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1992[X]
21Author    Frederick Kurzer, Zakir KapadiaRequires cookie*
 Title    Bicyclo[2.2.2]octane-2-spirocyclohexanes, Part 3 [1] Synthesis and Reactions of Mono-and Dibromospirodiisophoranes  
 Abstract    Royal Free H ospital School o f M edicine (U niversity o f L o n d o n), L ondon N W 3, G reat B ritain Z. N atu rfo rsch . 47b, 1 2 6 -138 (1992); received July 8, 1991 Bicyclo[2.2.2]octane-2-spirocyclohexanes, B icyclo[2.2.2]octane-2-spirocyclopentanes, S pirodiisophoranes, B ro m ospirodiisophorones, F av o rsk i R eactio n H alogenatio n by the a p p ro p ria te am o u n ts o f bro m in e o r N -b ro m o su ccin im id e converts spi-rodiisophora-3',6-dione successively into the 4'-ax -m o n o -an d 2',4'-diax-dibrom o-3',6-dione. T he latter is reduced by lithium alum inium h y d rid e to the co rresp o n d in g 6 ,3'-ketol. with reten ­ tion o f one or b oth b rom o-substituents, d epending on co n d itio n s. The b ro m o k eto n es undergo the F avorski ring-contraction under the influence o f alkalis to c o m p o u n d s o f the bicyclo[2.2.2]octane-2-spirocyclopentane ring-system . T he l3C N M R spectra o f the individual pro d u cts are assigned and correlated with th eir structures. 
  Reference    (Z. Naturforsch. 47b, 126 [1992]) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0126 
 Volume    47 
22Author    Requires cookie*
 Title    Crystal Structures of /7ier-Cr(pyridine)3(N 3)3 and Polymeric NaCr(pyridine)4(N 3)4. A Structure Containing //(1,3) Bridging Azido Ligands between Chromium-and Sodium-Centered Polyhedra  
  Reference    Z. Naturforsch. 47b, 139 (1992) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0139 
 Volume    47 
23Author    SolomonH. Abtem, AlexanderI. Gray, PeterG. WatermanRequires cookie*
 Title    Flavonoids from Three Ethiopian Species of Premna  
 Abstract    P hytochem istry R esearch L ab o rato ries, D e p artm en t o f P harm acy, U niversity o f Strathclyde, G lasgow G 1 1XW, S cotland. U .K . Z. N atu rfo rsch . 47b, 1 4 4 -147 (1992); received Ju n e 26. 1991 V erbenaceae, Premna, Polyoxygenated F lavonoids T w o novel h epta-oxygenated flavonols have been isolated from the aerial p arts o f Premna oligotricha and identified, prim arily on the basis o f N M R spectroscopy, as 3,5,5'-trihydroxy-6,7,3',4'-tetram ethoxyflavone (2) and 3,5,7,5'-tetrahydroxy-6,3',4'-trim ethoxyflavone (3). K now n flavonoids, with low er levels o f oxygenation were obtain ed from tw o o th e r Premna species, P. schimperi and P. recinosa. 
  Reference    Z. Naturforsch. 47b, 144 (1992) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0144 
 Volume    47 
24Author    Dieter LentzRequires cookie*
 Title    Cycloadditionsreaktion von Trifluorm ethylisocyanid an Diphenylethin Cycloaddition Reaction o f Trifluoromethyl Isocyanide to Diphenyl Ethyne  
  Reference    Z. Naturforsch. 47b, 148—150 (1992); eingegangen am 8. Juli 1991 
  Published    1992 
  Keywords    Trifluoromethyl Isocyanide, Cycloaddition Reaction, l, 2-Diphenyl-3, 4-bis(trifluoromethylimino)-cyclo-butene Crystal Structure 
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 Identifier    ZNB-1992-47b-0148_n 
 Volume    47 
25Author    W. S. Sheldrick, H.-G BraunbeckRequires cookie*
 Title    Darstellung und Kristallstruktur von Rb2Sn2S e5, ein Rubidium- Selenostannat(IV ) mit Raumnetzstruktur Preparation and Crystal Structure of Rb2Sn2Se5, a Rubidium Selenostannate(IV) with Framework Structure  
 Abstract    Z. N a tu rfo rsc h . 47b, 151 -153 (1992); eingegangen am 2 0 . Juni 1991 R ubidium S elenostannate(IV), M ethanolotherm al Synthesis, C rystal S tructure, P en ta-co o rd in ated Tin M ethanolotherm al reaction o f R b 2 C 0 3 with SnSe2 in the presence o f BaSe at 160 °C an d 13 bar yields R b 2S n2Se5, the stru ctu re o f w hich was established by X -ray analysis. The crystal stru c­ ture contains polyanions [Sn-jSej2-]^, w hich dis­ play a fram ew ork stru ctu re. The a n io n stru ctu re is built up from trigon al SnSe5 b ipyram ids, linked together via one co rn er an d tw o edges. T his leads to the form ation o f channels parallel to the 6 -axis, which contain the rub id iu m cations. T he crystal structure is isostructural to th a t o f T l2Sm S 5. 
