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1986[X]
61Author    Manfred Lissel, Achim GauRequires cookie*
 Title    Reaktionen mit Kaliumsuperoxid 2 [1] Spaltung von N-Acyl-glycinderivaten Reactions with Potassium Superoxide 2 [1] C leavage o f N -A cyl-glycine Derivatives  
 Abstract    Superoxide, Potassium Superoxide. N-A cyl-glycine Derivatives N -A cyl-glycine derivatives are cleaved by the action of potassium superoxide in ether or pyridine solution to give the corresponding carboxamides. 
  Reference    Z. Naturforsch. 41b, 367 (1986); eingegangen am 14. O ktober 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0367 
 Volume    41 
62Author    Piotr Milart, Janusz SepiolRequires cookie*
 Title    The Reaction of Arylidenemalonodinitriles with 1-Arylethylideneaminobenzenes. A New Synthesis of 5'-Amino-l,r:3',l"-terphenyl-2',6'-dicarbonitriles  
 Abstract    A rylidenem alonodinitriles, Schiff B ases, 5 '-A m in o-1,1 ':3',l"-terphenyl-2',6'-dicarbonitriles 
  Reference    Z. Naturforsch. 41b, 371 (1986); received October 3 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0371 
 Volume    41 
63Author    Hartmut LaatschRequires cookie*
 Title    Dimere Naphthochinone, 17* Synthesen von Stypandron und Dianellinon Dimeric Naphthoquinones, 17* Synthesis of Stypandrone and D ianellinone  
 Abstract    Naphthoquinones, Stypandrone. D ianellinone, Phenol O xidation The naphthoquinone stypandrone (2b) ist synthesized via the interm ediates 5 a , 6a and 6b. Selective monoalkylation of its hydroquinone yields the m onoether 12b, which, on phenol oxida­ tion and oxidative dealkylation, leads to 13 and dianellinone (2a). The synthesis confirms the 3.3'-dim erisation of the natural product. 
  Reference    Z. Naturforsch. 41b, 377 (1986); eingegangen am 25. Oktober 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0377 
 Volume    41 
64Author    Atta-Ur-Rahman, SohailM. Alik ', Klaus Albert, +.H E JRequires cookie*
 Title    Structural Studies on Vindolinine  
 Abstract    Catharanthus roseus. A pocynaceae. 19-S-V indolinine, 19-R-V indolinine. NM R Spectra 19-S-Vindolinine has been found to undergo an interesting isom erisation in chloroform to 19-R-vindolinine at room tem perature. N O E D S m easurem ents have been carried out on both isom ers and a I3C solid state CP-M A S spectrum recorded for 19-S-vindolinine. The structure assigned as 16-epi-19-S-vindolinine to an alkaloid isolated previously from Catharanthus roseus has been revised in the light of corrected l3C NM R values for 19-S-and 19-R-vindolinine. 
  Reference    Z. Naturforsch. 41b, 386 (1986); received Septem ber 12 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0386 
 Volume    41 
65Author    H. Erbert, W. Roesky, Jürgen Schimkowiak, FredW. AltherRequires cookie*
 Title    N O T IZ E N D arstellung und Eigenschaften des Br2V S2N 3 Synthesis and Properties of Br2VS2N3  
 Abstract    H eterocycle. N M R Spectra, C yclo-m etalla-dithiatriazene The m etallacycle Br2V S2N 3 has been obtained from the reaction o f S4N 4 with V Br, in CH 2 Br2. The r'lV NM R spectrum reveals a singulet at 445.6 ppm and the field ionisation mass spectrum shows only the m olecular ion at 317 m/e. 
  Reference    Z. Naturforsch. 41b, 393 (1986); eingegangen am 25. N ovem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0393_n 
 Volume    41 
66Author    Hubert Schmidbaur, R. Einhard Pichl, G. Erhard, M. Üller-Requires cookie*
 Title    D ie Umylidierungsreaktion von Zirkoniumtetrachlorid mit Phosphonium-yliden: Struktur von M ethyl-tris(diethylam ino)- phosphonium-Hexachlorozirkonat The Transylidation Reaction of Zirconium tetrachloride with Phosphonium Ylides: Structure of M ethyl-tris(diethylamino)- phosphonium Hexachlorozirconate  
 Abstract    Phosphorus Y lides, Zirconium Y lide Com plex, H exachlorozirconate, X-Ray The reaction between ZrCl4 and (E t2N),P = C H 2 affords the zirconium -substituted ylide [(E t2N)3PCZrCl2]2 (1). The transylidation by-pro­ duct [(E t2N)3PC H 3]Cl is trapped bv excess ZrCl4 to give the com plex salt [(Et2N)3P C H 3]2ZrClf, (2) the structure o f which was determ ined by single crystal X-ray diffraction. 
