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Facet Publication Year 1980 [X]
Facet section ZfN Section B [X]

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121	Author	Peter Paetzold, Günther Schimmel	Requires cookie*
	Title	ungesättigter Stickstoffbasen Boration Reactions with the N-Oxides and m-Imines of Unsaturated Nitrogen Bases
	Abstract	-Dipolar reagents with an unsaturated CNO-or CNN-skeleton undergo 1,3-organo-boration by triorganoboranes. On the other hand, the unsaturated NNO-skeletons in azoxybenzene or nitrous-oxide are reduced to the corresponding NN-fragment by trialkyl-boranes. The 1,3-addition of aminoborane Cl2BNMe2 to the aldimineoxide PhHC = NMe-0 represents one of the rare examples of analogous reactivity of BN-and CC-double bonds. O-Borylhydroxylamines PhHCR-NMe-OBR2 are reduced by BR'3 to PhHCR-NMe-BR'2 and R'0-BR2. Similar reduction products are isolated from liquid-phase thermolysis of PhHCEt-NMe-OBEt2 (16), whereas gas-phase thermolysis of 16 gives PhCH = NMe, (EtBO)3, and C4HI0.
	Reference	Z. Naturforsch. 35b, 568—577 (1980); eingegangen am 6. Dezember 1979
	Published	1980
	Keywords	O-Borylhydroxylamines, Borylhydrazines, 2-Borylhydrazones, Organoboration, Aminoboration 1, 3
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0568.pdf
	Identifier	ZNB-1980-35b-0568
	Volume	35

122	Author	Horst Richter, Ekkehard Fluck, Wolfgang Schwarz	Requires cookie*
	Title	Reaktion von Imidodiphosphorsäuretetraphenylester mit Quecksilber(II)-oxid und Phenylquecksilberhydroxid Reaction of Imidodiphosphoric Tetraphenylester with Mercury (II) Oxide and Phenylmercuryhydroxide
	Abstract	Imidodiphosphoric Tetraphenylester, Diazadiphosphadimercuracyclododecin Reaction of imidodiphosphoric tetraphenylester with HgO yields the twelve-membered ring system 1, the properties, NMR and X-ray structural data of which are reported. A reaction mechanism is suggested. Reaction product from imidodiphosphoric tetraphenyl-ester and CöHöHgOH is N-phenylmercury-bis(phosphoric diphenylester)-imide (2).
	Reference	Z. Naturforsch. 35b, 578—583 (1980); eingegangen am 3. Dezember 1979
	Published	1980
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0578.pdf
	Identifier	ZNB-1980-35b-0578
	Volume	35

123	Author	H. Schmidbaur, G. Blaschke	Requires cookie*
	Title	Ein Ylidkomplex des Rutheniums mit drei-und viergliedrigen Metallocyclen An Ylide Complex of Ruthenium with Three-and Four-Membered Metallocycles
	Abstract	A spirometallocyclic complex of ruthenium with (CH3)2P(CH2)2, (CH3)2PCH2 and two (CH3)3P ligands (formula 5) is synthesized from (CH3)2P(CH2)2Li and frans-[(CH3)3P]4RuCl2 in the molar ratio 2:1. Two equivalents of (CHs^P are liberated and the ionic complex frans-[(CH3)3P]4Ru[CH2P(CH3)3]Cl + Cl _ is formed as a by-product. The products were characterized by analytical and spectroscopic data.
	Reference	Z. Naturforsch. 35b, 584—587 (1980); eingegangen am 11. November 1979
	Published	1980
	Keywords	Ylide Complexes, Ruthenium, Metallocycle
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0584.pdf
	Identifier	ZNB-1980-35b-0584
	Volume	35

124	Author	GerhardN. Schrauzer, Masao Hashimoto, Abdussalam Maihub	Requires cookie*
	Title	Studies on Vitamin B12 and Related Compounds, 50 Synthesis of Substituted Alkylcobalamins from Vitamin B12r and Radicals Generated from Aldehydes, Alcohols and Ethers under "Oxidizing-Reducing" Conditions. A New Synthesis of Coenzyme B12 [1]
	Reference	Z. Naturforsch. 35b, 588 (1980)
	Published	1980
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	Identifier	ZNB-1980-35b-0588
	Volume	35