  Reference    Z. Naturforsch. 47b, 151 (1992) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0151_n 
 Volume    47 
26Author    Werner Wolfsberger, Wolfgang Burkart, Helmut WernerRequires cookie*
 Title    Darstellung und Charakterisierung einiger ß)-Cyanalkyldiorganophosphane Preparation and Characterization of Some a>-Cyanoalkyldiorgano Phosphines  
 Abstract    In stitu t für A norganische C hem ie der U n iv ersität W ürzburg, Am H ubland, D-W -8700 W ü rzburg 
  Reference    Z. Naturforsch. 47b, 155 (1992) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0155 
 Volume    47 
27Author    Anton Meller, G. Ünter, Ossig, W. Alter Maringgele, M. Athias Noltemeyer, Dietmar Stalke, Regine Herbst-Irm, Stefanie Er, GeorgeM. Freitag, SheldrickRequires cookie*
 Title    Reaktionen von Germylenen mit Säureaziden Reactions of Germylenes with Acid Azides  
  Reference    Z. Naturforsch. 47b, 162 (1992) 
  Published    1992 
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 Identifier    ZNB-1992-47b-0162 
 Volume    47 
28Author    H. W. Roesky, T. R. Aubold, M. Noltemeyer, M. Witt, R. BohraRequires cookie*
 Title      
 Abstract    Eight-Membered M etallacyclophosphazene, X-Ray The reaction o f C lS 0 2N = PPh2Cl (1) with N H 3 yields H 2N S 0 2N = PPh2N H 2 (2). This com ­ 
  Reference    Z. Naturforsch. 47b, 171 (1992); eingegangen am 9. Januar/3. September 1991 
  Published    1992 
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 Identifier    ZNB-1992-47b-0171 
 Volume    47 
29Author    WilhelmF M Aier, FeliciaA. EtzkornbRequires cookie*
 Title    Hinweise zur thermodynamischen Kontrolle von relativen Hydriergeschwindigkeiten an Platin Indications to a Thermodynamic Control of the Relative Rate of Hydrogenation on Platinum  
 Abstract    The relative rate o f hydrogenation o f various alkenes has been determined by competition experiments in the gas phase on platinum films. Despite big structural differences in the al­ kenes there is a good correlation o f the relative rate o f hydrogenation with the calculated heat o f hydrogen atom addition to the double bond, indicating thermodynamic control o f this reac­ tion. 
  Reference    Z. Naturforsch. 47b, 175—178 (1992); eingegangen am 9. Juli/9. September 1991 
  Published    1992 
  Keywords    Heterogeneous Catalysis, Alkene Hydrogenation, Platinum Films, Gas Phase, Reaction Kinetics 
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 Identifier    ZNB-1992-47b-0175 
 Volume    47 
30Author    A. Dalbert Lossin, Gerd Meyer, R. Obert Fuchs, Joachim SträhleRequires cookie*
 Title    [Sm(CH3C 0 0 )3 (H 20)2] * CH 3COOH, ein Essigsäureaddukt des Samarium(III)-acetatdihydrates [Sm(CH3C0 0 )3(H 20 )2] * CH 3COOH, an Acetic Acid Adduct o f Sam arium (III) Acetate Dihydrate  
 Abstract    The crystal structure o f the acetic acid adduct o f the so far unknown samarium(III) acetate dihydrate was determined from single-crystal four-circle diffractometer data. It has the com ­ position [Sm (CH 3C 0 0)3 (H 20) 2] C H 3C 0 0 H containing {[Sm (CH3C 0 0)3 (H 20) 2]}2 dimers and crystallizes in the trigonal system, R 3, a = 2695.1(3), c = 1030.8(4) pm, Vm = 216.97(5) cm 3/m ol, R = 0.041, Rw = 0.030. 