  Reference    Z. Naturforsch. 41b, 395—3 (1986); eingegangen am 4. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0395_n 
 Volume    41 
67Author    M. Arianne Bäudler, Loert De, Riese-M EyerRequires cookie*
 Title    Beiträge zur Chemie des Phosphors  
 Abstract    , 164 [1] (*-BuP)2P -P (M e)-P (f-B u P)2 -das erste Bis(cyclotriphosphano)phosphan, ein neuer P7R5-Strukturtyp Contributions to the Chemistry of Phosphorus, 164 [1] (r-BuP)2P -P (M e)-P (r-B u P)2 -The First Bis(cyclotriphosphano)phosphane, a Novel P7R 5 Structure Type B is(cyclotriphosphano)phosphane, C yclotriphosphanes, Organopolyphosphanes, Phosphinocyclotriphosphane The first bis(cyclotriphosphano)phosphane (r-BuP)2P —P (M e)-P (f-B u P)2 (1) has been syn­ thesized by reacting (?-BuP)2PSnM e3 with M ePC l2 in the molar ratio 2:1. With equim olar amounts of the reactants the chlorom ethylphosphino cyclotriphosphane (r-BuP)2P -P (M e)C l (2) has been obtained. 1 represents a novel P7R 5 structure type in addition to the types already known [4, 5]. The N M R parameters o f 1 and 2 are reported and discussed. 
  Reference    Z. Naturforsch. 41b, 399—404 (1986); eingegangen am 18. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0399 
 Volume    41 
68Author    P. Böttcher, W. FlammRequires cookie*
 Title    Darstellung und Kristallstruktur des Bis(tetramethylammonium)hexasulfids [1] Preparation and Crystal Structure of Bis(tetram ethylammonium)hexasulfide [1]  
 Abstract    Crystal Structure, P olychalcogenides B is(tetram ethylam m onium)hexasulfide has been synthesized from tetram ethylam m onium -chlorid and N a2S5 in aqueous solution. Single crystal X-ray investigations revealed its structure. It crystallizes in the m onoclinic system , space group P2/c, with two formula units in the cell. The cell constants are as follows: a = 7.353(1) A , b — 5.712(2) Ä, c = 20.318(4) Ä, ß = 99.3(1)°. 
  Reference    Z. Naturforsch. 41b, 405—408 (1986); eingegangen am 2. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0405 
 Volume    41 
69Author    Joachim Pickardt, N. Orbert, R. AutenbergRequires cookie*
 Title    Darstellung  
 Abstract    und Röntgenstrukturanalyse von (DichIoro)-(l,3,5,7-tetramethyI-2,4,6,8,9,10-hexathiaadamantan)palladium(II), PdCl2(CH3)4C4S6 Preparation and X-Ray Structure Analysis of (D ichloro)-(l,3,5,7-tetram ethyl-2,4,6,8,9,10-hexathiaadam antane)palladium (II), PdCl2(C H 3)4C4S6 Tetram ethyl-2,4,6,8,9,10-hexathiaadam antane, Palladium (II)chloride A dduct, Crystal Structure 
  Reference    Z. Naturforsch. 41b, 409 (1986); eingegangen am 9. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0409 
 Volume    41 
70Author    F. Fockenberg, A. HaasRequires cookie*
 Title    Beiträge zur Chemie perhalogenierter Thiocarbonyle, Selenocarbonyle und Selendiimine Advances in Perhalogeno Thiocarbonyl, Selenocarbonyl and Selenodiimine Chemistry  
 Abstract    Synthesis, Thiocarbonyl, Selenocarbonyl, Selenodiim ine Trifluorom ethylselenylthiocarbonyls form with CF3_"C1"SC1 or CF3SeCl the corresponding di-sulfanes or selanesulfanes. O xidation o f CF3SeC (S)X , X = CF3Se, CF3S, Cl, or Br, with 3-C1 — C6H 4 C (0) 0 0 H yields com pounds CF3S e (X) C = S = 0 . Only decom position products are obtained from (C F3S e)2CSe and Cl2, CF3SeCl, CF3SC1, or 3-C1—C6H 4 C (0) 0 0 H . The prepara­ tion o f com pounds R N = S e = N R , R = (C H 3)3Si, CF3C (0) , or CF3S 0 2, is described. Physical and spectroscopical data o f the new substances are provided. 