125	Author	Herbert Schumann, Manfred Meissner	Requires cookie*
	Title	Organometallphosphin-substituierte Übergangsmetallkomplexe, XXVI [1] Diearbonyl-nitrosyl-organometaUphosphin-kobalt-Komplexe Organometalphosphine-Substituted Transition Metal Complexes, XXVI [1] Dicarbonyl Nitrosjd Organometal Phosphine Cobalt Complexes
	Abstract	The reactions of tricarbonyl nitrosyl cobalt with tri-feri-butylphosphine, di(teri-butyl)-trimethylsilyl-, -germyl-, -stannylphosphine, £er£-butyl-bis(trimethylsilyl)-, -(germyl)-, -(stannyl)phosphine, as well as with tris(trimethylsilyl)-, -(germyl)-, and -(stannyl-phosphine result in the elimination of one CO-ligand and the formation of corresponding dicarbonyl-nitrosyl-organometal phosphine cobalt complexes. The NMR spectra of the products are reported and discussed.
	Reference	Z. Naturforsch. 35b, 594—598 (1980); eingegangen am 5. Dezember 1979
	Published	1980
	Keywords	Organometal Phosphines, Dicarbonyl-nitrosyl Cobalt Complexes, NMR Spectra
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0594.pdf
	Identifier	ZNB-1980-35b-0594
	Volume	35

126	Author	Nils Wiberg, Heinz-Wolfgang Häring, Ulrich Schubert	Requires cookie*
	Title	Darstellung und Eigenschaften des Nitrenkomplexes (C5H5)2VNSiMe3 Zur Reaktion von Vanadocen mit Silylaziden [1] Reaction of Vanadocene with Silyl Azides Preparation and Properties of the Nitrene Complex (CsHs^VNSiMes [1]
	Abstract	Trimethy lsily lnitrene -bis (n-cyclopentadienyl) vanadium, Bis(trimethylsilylnitrene)-bis(^-cyclopentadienyl)divanadiumdichloride, Tris(^-trimethylsilylnitrene)-bis(rc-cyclopentadienyl)divanadium
	Reference	Z. Naturforsch. 35b, 599—603 (1980); eingegangen am 11. Dezember 1979
	Published	1980
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0599.pdf
	Identifier	ZNB-1980-35b-0599
	Volume	35

127	Author	Eine Neutronenbeugungsuntersuchung, M. Wintenberger, F. Tcheou, J. David, J. Lang	Requires cookie*
	Title	Verfeinerung der Struktur des Nitrids MgSiN2 - A Refinement of the Structure of the Nitride MgSiN2 -a Study by Neutron Diffraction
	Abstract	The tetrahedral wurtzite type structure of MgSiN2 has been refined with the help of neutron diffraction. The interatomic distances for Mg-N and Si-N are in complete agreement with the previously known values and the SiN4 tetrahedra in the structure are slightly deformed.
	Reference	Z. Naturforsch. 35b, 604—606 (1980); eingegangen am 27. Dezember 1979
	Published	1980
	Keywords	Nitride, Tetrahedral Structure, Neutron Diffraction
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	Identifier	ZNB-1980-35b-0604
	Volume	35

