the pyramid towards the chlorine atom. The complicated system of hydrogen bonding involving the water of crystallization connects copper complex units in to the chains in the c direction. 
  Reference    Z. Naturforsch. 50b, 864—866 (1995); received O ctober 17 1994 
  Published    1995 
  Keywords    Copper(II), Oximes, 2, 2-Dipyridyl, X-Ray Spectra 
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 TEI-XML for    default:Reihe_B/50/ZNB-1995-50b-0864.pdf 
 Identifier    ZNB-1995-50b-0864 
 Volume    50