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1Author    Atta-Ur -Rahman, Nader Daulatabadi, D. Smith+, H.E JRequires cookie*
 Title    C-13 NMR of Hecubine and Voaphylline, and a Study of Mass Spectral Fragmentation of Hecubine by Linked Scan Measurements  
 Abstract    The C-13 NMR of hecubine and voaphylline are reported. The mass spectrum of hecubine has been studied by high resolution mass meas-urements, and the fragmentation patterns fol-lowed by a study of metastable ion transitions as determined by linked scan measurements. 
  Reference    (Z. Naturforsch. 38b, 117—119 [1983]; received July 20 1982) 
  Published    1983 
  Keywords    13 C NMR Spectra, Hecubine, Voaphylline 
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 TEI-XML for    default:Reihe_B/38/ZNB-1983-38b-0117_n.pdf 
 Identifier    ZNB-1983-38b-0117_n 
 Volume    38 
2Author    MohammadAtaullah Khan, Hans Horn, Wolfgang VoelterRequires cookie*
 Title    Isolierungen und 11 C-NMR-Spektroskopie von Indoleninalkaloiden Isolation and 13 C NMR Spectroscopy of Indolenine Alkaloids  
 Abstract    The indolenine alkaloids raucaffricine and perakine were isolated from Rauwolfia caffra Sonder and their PFT 13 C{ 1 H}-NMR spectra studied for the first time. The interpretations of their spectra were accomplished in correlating with those of quinuclidine, indole, methyl-a-D-galactopyranoside, methyl-ß-D-galactopyranoside, methyl-2,6-di-0-methyl-a-D-galactopyranoside and methyl-3-O-methyl-/S-D-galactopyranoside. 
  Reference    Z. Naturforsch. 37b, 494—498 (1982); eingegangen am 13. Oktober 1981 
  Published    1982 
  Keywords    13 C NMR Spectra, Indolenine Alkaloids, Rauaffricine, Perakine 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-0494.pdf 
 Identifier    ZNB-1982-37b-0494 
 Volume    37 
3Author    Christoph Bihlmayer, Susanna Kerschl, Bernd WrackmeyerRequires cookie*
 Title    Organoborierung von Alkinylstannanen, XX [1] Oligomerisation von 1-Propinyltrimethylstannan Organoboration of Alkynylstannanes, XX [1] Oligomerisation of 1-Propynyltrimethylstannane  
 Abstract    1-Propynylstannane (1) reacts with B-ethyl-9-borabicyclo[3.3.1]nonane (10) (ratio 2:1) to giva a new butadiene derivative (11). Attempts to oligomerize 1 by organoboration with trimethyl-borane (13) (ratio 2:1) lead to a hexatriene derivative (14). A larger excess of 1 (5:1) gives a mixture of higher oligomers, analogous to 14. The proposed structures of the new compounds 11, 14 are supported by "B, 13 C and 119 Sn NMR and mass spectra. 