128	Author	JohannesC P M Lapidaire, WillemL. Groeneveld	Requires cookie*
	Title	Dodecamethyl Bisimidotriphosphoramide (TRIPA) A Tridentate Ligand, Part II [1]
	Abstract	In this article we describe the synthesis of TRIPA, dodecamethyl bisimidotriphosphor-amide (C12H36N7O3P3) and of its complexes with various lanthanide-nitrates. Five types of complexes have been isolated according to the compositions, X-ray diffraction patterns and IR spectra. 1. M(N03)3(TRIPA)3(acetone) M = La, Pr, Nd, 2. M(N03)3(TRIPA) M = Y, 3. M(N03)3(TRIPA)2(nitromethane) M = Er, Y, 4. M(N03)3(TRIPA)2(acetone) M = Sm, Gd, Dy, Er, Y (type I), 5. M(N03)3(TRIPA)2(acetone) M = Y (type II). The yttrium complexes, type I and II, are isomeric. IR spectra are given together with the NMR spectra. It is concluded that in all complexes the three TRIPA oxygens are coordinated, except in group 1. The nitrate groups in group 2 to 5 are involved in the coordination, particularly in the type 2 complex, where there are bidentate nitrate groups. There seems to be a difference in the conformation of the TRIPA molecules between the free ligand, the complexes in group 1, in group 2 and in group 3, 4, 5 Hygroscopic TRIPA can be easily confused with a stable mono-hydrate, TRIPA • H20.
	Reference	Z. Naturforsch. 35b, 607—613 (1980); received October 15 1979/January 9 1980
	Published	1980
	Keywords	Complex Formation, Lanthanide-nitrates, Tridentate ligand, Phosphoryl Compound, TRIPA
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0607.pdf
	Identifier	ZNB-1980-35b-0607
	Volume	35

129	Author	Hans-Friedrich Klein, Joachim Groß, Jean-Marie Bassett, Ulrich Schubert	Requires cookie*
	Title	Semicobaltate -Alkalimetall-Träger in Kohlenwasserstoffen Darstellung, Eigenschaften und Struktur von K[Co(C2H4)(PMe3)3]2 Semicobaltates -Alkali Metal Carriers in Hydrocarbons Synthesis, Properties, and Structure of K[Co(C2H4)(PMe3)3]2
	Abstract	Semicobaltates (Co-1/2) containing olefin and trimethylphosphane ligands are synthe-sized from Co(olefin)(PMe3)3 and potassium metal. The X-ray crystal structure determina-tion of the title compound shows that the unit cell contains two K atoms in equal ionic contact with the ethylene ligands of four Co(C2H4)(PMe3)3 complex units, two of which are interacting with both K atoms. In solution the semicobaltates exist in hydrocarbon solvents under argon only, while in contrast under ethylene or nitrogen atmospheres or in donor solvents disproportionation occurs to give Co(O) and Co(-I) species. Allgemeines
	Reference	Z. Naturforsch. 35b, 614—619 (1980); eingegangen am 3. Januar 1980
	Published	1980
	Keywords	Potassium-Ethylene Semicobaltate, Synthesis, Molecular Structure, Crystal Structure
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0614.pdf
	Identifier	ZNB-1980-35b-0614
	Volume	35

130	Author	Albrecht Mewis	Requires cookie*
	Title	Neue ternäre Phosphor-und Arsenverbindungen mit Zr2Fe12P7-Struktur New Ternary Compounds of Phosphorus and Arsenic with the Zr2Fei2P7-Structure
	Abstract	The ternary compounds Mg2.5Ni11.5P7, Ca2.1Ni11.9P7 and Ca2.3Nin.7As7 were structurally characterized. They are isotypic and crystallize in the Zr2Fei2P7-type (space group P 6) with the following constants:
	Reference	Z. Naturforsch. 35b, 620—625 (1980); eingegangen am 11. Januar 1980
	Published	1980
	Keywords	Phosphides, Arsenide, 2 A Elements, Nickel, Crystal Structure
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0620.pdf
	Identifier	ZNB-1980-35b-0620
	Volume	35