  Reference    Z. Naturforsch. 47b, 179—182 (1992); eingegangen am 5. September 1991 
  Published    1992 
  Keywords    Samarium Acetate, Acetic Acid Adduct, Synthesis, Crystal Structure 
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 Identifier    ZNB-1992-47b-0179 
 Volume    47 
31Author    Jürgen Hartung, Lothar Beyer, EnriqueG. Utiérrez-Puebla, VicenteF. Erná Ndez, Bernhard OlkRequires cookie*
 Title    Kristallstruktur von Acetonitril-trichlorocobaltat(II) Synthese und Struktur von 2,6-Dimorpholino-4-phenyI-l,3,5-oxadiazinium-Salzen Crystal Structure of Acetonitrile Trichlorocobaltates(II) Synthesis and Structure of 2,6-Dimorpholino-4-phenyl-l,3,5-oxadiazinium Salts 0 3 0 Leipzig  
 Abstract    A cetonitrile Trichlorocobaltate(II), 2,6-D im orpholino-4-phenyl-l,3,5-oxadiazinium Salts, Synthesis, Crystal Structure R eactions o f tris[(N-m orpholinothiocarbonyl)benzamidato]cobalt(III) and o f the free li­ gand in the presence o f C oCl, with SOCl2 in acetonitrile yield stable acetonitrile trichloro-cobaltate(II) salts with 2,6-dim orpholino-4-phenyl-l,3,5-oxadiazinium cations, suitable for X-ray structure determination. Space group P 2,/n, Z = 4, 4387 observed unique reflexions, R = 0.049, Lattice dimensions (22 °C): a = 772.94(9), b = 1611.5(4), c = 1911.1(5) pm; ß = 96.23(2)°. 
  Reference    Z. Naturforsch. 47b, 183—186 (1992); eingegangen am 24. Juni 1991 
  Published    1992 
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 Identifier    ZNB-1992-47b-0183 
 Volume    47 
32Author    M. Maneva, D. RizovaRequires cookie*
 Title    Löslichkeit und Dehydratisierungsprozesse bei M e S 0 4  
 Abstract    /iH20 (Me = Fe, Co, Ni, Zn, Mg; n = 7,6,4,1) in Methanol und Ethanol Solubility and Dehydration o f M eS 0 4 «H 20 (Me = Fe, Co, Ni, Zn, Mg; n = 7, 6,4 , 1) in Methyl and Ethyl Alcohols Dehydration o f M eS 0 4 • « H 20 A study has been made o f the solubility o f M e S 0 4 « H 20 (Me = Fe, Co, N i, Zn, Mg; 
  Reference    Z. Naturforsch. 47b, 187—1 (1992); eingegangen am 13. Mai/24. Juli 1991 
  Published    1992 
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 Identifier    ZNB-1992-47b-0187 
 Volume    47 
33Author    Wolfgang Jeitschko, Reinhold BrinkRequires cookie*
 Title    Preparation, Crystal Structures and Properties of Two Modifications of UCr6P4  
 Abstract    U Cr6P4 was prepared from a tin flux in two forms at low (a) and high (ß) temperatures (880 °C and 1000 °C), respectively. The crystal structures o f both m odifications were deter­ 
  Reference    Z. Naturforsch. 47b, 192—196 (1992); received September 5 1991 
  Published    1992 
  Keywords    Tin Flux, Crystal Structure, Magnetic Properties, Structural Relationships 
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 Identifier    ZNB-1992-47b-0192 
 Volume    47 
34Author    K. Urt, O. KleppRequires cookie*
 Title    Darstellung und Kristallstruktur von K2Sn2S 5 und K2Sn2Se5 Preparation and Crystal Structure of K2Sn2S5 and K 2Sn2Se5  
 Abstract    Thiostannate(IV), Selenostannate(IV), Crystal Structure K 2S n2S5 and K 2S n2Se5 were prepared by reacting stoichiometric powdered mixtures o f the binary com pounds K2S or K2Se with Sn and the corresponding chalcogen at 1070 K, followed by slow cooling o f the melt. The two com pounds are isostructural and crystallize with the TLSn-,S5 structure type, s.g. C2/c, Z = 4 with a = 11.072(5) Ä, b = 7.806(3)Ä , c = 11.517(5)Ä, ß = 108.43(2)° for K 2S n2S5 and a = 11.613(5)Ä, b = 8.189(3) A, c = 11,897(6) A, £ = 108.28(2)° for K 2 Sn2Se5. The crystal structures were refined to conventional R-factors o f 0.032 and 0.031, respectively. Sn-atoms are in a distorted trigonal-bipyramidal chalcogen coordination. The av­ erage equatorial bond lengths are S n -S : 2.427 A and S n -S e: 2.552Ä , the axial ones are S n -S ; 2.600Ä and S n -S e: 2.774Ä. 