  Reference    Z. Naturforsch. 42b, 715—719 (1987); eingegangen am 17. Dezember 1986/20. Januar 1987 
  Published    1987 
  Keywords    Alkynylstannanes, Organoboration, u9 Sn NMR Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/42/ZNB-1987-42b-0715.pdf 
 Identifier    ZNB-1987-42b-0715 
 Volume    42 
4Author    Bernd WrackmeyerRequires cookie*
 Title    Vergleich zwischen n B-und 13 C-chemischen Verschiebungen dreifach koordinierter Borverbindungen und Carbenium-Ionen Comparison between n B and 13 C Chemical Shifts of Three-Coordinate Boron Compounds and Carbenium Ions  
 Abstract    The relationship between U B chemical shifts (<5 n B) of trigonal boranes and 13 C® chemical shifts (<5 13 C®) of carbenium ions was found to be more complex than previously reported. The trends observed allow for the comparison of (pp) n bonding between boron and suitable substituents with the TT-charge derealization in carbenium ions. In case of the ferrocenyl boranes and ferrocenyl carbenium ions the markedly different trend in the shielding of 11 B and 13 C® favours a fulvene-like structure for the substituted cyclopenta-dienyl ring in the latter. Structural features are analogously reflected by <5 U B and d 13 C® data for both series of compounds. Comparison of <5 13 C data of organoboranes and carbe-nium ions can be useful in conformational studies. Einführung 
  Reference    Z. Naturforsch. 35b, 439—446 (1980); eingegangen am 5. November/14. Dezember 1979 
  Published    1980 
  Keywords    Boranes, Carbenium Ions, 13 C NMR Spectra, U B NMR Spectra 
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 TEI-XML for    default:Reihe_B/35/ZNB-1980-35b-0439.pdf 
 Identifier    ZNB-1980-35b-0439 
 Volume    35 
5Author    Richard Goetze, Heinrich NöthRequires cookie*
 Title    Zur Kenntnis von 1.3.2-Dithiaborolen [2] Contributions to the Chemistry of Boron, 112 [1] 1,3,2-Dithiaboroles [2]  
 Abstract    Several methods were used to prepare a series of boron substituted 1,3,2-dithiaborols. The NMR data of this new class of compounds indicate in comparison to 1,3,2-dithia-borolanes, that the heterocycle can be looked at as a 6 jt-electron system. A high degree of analogy in the mass spectrometric fragmentation of dithiaborolanes and dithiaborols exists, however, the parent ion of 2-methyl dithiaborol is more stable than that of the saturated analogon. 
  Reference    Z. Naturforsch. 35b, 1212—1221 (1980); eingegangen am 30. Januar 1980 
  Published    1980 
  Keywords    1, 3, 2 -Dithiaboroles, n B NMR Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/35/ZNB-1980-35b-1212.pdf 
 Identifier    ZNB-1980-35b-1212 
 Volume    35 
6Author    *-*, Gerhard Nonnenmacher, Gottfried Zimmermann®, Otto Isaac»Requires cookie*
 Title    Elmar Flaskamp  
 Abstract    The stereochemistry of the bisaboloids in chamomile—with the exception of bisabolol-oxide C—has been elucidated. The in-vitro-examination of the mutual convertibüities of some bisaboloids gave evidence for the stereochemical accordance of the common chiral centres of all the bisaboloids. The absolute configurations of the remaining third asym-metric carbon atoms in bisabololoxide A and B have been determined by NMR spectro-metric studies in comparison with their unnatural semisynthetic epimers. All the stereo-genie centres of the bisabololoxides A and B, of (—)-a-bisabolol and of bisabolonoxide A turn out to be S-configurated. 
  Reference    Z. Naturforsch. 36b, 1023—1030 (1981); eingegangen am 30. April 1981 
  Published    1981 
  Keywords    Matricaria chamomilla L, Bisaboloids, 13 C NMR Spectra, Shift-Reagents 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-1023.pdf 
 Identifier    ZNB-1981-36b-1023 
 Volume    36 
7Author    Alfred Schmidpeter, Konstantin KaraghiosoffRequires cookie*
 Title    4.5 -Dicyano-1.3.2A 3 -diazaphospholat - ein anionisches, als Monomer stabiles 1.3.2-Diazaphosphol [1] 4,5-Dicyano-1,3,2 A 3 -diazaphospholate -an Anionic 1,3,2-Diazaphosphole, Stable as a Monomer [1]  
 Abstract    Diamino-maleodinitrile and P(NMe2)3 condense at room temperature to the dimethyl -ammonium salt of the dicyano-1,3,2-diazaphosphole. Other products may result under different conditions. Mel methylates the ambivalent diazaphosphole anion at nitrogen. 
