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1997 (1)
1Author    WolfgangK. Läuia, Susanne Schoger2, Martin NiegerbRequires cookie*
 Title    Synthesis and Crystal Structure of Perhydro-l,4-benzoxazino[2,3-n]phenoxazine  
 Abstract    The oxidation of fra«s-2-aminocyclohexanol with nitrobenzene in the presence of catalytic amounts of iron inter alia yields perhydro-l,4-benzoxazino[2,3-n]phenoxazine (1). This com­ pound has been characterized analytically, spectroscopically and by X-ray diffraction. It is postulated that the oxidation of the 2-aminoalcohol leads to the intermediate formation of a 1,2-dione. The direct synthesis of 1 from trans-2-aminocyclohexanol and 1,2-cyclohexandione supports this hypothesis. 
  Reference    Z. Naturforsch. 52b, 801—804 (1997); eingegangen am 14. Oktober 1996 
  Published    1997 
  Keywords    Nitrobenzene, Reduction, Aniline, 2-Aminoalcohols, Catalysis 
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 TEI-XML for    default:Reihe_B/52/ZNB-1997-52b-0801.pdf 
 Identifier    ZNB-1997-52b-0801 
 Volume    52