  Reference    Z. Naturforsch. 41b, 413 (1986); eingegangen am 25. O ktober/16. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0413 
 Volume    41 
71Author    M. Anfredo, H. Örner, K. Laus-, Peter Frank, Joachim Strähle, ProfessorD J M BevanRequires cookie*
 Title    Bildung von Nitridokomplexen durch  
 Abstract    Ammonolyse von Metallhalogeniden mit NH4+. Synthese und Struktur von (NH4)3Nb2NBr10, (NH4)3Ta2NI10 und (NH4)3W2NBr10 Formation of Nitrido Complexes by Ammonolysis of Metal Halides with NH 4+. Synthesis and Structure of (N H 4)3N b2N B r10, (N H 4)3T a2N I10 and (N H 4)3W 2N B r10 Am m onolysis, ^-N itrido-decahalogeno-dim etallateC V), Synthesis, Crystal Structure The reaction o f WC16 or R eC l5 with N H 4 C1 in a sealed glas am poule betw een 350 and 400 °C yields the hexachlorom etallates(IV) (N H 4)2MC16. M oC l5 forms (N H 4)2MoC16 at 275 °C, whereas at 420 °C (N H 4) 3M o2C19 is obtained. The salts (N H 4)2MC16 crystallize in the K2PtCl6 type struc­ ture. NbBr5, W Br6 and T a l5 undergo am m onolysis reactions with N H 4+ forming the nitrido 
  Reference    Z. Naturforsch. 41b, 423 (1986); eingegangen am 14. N ovem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0423 
 Volume    41 
72Author    Elke Conradi, Ulrich Müller, Kurt DehnickeRequires cookie*
 Title    Die Reaktionen von Trithiazylchlorid mit Molybdän, Molybdäntrioxid und Natriummolybdat. Die Kristallstruktur von PPh4[MoCl4(N3S2)] und ihre Packung  
 Abstract    The Reactions of Trithiazyl Chloride with M olybdenum, M olybdenum Trioxide and Sodium M olybdate. The Crystal Structure of PPh4[MoCl4(N3S2)] and its Packing H eribert W adle, C yclothiazeno Com plexes o f M olybdenum (V I), Preparation, Crystal Structure Trithiazylchloride, (NSC1)3, reacts with M o, M o 0 3 or N a2M o 0 4 at 75 — 80 °C to give high yields o f S4N 3 [M oCl4(N 3S2)]. By interaction with a solution o f PPh4Cl in C H 2C12 this product can be converted into PPh4[M oCl4(N 3S2)], from which [M oCl3(N 3S2) ] 2 can be obtained by reaction with gallium trichloride. The crystal structure o f PPh4 [M oCl4(N 3S2)] was determ ined by X-ray diffrac­ tion (2436 observed reflexions, R = 0.047). Crystal data: orthorhom bic, space group Pbca, Z = 8 , a = 1384.3, b = 2092.4, c = 1898.6 pm. The structure consists o f PPh4+ cations and [M oC l4(N 3 S2)]~ anions in which the Mo atom s are part o f a planar M oN 3S2 ring with M oN bond lengths o f 183 and 184 pm and nearly equal NS bond lengths (m ean value 158 pm). The PPh4® ions are arranged in centrosymmetric (PPh4®) 2 pairs in a manner that normally is encountered with doubly charged anions. The structure found for PPh4 [M oCl4(N 3S2)j differs from the known m onoclinic structures o f A sPh4[M oCl4(N 3S2)] and A sPh4[WCl4(N 3S2)]; an analysis o f their pack­ ing show ed that they form layers o f AsPh4® ions in which three phenyl groups o f every A sP h4® ion are adjacent to phenyl groups of four other A sPh4® ions. 