131	Author	Karl Berroth, Hansjürgen Mattausch, Arndt Simon	Requires cookie*
	Title	Neue reduzierte Halogenide der Lanthanoide mit kondensierten Clustern: Tb6Br7 und Er6I7 New Reduced Halides of Rare Earth Metals with Condensed Clusters: TböBr? and Er6l7
	Abstract	The new compounds TböBr? and Er6l7 are formed from the trihalides with an excess of metal in sealed tantalum containers. X-ray structure investigations [space group C2/m; Tb6Br7 (Er6I7): a = 2057.1 (2137.5), b = 379.3 (386.9), c = 1180.0 (1231.9) pm, ß = 124.59° (123.50°)] show one-dimensional regions connected by Ln-Ln bonds. The structure type can be described in terms of LnöXi2-clusters which are linked via edges of Ln6-octahedra to form double strings. The structure is derived from an FCC arrangement of halogen atoms part of which is systematically substituted by Ln6-octahedra.
	Reference	Z. Naturforsch. 35b, 626—630 (1980); eingegangen am 10. Januar 1980
	Published	1980
	Keywords	Condensed Clusters, Reduced Rare Earth Halides, Crystal Structure
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0626.pdf
	Identifier	ZNB-1980-35b-0626
	Volume	35

132	Author	Fritz Seel, Rudi Lehnert, Eckhard Bill, Alfred Trautwein	Requires cookie*
	Title	Produkte der Umsetzung des Pentacarbonyleisens mit N-substituierten Imidazolen Products of the Reaction of Pentacarbonyl Iron with N-Substituted Imidazoles
	Abstract	1-Methyl-, 1-ethyl-, 1,2-dimethyl-and 1,2,3,4-tetramethylimidazole react with penta-carbonyliron to yield [FeIm6][Fe(CO)8] (1), [FeIm6][Fe(CO)4]2 (2), [FeIm4][Fe(CO)4] (3) and Fe(Im)(CO)2 (4) (Im = substituted imidazole). The crystal and molecular structures of 1 and 2 have been determined by X-ray diffraction. For 1 and 2 agreement between calculated and measured Mössbauer absorption intensities was obtained by taking into account Debye-Waller-factors, which were derived from the X-ray diffraction experiments.
	Reference	Z. Naturforsch. 35b, 631—638 (1980); eingegangen am 18. Dezember 1979
	Published	1980
	Keywords	Imidazole Derivatives, Pentacarbonyl Iron, Crystal Structure, Molecular Structure, Mößbauer Spectra
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0631.pdf
	Identifier	ZNB-1980-35b-0631
	Volume	35

133	Author	Herbert Schumann, Manfred Meißner, Heinz-Jürgen Kroth	Requires cookie*
	Title	NMR-Untersuchungen an Organoelement(IVb)-phosphinen, VI [1] 61 Ni-NMR-Untersuchungen an Organoelement(rVb)-phosphin-8ubstituierten Komplexen des Tetracarbonylnickel NMR Studies on Organoelement(IVb)-phosphines, VI [1] 61 Ni NMR Spectroscopic Investigations on Organoelement(IVb) Substituted Complexes of Tetracarbonylnickel
	Reference	Z. Naturforsch. 35b, 639—641 (1980); eingegangen am 7. Januar 1980
	Published	1980
	Keywords	Phosphine Substituted Carbonyl Nickel Complexes, 61 Ni NMR Organometal Phosphines, Tricarbonyl Nickel Complexes, 61 Ni NMR
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0639.pdf
	Identifier	ZNB-1980-35b-0639
	Volume	35

134	Author	KlausG. Heumann, Klaus Baier, Gerald Wibmer	Requires cookie*
	Title	Chlor-Isotopenseparation an einem wasserhaltigen Zirkondioxidaustauscher Chlorine Isotope Separation Using an Hydrous Zirconium Dioxide Exchanger
	Abstract	zirconium dioxide is used in column experiments for separating the halide ions as well as for isotope fractionation of chlorine. The preparation of the zirconium dioxide particles is carried out by homogeneous hydrolysis of a zirconyl chloride solution using hexamethylenetetramine. The separation order of the halides is I -, Br -and Cl -in contrast to the inverse separation order using a strongly basic anion exchange resin. In chlorine isotope separation experiments an enrichment of 35 C1~ is found in the first fractions, whereas the last fractions show a significant enrichment of 37 C1~. This also indicates an inversion of the isotope separation compared with a strongly basic anion exchange resin. A dependence of the isotope fractionation on the concentration of the NaNC>3 solution used as eluant is found. With increasing concentration the isotope fractionation decreases. Using a 0.5 M NaN03 solution the elementary separation effect was calculated e = 6,1 • 10~ 4 . This is one of the highest isotope fractionations known in a chloride isotope exchange system. The results show that the electrolyte behaviour of isotopes is comparable to that of a series of homologous elements.
	Reference	Z. Naturforsch. 35b, 642—647 (1980); eingegangen am 11. Januar 1980
	Published	1980
	Keywords	Isotope Separation, Chlorine, Zirconium Dioxide, Column Experiments, Halide Separation Hydrous
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0642.pdf
	Identifier	ZNB-1980-35b-0642
	Volume	35