  Reference    Z. Naturforsch. 36b, 1273—1276 (1981); eingegangen am 17. Juli 1981 
  Published    1981 
  Keywords    Dicoordinate Phosphorus, Azaphospholes, Ambivalent System, 13 C NMR Spectra, Mass Spectra 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-1273.pdf 
 Identifier    ZNB-1981-36b-1273 
 Volume    36 
8Author    Hans Geiger, Sven Reichert, KenR. MarkhamRequires cookie*
 Title    Herbacetin-3-/9-D-(2-0-/?-D-glucopyranosidoglucopyranosid)- 8-/?-D-glucopyranosid und Gossypetin-3-^-D-(2-0-^-D-glucopyranosido- glucopyranosid)-8-ß-D-glucopyranosid, zwei neue Flavonolglykoside aus Equisetum hyemale L. (Equisetaceae) Herbacetin-3-/S-D-(2-0-/3-D-glucopyranosidoglucopyranoside)-8-/?-D-glucopyranoside and Gossypetin-3-/3-D-(2-0-/9-D-glucopyranosidoglucopyranoside)-8-/3-D-glucopyTanoside, two New Flavonol-glycosides from Equisetum hyemale L. (Equisetaceae)  
 Abstract    Two new flavonol glycosides, herbacetin-and gossypetin-3-/3-D-(2-0-/3-D-glucopyrano-sidoglucopyranoside)-8-ß-D -glucopyranoside have been isolated from the aerial parts of Equisetum hyemale L. together with the known kaempferol-3-/?-D-(2-0-/S-D-glucopyrano-sidoglucopyranoside) -7-ß-D -glucopyranoside. 
  Reference    Z. Naturforsch. 37b, 504—507 (1982); eingegangen am 12. November 1981 
  Published    1982 
  Keywords    Equisetum hyemale, Equisetaceae, Herbacetin-glycosides, Gossypetin-glycosides, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-0504.pdf 
 Identifier    ZNB-1982-37b-0504 
 Volume    37 
9Author    Bernd WrackmeyerRequires cookie*
 Title    Austauschreaktionen von Tri-/i -butylethinylstannan mit Zinntetrachlorid und Zinntetrabromid -Anwendung der 119 Sn-NMR Spektroskopie Exchange Reactions between Tri-n-butyl Ethynyl Stannane and Tintetrachloride and Tintetrabromide -Application of U9 Sn NMR Spectroscopy  
 Abstract    The formation of ethynyl stannanes Xra Sn(C = C-H)4 -n (X = Cl, Br; n — 0—3) via ex-change reactions between tri-n-butvl ethynyl stannane and SnX4 is readily monitored by 119 Sn NMR spectroscopy. Advantages of il9 Sn NMR as compared with iH or 13 C NMR are discussed. The 119 Sn and 13 C NMR parameters (<5 119 Sn, <5 13 C, W (119 Sn 13 C), WpCiH)) for these reaction mixtures are reported. Tri-n-butyl ethynyl stannane and bis(tri-n-butyl-stannyl)ethyne are both obtained from the reaction of tri-n-butylstannylchloride with L^Ca in hexane in the presence of excess ethyne. 
  Reference    Z. Naturforsch. 37b, 1524—1528 (1982); eingegangen am 7. Juli 1982 
  Published    1982 
  Keywords    Exchange Reactions, Ethynyl Stannanes, 119 Sn NMR Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-1524.pdf 
 Identifier    ZNB-1982-37b-1524 
 Volume    37 
10Author    Martin Feigel+, Gerhard Hägele, >.* Axel Hinke, Gudrun TossingRequires cookie*
 Title    Beispiel: L-Menthyldichlorphosphan Applications of the 2D NMR Spectroscopy in the Organophosphorus Chemistry Example: L-Menthyldichlorophosphine  
 Abstract    2D NMR ist used to determine the X H NMR parameters of L-Menthyldichlorophosphine. 13 C NMR data are given. 
