| | 1 | Author
| Rolf Minkwitz, AndreasK. Ornath, Renate Krause, Hans Preut | Requires cookie* | | | Title
| Über die Darstellung der  | | | | Abstract
| (Chlorthio)sulfoniumsalze [(CH3)2SSSC l]+SbF6-, I(CH3)2SSCI]+SbF6-und des isomeren [(CH3)(C I)S -S C H 3]+SbCl6-[ l ] On the Preparation o f the (Chlorothio)sulfonium Salts [(CH3):SSSCl]+SbF6-, [(CH3),SSCl]+SbF6-and the Isomer [(CH3)(C l)S -S C H 3]+SbCl6-[1] The preparation o f the stable com pounds [(CH3)2SSCl]+SbF6~ and [(CH3)2SSSCl]+SbF6~ from [(CH3)2SH ]+SbF6~ and SC12 and S2C12, resp., is reported. The isomer [(CH3)(C l)S -S C H 3]+SbCl6" is prepared from [SCl3]+SbCl6~ and CH,SH in the molar ratio 1:2. For this salt a crystal structure analysis was carried out (Space group P 2,2,2,, Z = 4,a = 750.1(4), b = 1133.7(3), c= 1614.8(3) pm). | | | |
Reference
| Z. Naturforsch. 45b, 1637—7 (1990); eingegangen am 4. April 1990 | | | |
Published
| 1990 | | | |
Keywords
| (Chlorothio)sulfonium Salts, Preparation, Crystal Structure | | | |
Similar Items
| Find | | | DEBUG INFO
| | | | | TEI-XML for
| default:Reihe_B/45/ZNB-1990-45b-1637.pdf | | | | Identifier
| ZNB-1990-45b-1637 | | | | Volume
| 45 | |
|