135	Author	Walter Strohmeier, Manfred Michel, Luise Weigelt	Requires cookie*
	Title	mit homogenen Ir-und Ru-Katalysatoren Selective Bulk-Hydrogenation of a,ß Unsaturated Ketones to Ketones with Homogeneous Ir and Ru Catalysts
	Abstract	a,ß Unsaturated ketones are selectively hydrogenated to ketones in homogeneous bulk-catalysis under mild conditions by iridium-and ruthenium complexes. The range of mean turnover is from 6 to 196 depending on substrate, catalyst and reaction conditions. Selectivity ketone/alcohol depends on the degree of conversion and exceeds 100 on con-version of 90%. Einleitende Bemerkungen
	Reference	Z. Naturforsch. 35b, 648—650 (1980); eingegangen am 7. Dezember 1979
	Published	1980
	Keywords	Catalysis, Homogeneous, Selective, Hydrogenation, Unsaturated Ketones
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0648.pdf
	Identifier	ZNB-1980-35b-0648
	Volume	35

136	Author	HansJoachim Berthold, Wolfgang Ludwig	Requires cookie*
	Title	Präparative und röntgenographische Untersuchungen über Cäsium-Silber-Gold(III)-Chlorid Preparation and X-ray Investigations of Cesium Silver Gold(III) Chloride
	Abstract	Cesium silver gold(III) chloride has been prepared from hydrochloric acid solutions. The composition of the preparations is variable and depends on the ratio [Au(III)]/[Ag(I)] in solution. It corresponds to the formula Cs2Agi_aAui+a;/3Cl6. In the range 0 < x < 0,64 six crystallographically different phases have been observed. Above x — 0,42 a cubic phase is obtained. The stoichiometric compound Cs2AgAuCl6 is obtained only from solutions with [Au(III)]/[Ag(I)] < 1. Reports in the literature which claim the stoichiometric compound Cs2AgAuCl6 to exist in a cubic and in a tetragonal form cannot be confirmed. Cs2AgAuCl6 crystallizes ortho-rhombically with the lattice constants a = 15,21 A, b= 15,16 A and c= 10,32 A (Z = 8).
	Reference	Z. Naturforsch. 35b, 651—656 (1980); eingegangen am 7. Februar 1980
	Published	1980
	Keywords	Cesium Silver Gold(III) Chloride, Preparation, Chemical Composition, Nonstoichiometric Phases, Lattice Constants
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0651.pdf
	Identifier	ZNB-1980-35b-0651
	Volume	35

137	Author	Oskar Glemser, Eckehard Kindler, Bernt Krebs, Rüdiger Mews, Frank-Michael Schnepel, Joachim Wegener	Requires cookie*
	Title	Über das Bis(chlor8chwefel)stick8loff-Kation N(SC1)2 + On the Bis(chlorosulfur)nitrogen Cation N(SC1)2 +
	Abstract	The synthesis of N(SC1)2+ MF6~ (M = As, Sb) is reported, the structure of N(SC1)2+ AlCLr is determined and some of the spectroscopic properties of the N(SC1)2 + cation are discussed. Das Bis(chlorschwefel)Stickstoff-Kation wurde erstmals aus NSF3 und BCI3 dargestellt [1]:
	Reference	Z. Naturforsch. 35b, 657—660 (1980); eingegangen am 15. Februar 1980
	Published	1980
	Keywords	Bis(chlorosulfur)nitrogen Hexafluoroarsenate, Hexafluoroantimonate, Tetrachloroaluminate, Vibrational Spectra
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0657.pdf
	Identifier	ZNB-1980-35b-0657
	Volume	35