  Reference    Z. Naturforsch. 41b, 429 (1986); eingegangen am 9. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0429 
 Volume    41 
73Author    Jürgen KaubRequires cookie*
 Title    Darstellung und Struktur von Ba2AsSe4(OH) *2H20  
 Abstract    Barium T etraselenoarsenate(V) H ydroxide Dihydrate, Crystal Structure Ba2A sS e 4 (O H)-2 H :0 1 has been prepared by the reaction o f B a(O H) 2 with A s2S e3 in aqueous solution and its structure established by X-ray structural analysis. 1 crystallizes in the m onoclinic system , space group Cm (N o. 8) with a = 8.992(4), b = 9.967(3). c = 6.340(1) A . ß — 104.51(4). Z = 2. M = 718.5, D ber = 4.34 g-cm \ In the structure there are isolated A sSe43~ tetrahedra with Cs-symmetry and A s —Se bond lengths betw een 2.303 and 2.329 Ä . The Ba:+ ions are coordinated by 6 Se and 3 O atoms. 
  Reference    Z. Naturforsch. 41b, 436 (1986); eingegangen am 26. N ovem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0436 
 Volume    41 
74Author    Klaus Brodersen, Karl BöhmRequires cookie*
 Title    Zur Koordination von Thiocyanat in ternären Metallkomplexen Die Kristallstruktur von Ba2Cd(SCN)6 * 7 H20 On the Coordination of Thiocyanate in Ternary M etal Complexes The Crystal Structure of Ba2Cd(SCN )6 * 7 H 20  
 Abstract    Crystal Structure, Ternary M etal C om plex The title com pound was prepared by reaction o f aqueous solutions o f B a(S C N)2-3 H 20 and C d S 0 4 • 8/3 H 20 in the m olar ratio o f 3:1. The crystal structure was solved by X-ray m ethods (M r = 861.61, space group P 2 x!c, Z = 4, a = 943.6(3) pm, b = 1469.7(6) pm, c = 1827.1(6) pm , ß = 109.02(7), V -2395.4 106 pm 3, A (A gK a) = 55.83 pm, dc = 2.38 gem -3, ^ (A g K a) = 22.4 cm -1, 
  Reference    Z. Naturforsch. 41b, 439 (1986); eingegangen am 19. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0439 
 Volume    41 
75Author    Siegfried Lochschmidta, G. Erhard, M. Üllerb, BrigitteH. Uberh, Alfred SchmidpeteraRequires cookie*
 Title    ,2-Diphosphonio-diphosphirane 1,2-Diphosphonio-diphosphiranes  
  Reference    Z. Naturforsch. 41b, 444—454 (1986); eingegangen am 27. N ovem ber 1985 
  Published    1986 
  Keywords    Am inosubstituted Triphosphenium Ions, Diphosphiranes, Tetraphosphane-1, 4-diium Ions Phosphoniophosphinidene Transfer, X -R ay 
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 Identifier    ZNB-1986-41b-0444 
 Volume    41 
76Author    Klaus Angerm, Borislav Bogdanović, GudrunK. Oppetsch, Carl Krüger, RichardM. Ynott, Manfred Schwickardi, Yi-H Ung TsayRequires cookie*
 Title    Magnesiumorganische Innerkomplexe, Teil I [1] Bis(dialkylaminoalkyl)-und Bis(alkoxybutyl)magnesium-Verbindungen Organomagnesium Inner C om plexes, Part I [1] Bis(dialkylaminoalkyl)-and Bis(alkoxybutyl)m agnesium Compounds  
 Abstract    A series of magnesium inner complexes has been prepared by reacting M gH2 (prepared by homogeneous catalysis) with dialkylallyl-and -3-butenylam ines and -3-butenylethers in the p re­ sence of catalytic amounts of Z rC l4. The m onom eric nature of bis(4-m ethoxybutyl)m agnesium has been confirmed by X-ray diffraction. The analogous syntheses of bis(3-alkoxypropyl)magnesium com pounds failed: cleavage of the allyl ether with elimination of propene occurred. This cleavage reaction is accelerated by catalytic amounts of NiCl2 or ZrC l4. 