  Reference    Z. Naturforsch. 37b, 1661—1664 (1982); eingegangen am 10. August 1982 
  Published    1982 
  Keywords    m NMR Spectra, 13 C NMR Spectra, 2D NMR Spectra, L-Menthyldichlorophosphine 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-1661_n.pdf 
 Identifier    ZNB-1982-37b-1661_n 
 Volume    37 
11Author    Alicia Baldessari, EduardoG. GrosRequires cookie*
 Title    Synthesis of Some N-Alkylamino-N-vanillylpropionamides  
  Reference    Z. Naturforsch. 38b, 997—999 (1983); received April 11 1983 
  Published    1983 
  Keywords    N-Alkylamino-N-vanillylpropionamides, Synthesis, X H NMR Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/38/ZNB-1983-38b-0997.pdf 
 Identifier    ZNB-1983-38b-0997 
 Volume    38 
12Author    Rahman, Sajida Khanum, Yasmin Badar, Kaneez Fatima, Yusuf Ahmad, H.E JRequires cookie*
 Title    Atta-ur  
 Abstract    Continuing studies on the leaves of Rhazya stricta have resulted in the isolation of a new Picralima alkaloid, N h -methyl strictamine 2. 
  Reference    (Z. Naturforsch. 42b, 91—93 [1987]; received June 10 1986) 
  Published    1987 
  Keywords    Rhazya stricta, Alkaloids, Indolenine, 13 C NMR Spectra, Mass Spectra 
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 TEI-XML for    default:Reihe_B/42/ZNB-1987-42b-0091.pdf 
 Identifier    ZNB-1987-42b-0091 
 Volume    42 
13Author    KlausR. Pörschke, Richard MynottRequires cookie*
 Title    Bis(dimethyIphosphino)methan-Nickel(0)-Komplexe Bis(dimethylphosphino)methane-Nickel(0) Complexes  
 Abstract    The reaction of tris(ethene)nickel(0) with stoichiometric amounts of bis(dimethylphos-phino)methane (dmpm) in ether at low temperature affords the yellow crystalline, dinuclear complexes (dmpm)Ni 2 (QH 4) 4 (1) and (dmpm)2Ni 2 (C 2 H 4)2 (2). 2 reacts with ethyne to yield (dmpm) 2 Ni 2 (C 2 H 2) 2 (3). When 2 is treated with CO at —40 °C the primary product is (dmpm) 2 Ni 2 (CÖ) 2 (w-CO) (4). At 20 °C 4 is converted by additional CO into (dmpm) 2 Ni 2 (CO) 4 (5), which has already been characterized as the reaction product of Ni(CO) 4 with dmpm. In compounds 1—5 the bidentate dmpm acts as a bridging and not as a chelating ligand. The structures of complexes 1—4 were assigned on the basis of their 13 C and 31 P NMR spectra. 
  Reference    Z. Naturforsch. 42b, 421—424 (1987); eingegangen am 9. August 1986 
  Published    1987 
  Keywords    Carbonyl, Ethyne, Nickel(O), Phosphane, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/42/ZNB-1987-42b-0421.pdf 
 Identifier    ZNB-1987-42b-0421 
 Volume    42 
14Author    HeinzP. Fritz, Peter DavidRequires cookie*
 Title    Alkali-Polyketenenolat, ein Polyacetylen-Derivat Alkali-Polyketene-Enolate, a Polyacetylene Derivative  
 Abstract    An alkali-polyketene-enolate was made from polyketene by using aqueous bases MOH (M = Li, Na, K, Rb, Cs). The structure is proposed on the basis of IR and 13 C NMR spectra, the paramagnetic properties were investigated by EPR spectroscopy. AC conductivity measurements show a maximum conductivity of 1CT 2 Sern -1 (at 115 °C), where marked ionic participation is expected. Doping of the polyacetylene backbone with iodine gives no increase of conductivity; CV measurements indicate the presence of triiodide anions. 