138	Author	Helmut Behrens, Jochen Ellermann, EwaldF. Hohenberger	Requires cookie*
	Title	Dicarbonyl-, Carbamoyl-carbonyl-und Carbomethoxo-carbonyl-Komplexe des Rhodiums mit tri-und tetratertiären Phosphinliganden [1] Dicarbonyl-, Carbamoyl-carbonyl-and Carbomethoxo-carbonyl Complexes of Rhodium with Tri-and Tetratertiary Phosphine Ligands [1]
	Abstract	The cationic dicarbonyl complexes [Rh(CO)2(R2PCH2)3CR']PF6 (R = C6H5; R' = CH3, -CH2PR2), formed by high pressure synthesis from RhCl3(H20)3, CO and (R2PCH2)3CR' react with liquid ammonia at 20 °C to give the carbamoyl complexes Rh(CO)(CONH2)(R2PCH2)3CR'. At 100 °C in liquid ammonia the carbamoyl-carbonyl complexes Rh(CO)(CONH2)(R2PCH2)3CR' form the CO-bridged, dinuclear compounds (^-CO)2[Rh(R2PCH2)3CR']2. Upon treatment of Rh(CO)(CONH2)(R2PCH2)3CR' with CH3OH the carbomethoxo carbonyl complexes Rh(CO)(COOCH3)(R2PCH2)3CR' are obtained. The new compounds were characterised, as far as possible, by their IR, Raman and 31 P NMR spectra.
	Reference	Z. Naturforsch. 35b, 661—668 (1980); eingegangen am 10. Dezember 1979/30. Januar 1980
	Published	1980
	Keywords	Rhodium Complexes, Polytertiary Phosphines, IR Spectra, Raman Spectra, 31 P NMR Spectra
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0661.pdf
	Identifier	ZNB-1980-35b-0661
	Volume	35

139	Author	D. Chales De Beaulieu, Hk Müller-Buschbaum	Requires cookie*
	Title	Gemischtvalente Oxovanadate, I Ein neuer Strukturtyp für die Verbindung BaV10O15 Oxovanadates with Mixed Valence, I A New Crystal Structure of BaVioOis
	Abstract	BaVioOis was prepared by high temperature reaction of BaO and V2O3 in H2-atmosphere (T > 1800°). X-ray investigations of single crystals show a new structure type with octa-hedral coordination of V 3+ /V 2+ (statistical distribution) and cuboctahedral surrounding of Ba 2+ . Orthorhombic symmetry, space group D^\|-Ccmb, a = 995,8; b = 1161,8; c = 941,0; Z = 4.
	Reference	Z. Naturforsch. 35b, 669—671 (1980); eingegangen am 5. Februar 1980
	Published	1980
	Keywords	Barium, Vanadium, Oxide, Mixed Valence State, Crystal Structure
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	Identifier	ZNB-1980-35b-0669
	Volume	35

140	Author	ChrL. Teske	Requires cookie*
	Title	Ba2ZnGe2S60: Ein neues Oxidsulfid mit Tetraedergerüststruktur On Ba2ZnGe2S60. A New Oxide Sulfide with Tetrahedral Framework Structure
	Abstract	Crystal Structure, Topological Linkage of Tetrahedra Ba2ZnGe2SeO was prepared for the first time and the crystal structure determined by using single crystal X-ray methods. The space group is Dfd-P42im, tetragonal (No. 113). Lattice constants: a = 963.59 ± 0.22; c = 645.06 ± 0.25 pm. The tetrahedral framework structure is described and discussed. Zn is linked only to sulfur. The oxygen belongs to the coordination sphere of Ge and Ba.
	Reference	Z. Naturforsch. 35b, 672—675 (1980); eingegangen am 21. Januar 1980
	Published	1980
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	TEI-XML for	default:Reihe_B/35/ZNB-1980-35b-0672.pdf
	Identifier	ZNB-1980-35b-0672
	Volume	35

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