  Reference    Z. Naturforsch. 47b, 197—200 (1992); eingegangen am 5. August 1991 
  Published    1992 
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 Identifier    ZNB-1992-47b-0197 
 Volume    47 
35Author    K. Urt, O. KleppRequires cookie*
 Title    K2TiS3, ein neues Thiotitanat(IV) mit fünffach koordiniertem Titan K 2TiS3, A New Thiotitanate(IV) with Pentacoordinate Titanium  
 Abstract    Fibrous red crystals o f the new compound K 0T iS3 were obtained by reacting K 1 S, Ti and S at 1070 K. K 2T iS3 is m onoclinic, space group C2/c with a = 11.667(6) Ä, b = 8.325(4) Ä, c = 6.494(4) Ä , ß = 9 i . 81(4)°, Z = 4. The crystal structure was refined to a conventional residual o f 0.070. The atom ic arrangement is characterized by /wei^/o-one-dimensional ^-[TiS3]2' chains formed by distorted TiS5 square pyramids sharing opposite edges o f their basal planes. The structure -though closely related to that o f Cs2TiS3 -is o f a new type. 
  Reference    Z. Naturforsch. 47b, 201—2 (1992); eingegangen am 26. August 1991 
  Published    1992 
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 Identifier    ZNB-1992-47b-0201 
 Volume    47 
36Author    Volker Müller, Gerlinde Frenzen, K. Urt Dehnicke, Dieter FenskeRequires cookie*
 Title    Synthese, FIR-Spektren und Kristallstrukturen der Pentaselenide K2Se5 und [Na(15-Krone-5)l2Se5 Syntheses, F IR Spectra, and Crystal Structures of the Pentaselenides K 2Se5 and [Na( 15-crown-5)]2Se5  
 Abstract    K2Se5 has been prepared by crystallization from a potassium polyselenide solution in D M F. In a similar way [Na(15-crown-5)]2Se5 can be prepared by crystallization from a sodium p oly­ selenide solution in D M F in the presence o f 15-crown-5. Both com pounds were characterized by FIR spectroscopy as well as by X-ray structure determinations. K2Se5: Space group P 2,2,2,, Z -4, 1659 observed independent reflections, R = 0.061. Lat­ tice dim ensions at -9 0 °C; a = 671.5(5), b = 694.9(5), c = 1776.4(9) pm. The com pound crys­ tallizes with the K2S5 type structure. [Na(15-crown-5)]2Se5: Space group P 1, Z = 2, 3026 observed indenpendent reflections, R = 0.140. Lattice dim ensions at -1 0 0 °C: a = 853.7(5), b = 1042.8(10), c = 2011.0(10) pm; a = 88.95(5)°, ß = 79.42(5)°, y = 66.15(5)°. The compound forms an ion triple, in which the sodium ions are coordinated by the five oxygen atoms o f the crown ether molecules as well as by the terminal selenium atom s o f the pentaselenide chain. The rather high R value is a result o f the disordered crown ether molecules. 
  Reference    Z. Naturforsch. 47b, 205 (1992); eingegangen am 23. August 1991 
  Published    1992 
  Keywords    Pentaselenides, Syntheses, FIR Spectra, Crystal Structure 
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 Identifier    ZNB-1992-47b-0205 
 Volume    47 
37Author    Peer Berges, Volker Mansei, G. Ünter KlarRequires cookie*
 Title    Elementorganische Verbindungen mit ö-Phenylenresten, XXIII [1]  
 Abstract    2.3.6.9.10.13-Hexam ethoxy-5,7,12,14-tetrathia-5,7,12,14-tetrahydropentacen -2.3-Dichlor-5,6-dicyan-l,4-benzochinon (1/2) Organometalloidal Com pounds with o-Phenylene Substituents, XXIII [1] 2.3.6.9.10.13-Hexamethoxy-5,7,12,14-tetrathia-5,7,12,14-tetrahydropentacene -2.3-Dichloro-5,6-dicyano-1,4-benzoquinone (1 /2) The title com pound is prepared by com bining hot solutions o f the components. X-ray anal­ ysis shows hexam ethoxytetrathiatetrahydropentacene to act as a bifunctional donor, each o f its dimethoxybis(organylthio)benzene units being in contact with a dichlorodicyanoquinone molecule. In the crystal stacks o f the type D A 2 ,D A 2, with an alternating arrangement o f d o­ nor and acceptor molecules are formed. In the com plex the donor has a m -conform ation (boat form) in contrast to its pure form where the /ra/w-conformation (chair form) is found. 
