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'Chlorothio sulfonium Salts' in keywords
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1990 (1)
1Author    Rolf Minkwitz, AndreasK. Ornath, Renate Krause, Hans PreutRequires cookie*
 Title    Über die Darstellung der  
 Abstract    (Chlorthio)sulfoniumsalze [(CH3)2SSSC l]+SbF6-, I(CH3)2SSCI]+SbF6-und des isomeren [(CH3)(C I)S -S C H 3]+SbCl6-[ l ] On the Preparation o f the (Chlorothio)sulfonium Salts [(CH3):SSSCl]+SbF6-, [(CH3),SSCl]+SbF6-and the Isomer [(CH3)(C l)S -S C H 3]+SbCl6-[1] The preparation o f the stable com pounds [(CH3)2SSCl]+SbF6~ and [(CH3)2SSSCl]+SbF6~ from [(CH3)2SH ]+SbF6~ and SC12 and S2C12, resp., is reported. The isomer [(CH3)(C l)S -S C H 3]+SbCl6" is prepared from [SCl3]+SbCl6~ and CH,SH in the molar ratio 1:2. For this salt a crystal structure analysis was carried out (Space group P 2,2,2,, Z = 4,a = 750.1(4), b = 1133.7(3), c= 1614.8(3) pm). 
  Reference    Z. Naturforsch. 45b, 1637—7 (1990); eingegangen am 4. April 1990 
  Published    1990 
  Keywords    (Chlorothio)sulfonium Salts, Preparation, Crystal Structure 
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 TEI-XML for    default:Reihe_B/45/ZNB-1990-45b-1637.pdf 
 Identifier    ZNB-1990-45b-1637 
 Volume    45