  Reference    Z. Naturforsch. 41b, 455 (1986); eingegangen am 21. N ovem ber 1985 
  Published    1986 
  Keywords    Magnesium, Inner Complexes, Crystal Structure, X-Ray 
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 Identifier    ZNB-1986-41b-0455 
 Volume    41 
77Author    A.L F E R Study, R. Je, R. Shanker, OmP. SachdevaRequires cookie*
 Title    Kinetics of Pb(IV) Oxidation of Substituted Methyl Mandelates —  
 Abstract    Kinetics of P b(IV), Substituted Methyl M andelates Lead tetra acetate (Pb(IV) or LTA) oxidation of the esters X —C,,H4—C H (O H) — C O O C H , (X = H , m -N O : , p -N O : , /?;-Cl. /?-Cl. p-B r. p-C H , and p-C :H s) gives corresponding keto esters. The reaction is first ord er in [Pb(IV)] and second order in [Ester], and is catalysed by pyridine and 2,6-lutidine. The pyridine catalysed reaction is first order each in [Pb(IV)]. [Ester] and [Pyridine]. A kinetic isotope effect is observed in oxidation of methyl m andelate for both uncatalysed reaction (kH/kD = 4.2) and pyridine catalysed reaction (kH/kD = 1.8). Activation param eters for both uncatalysed and pyridine catalysed reactions are evaluated. The results are in accord with Linear Free Energy Relationship (L .F . E .R .) and the reaction constant (o = +0.75) obtained supports proton transfer in the a -C —H bond rupture in in catalysis, as a ligand or as a base is discussed. 
  Reference    Z. Naturforsch. 41b, 467—472 (1986); received March 25/July 31 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0467 
 Volume    41 
78Author    Heinrich Lang, Gottfried Hüttner, Ibrahim JibrilRequires cookie*
 Title    Halogen-Metall-Austausch an Dihalogenphosphan-Komplexen; Synthese von Diphosphan-, Diphosphen-und Phosphiniden-Derivaten Halogen M etal Exchange; D iphosphane-, D iphosphene-, Phosphinidene-Com plexes  
 Abstract    Halogen M etal Exchange, D ihalophosphane C om plexes, Phosphinidene Complexes, D iphosphene Complexes Complexes of dihalophosphanes L "M -P (R)(H a l)2 (L"M = 16-electron fragm ent e.g. C p(C O)2Mn) undergo transform ations into phosphinidene-, diphosphene-or diphosphane-derivatives upon treatm ent with metallating agents (e.g. "BuLi/TMEDA). On the basis of many experim ental observations a unified reaction scheme is p ro ­ posed for these syntheses. The preparation and reactivity of diphosphane complexes L"M—(R)P(H) —(R)P (H) —ML" is discussed in som e detail. Analytic, spectroscopic and X-ray techniques are used to establish the results. A prom inent finding is the observation of an ex­ tremely long P —P distance (235.1(3) pm) for the sterically strained meso-[Cp(CO)2Mn]2('C4H 9)P (C H 3) —('C4H 9)P (C H 3). 
  Reference    Z. Naturforsch. 41b, 473—485 (1986); eingegangen am 6. N ovem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0473 
 Volume    41 
79Author    M.A M A Etwally—hRequires cookie*
 Title    G >-' CH, B m /z 347 Chart  
 Abstract    tm an • The Synthesis of Indeno[l ,2:4,5]pyrim ido[l,2-a]benzim idazole 487 
  Reference    Z. Naturforsch. 41b, 486 (1986) 
  Published    1986 
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 Identifier    ZNB-1986-41b-0486 
 Volume    41 
80Author    SaidA. Hm, Ed Soliman Ghozlan, Fatma Abd, El Maksoud, Abd El, A. Al, Mona Hassan, M. Oham, Ed, M. Ohamed, Hilmy ElnagdiRequires cookie*
 Title    Nitriles in Heterocyclic Synthesis: Novel Syntheses of Functionally Substituted Isoxazoles, Pyrazoles, Pyrazines and their Condensed Derivatives  
 Abstract    a-O xim inonitriles, 13C NM R Spectra, Aminoisoxazole Novel syntheses of functionally substituted isoxazoles, pyrazoles and pyrazines have been re­ ported utilizing ethyl tosyloximinoglyoxalate (1) and the pyridinium salt 2 as starting materials. 
  Reference    Z. Naturforsch. 41b, 489—495 (1986); received July 26 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0489 
 Volume    41 
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