  Reference    Z. Naturforsch. 47b, 211 (1992); eingegangen am 26. August 1991 
  Published    1992 
  Keywords    Hexamethoxytetrathiatetrahydropentacene, Bifunctional D onor, D ichlorodicyanoquinone, Crystal Structure, X-Ray 
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 Identifier    ZNB-1992-47b-0211 
 Volume    47 
38Author    N. Orbert Auner, Erika PenzenstadlerRequires cookie*
 Title    Silaheterocyclen, XIII Erzeugung und Cycloadditionsverhalten von l,3-Diaza-2,4-disila-unj 1.3-Disilacyclobutanen mit exocyclischer SiC-Doppelbindung Silaheterocycles, XIII Form ation and Cycloaddition Reactions of l,3-Diaza-2,4-disila-and 1.3-Disilacyclobutanes Containing an Exocyclic SiC Double Bond  
  Reference    Z. Naturforsch. 47b, 217 (1992); eingegangen am 16. Juli/19. August 1991 
  Published    1992 
  Keywords    Silaheterocycles, Synthesis o f l, 3-Diaza-2, 4-disilacyclobutane, Form ation o f Silenes, Cycloaddition Reactions 
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 Identifier    ZNB-1992-47b-0217 
 Volume    47 
39Author    Z. NaturforschRequires cookie*
 Title    Übergangsmetall-substituierte Diphosphene, XXIV [ 1 ]  
 Abstract    Cheletrope [1 +4]-Cycloaddition von Azodicarbonsäureestern und -amiden an das metallsubstituierte Diphosphen (i75-C5M e5)(CO)2F e -P = P -Mes* (Mes* = 2,4,6-*Bu3C6H 2). Struktur von (i/5-C5M e5)(CO)2F e -P (= P -M e s *)|N (C 0 2E t)N = C (0 E t)Ö | Transition M etal Substituted Diphosphenes, XXIV [1] Cheletropic [1+4] Cycloaddition of Azodicarboxylic Esters and Amides to the Metal Substituted Diphosphene (^5-C5Me5)(CO)2F e -P = P -M e s * (Mes* = 2,4,6/Bu3C6H 2). Structure o f (^5-C5M e5)(CO)2F e -P(= P -M es*)[N (C 0 2Et)N = C (0 E t)0 ]. L othar Weber*, Holger Bastian, Achim Müller [2] und H artm ut Bögge [2] The diphosphenyl complex (>75-C 5M e5XCO)2F e -P = P -M e s * (1) (M es* = 2,4,6rBu3C6H2) 
  Reference    Z. Naturforsch. 47b, 231—2 (1992); eingegangen am 9. Juli/26. September 1991 
  Published    1992 
  Keywords    Diphosphene, Cycloaddition, Azodicarboxylates, X-Ray 
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 Identifier    ZNB-1992-47b-0231 
 Volume    47 
40Author    Kerstin Müller3, AntonM. Heynsb, Klaus-Jürgen Range3, M. Anfred ZabelaRequires cookie*
 Title    The Polymorphism of Alkali Metal Formates, Part 3 A Raman Spectroscopic, X-Ray and Thermoanalytical Study of the Polymorphism of Lithium Formate  
 Abstract    The crystal structure o f anhydrous lithium formate, published recently by Kansikas and Hermansson, is in fact that o f a quenchable high-temperature m odification (L iH C O O -I). The low-temperature modification L iH C O O -II can be obtained by thermal dehydration o f the monohydrate, LiHCOO-H20 , or by drying it over P4O 10. L iH C O O -II persists up to 228 C, at which temperature it transforms to L iH C O O -I, which in turn is stable up to its melting point at 272 °C. L iH C O O -I is also the m odification which crystallizes when a melt o f lithium formate is cooled down, in spite o f the fact that solidification occurs only at 165 "C, i.e. at a temperature well within the stability region o f L iH C O O -II. The Raman spectra o f the differ­ ent forms o f lithium formate are discussed in some detail. 
  Reference    Z. Naturforsch. 47b, 238 (1992); received June 10 1991 
  Published    1992 
  Keywords    Lithium Formate, Polymorphism, Raman Spectra, Crystal Structure 
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 Identifier    ZNB-1992-47b-0238 
 Volume    47 
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