  Reference    Z. Naturforsch. 43b, 671—676 (1988); eingegangen am 8. November 1987 
  Published    1988 
  Keywords    Alkali-Polyketene-Enolate, Polyketene, 13 C NMR Spectra, EPR Spectra, Conductivity 
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 TEI-XML for    default:Reihe_B/43/ZNB-1988-43b-0671.pdf 
 Identifier    ZNB-1988-43b-0671 
 Volume    43 
15Author    Helmut Burdorf, Christoph EischenbroichRequires cookie*
 Title    Metall-rr-Komplexe yon Benzolderivaten, XIII [1] Bis(methylthio-/-beiizol)chrom(0) Darstellung und Einsatz als zweizähniger Chelatligand  
 Abstract    The thioanisole-7r-complexes (methylthio-^-benzene)-(^-benzene)-chromium (2) and bis(methylthio-r/-benzene)chromium (3) have been prepared via lithiation of bis(rj-benzene)-chromium and consecutive reaction with dimethyldisulfide. *H NMR and 13 C NMR spectra of 2 and 3 as well as ESR-spectra of the corresponding radical cations 2t and 3t were recorded and analyzed. In contrast to C(»?.arene)-Si and C(r/-arene)-P bonds, C(1/.arene)-S bonds are stable to solvolysis. With (norbornadiene)tetracarbonylmolybdenum, 3 readily forms [bis(methylthio-?j-benzene)chromium]tetracarbonylmolybdenum (6) wherein 3 functions as a chelating ligand. *H and 13 C NMR evidence suggests, that at room temperature 6 undergoes rapid conformational interconversions. 
  Reference    (Z. Naturforsch. 36b, 94—101 [1981]; eingegangen am 9. September 1980) 
  Published    1981 
  Keywords    Thioanisole Sandwich Complexes, X H NMR Spectra, 13 C NMR Spectra, ESR Spectra, Coordination Chemistry 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-0094.pdf 
 Identifier    ZNB-1981-36b-0094 
 Volume    36 
16Author    Rolf Appel, Karl WaidRequires cookie*
 Title    Darstellung symmetrisch bisaminierter Carbodiphosphorane R2NPh2P=C=PPh2NR2 [1] Synthesis of Symmetrical Diaminocarbodiphosphoranes R2NPh2P=C=PPh 2 NR2 [1]  
 Abstract    The hitherto unknown symmetrical diamino carbodiphosphoranes R2NPh2P = C — PPh2NR2 (5 a-d (R = CH3, Et, nPr, nBu) are obtained in good yield by NaH dehydrohalogenation of the corresponding aminophosphonium salts R2NPh2P^CH^PPh2NR2-i+Cl-(3a-d). 3 a-d can be prepared by aminolysis of C(PPh2Cl)2 (1) or, more conveniently, directly in the three component reaction ditertiary phosphine/amine/CCU (31 P{ 1 H} and 13 C{ 1 H} NMR). 
  Reference    Z. Naturforsch. 36b, 131—134 (1981); eingegangen am 22. Mai 1980 
  Published    1981 
  Keywords    Carbodiphosphoranes, Diorganylamino Substitution, Ylid Reaction, 31 P NMR Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-0131.pdf 
 Identifier    ZNB-1981-36b-0131 
 Volume    36 
17Author    Hartmut Hlawatschek, Gertrud Kiel, Gerhard GattowRequires cookie*
 Title    Kristallstruktur und spektroskopische Untersuchungen von Dithiomalonsäurediamid H2C(CS-NH2)2: Ein Beispiel für eine Helixstruktur Crystal Structure and Spectroscopic Investigations of H2C(CS-NH2)2: An Example for an Helix Structure  
 Abstract    The crystal structure of dithiomalonediamide (H2C(CS-NH2)2) has been determined. The compound crystallizes in the orthorhombic space group P2nn, No. 34, with a — 4.354(3), b = 7.940(5) and c = 8.458(5) A. The molecules are connected by S • • • H bridges to form helices along the crystallographic a axes. 
  Reference    Z. Naturforsch. 36b, 1386—1391 (1981); eingegangen am 7. Mai 1981 
  Published    1981 
  Keywords    Crystal Structure, Vibrational Spectra, 13 C NMR Spectra, !H NMR Spectra, Dithiomalonediamide 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-1386.pdf 
 Identifier    ZNB-1981-36b-1386 
 Volume    36 
18Author    Willy GomblerRequires cookie*
 Title    Se-und 18 C-NMR-Daten von Verbindungen mit C=S-und C—Se-Doppelbindung NMR Spectroscopic Studies on Chalcogen Compounds, III 77 Se and 13 C NMR Data of Compounds Containing C=S and C=Se Double Bonds  
 Abstract    77 Se and 13 C chemical shifts of compounds of type E = C = E' (E, E' = O, S, Se), Se = CF 2 , Se=C(NH2)2, Se = C(J-Bu)2 and l,l,3,3-tetramethyl-2-indanselon are reported. The shielding of both nuclei in the C = Se entity depends strongly on the lowest electron excitation energy. 77 Se-13 C spin-spin coupling constants for the C = Se double bond are presented for the first time. The values show a strong dependence on the s-character of the carbon atom. This indicates an important Fermi contact contribution. Furthermore the influence of halogens, CF3S and CF3SS groups on the 13 C chemical shift in thiocarbonyl compounds of the type S = C(Y)SCF 3 (Y= F, Cl, Br) and S = C(SSCF 3) 2 is described. 
  Reference    Z. Naturforsch. 36b, 1561—1565 (1981); eingegangen am 27. Juli 1981 
  Published    1981 
  Keywords    77 Se NMR Spectra, 13 C NMR Spectra, Coupling Constants, Thiocarbonyl Compounds, Selenocarbonyl Compounds 
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 TEI-XML for    default:Reihe_B/36/ZNB-1981-36b-1561.pdf 
 Identifier    ZNB-1981-36b-1561 
 Volume    36 
19Author    Christian Reichardt, Ulrich RustRequires cookie*
 Title    Synthesen mit aliphatischen Dialdehyden, XXXII [1] Darstellung und Reaktionen N-substituierter 2-Aminomalondialdehyde Syntheses with Aliphatic Dialdehydes, XXXII [1] Syntheses and Reactions of N-Substituted 2-Aminomalondialdehydes  
 Abstract    The 2-amino malondialdehyde bis[dimethylacetal] 2 and some of its N-monosubstituted derivatives 7 a-d as well as the o-carboxy benzoyl malondialdehyde 12 have been prepared. With heterocyclic imonium salts these amino malondialdehyde derivatives form, by a twofold condensation reaction, the y-acylamino-substituted pentamethine cyanine dyes 15 a-c, 17, and 18a-b, the UV/Vis and 13 C NMR spectra of which are recorded with respect to the influence of the y-substituent on these spectra. 
  Reference    Z. Naturforsch. 37b, 236—245 (1982); eingegangen am 22. September 1981 
  Published    1982 
  Keywords    2-Aminomalondialdehyde Derivatives, y-Acylaminopentamethinecyanine Dyes, UV/Vis Spectra, 13 C NMR Spectra 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-0236.pdf 
 Identifier    ZNB-1982-37b-0236 
 Volume    37 
20Author    Bernd WrackmeyerRequires cookie*
 Title    U B-und 18 C-NMR-Spektroskopie von riic7o-Hexaalkyl-2.3.4.5-tetracarbahexaboranen(6) n B and 13 C NMR Spectroscopy of 7iüZo-Hexaalkyl-2,3,4,5-tetracarbahexaboranes(6)  
  Reference    Z. Naturforsch. 37b, 412—419 (1982); eingegangen am 26. Oktober 1981 
  Published    1982 
  Keywords    U B NMR Spectra, 13 C NMR Spectra, nido -Hexaalky 1 -2, 3, 4, 5-tetracarbahexaboranes( 6) 
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 TEI-XML for    default:Reihe_B/37/ZNB-1982-37b-0412.pdf 
 Identifier    ZNB-1982-37b-0412 
 Volume    37 
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