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1999 (254)
81Author    Requires cookie*
 Title    Reaktionen von Isochinolinium-Salzen mit Hydroxylamin-Derivaten, 2. Mitteilung N-(Alkyl)-und N-(Aryl)-substituierte Verbindungen  
  Reference    Z. Naturforsch. 54b, 532 (1999) 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0532.pdf 
 Identifier    ZNB-1999-54b-0532 
 Volume    54 
82Author    C. N.Requires cookie*
 Title      
 Abstract    Consequently a systematic study of this reaction to establish the generality of the m ethod has been undertaken with various aldehydes and active methylene compounds utilizing m ontmorillonite K-10 under microwave irradiation in solventless system. Aliphatic aldehydes did not give any good results but aromatic aldehydes bearing a variety of functional group namely p-bromobenzaldehyde and p-nitrobenzaldehyde are reacted with 
  Reference    Z. Naturforsch. 54b, 541 (1999) 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0541.pdf 
 Identifier    ZNB-1999-54b-0541 
 Volume    54 
83Author    PirM. Uhammad, Saeed Ahmad, Hafiz Rubnawaz, Nisar Ullah, Abdul MalikRequires cookie*
 Title    New Monoterpene Glycosides from Paeonia emodi  
 Abstract    Wurdin, B enzoylw urdin, M on oterp en e G lycosides. Paeonia em odi, P aeon iaceae Two n ew m on oterp en e glycosides, wurdin and benzoylw urdin along with know n c o m ­ pounds, paeoniflorin. lactiflorin and oxyp aeon iflorin have been isolated from Paeonia em odi. The identity o f new com p ou n d s have b een established by a com bination o f sp ectroscop ic tech niques and chem ical transform ations. 
  Reference    Z. Naturforsch. 54b, 544 (1999); received O ctob er 20 1998 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0544.pdf 
 Identifier    ZNB-1999-54b-0544 
 Volume    54 
84Author    G. Unther Seitz, Jens LachmannRequires cookie*
 Title    Synthese neuer Pyridin-, Pyrindin-bzw. Isochinolin-substituierter a-und /?-C-Nukleoside der 2-Desoxy-D-ribose Synthesis of Novel Pyridine-, Pyrindine-and Isoquinoline-Substituted a-and ß-C-Nucleosides of 2-Deoxy-D-ribose  
 Abstract    Institut für P harm azeutische C h em ie der P hilipp s-U niversität M arburg, M arbacher W eg 6, D -35032 M arburg/Lahn Z. Naturforsch. 54b, 5 4 9 -5 5 8 (1999); ein gegan gen am 29. Januar 1999 a,/3-C -N ucleosides, In verse Type C ycloadditions, 1,2,4-T riazine-C -nucleosides, 2-D eo xy-D -rib ose, 2'-D eoxy-/3-D -ribofuranosyl-p yrid in e The n ovel im ido esters o f 2-d eo x y -a -and -/3-D -ribose 8 and 9 have been synthesized and successfully transform ed to the p rotected 1,2,4-triazin e-C -nucleosid es 11 and 12 using an inverse type D iels-A ld er reaction with the 1,2,4,5-tetrazine 10. The electron deficien t diaza-diene system o f both C -n u cleosid es 11 and 12 proved to be highly reactive in a consecutive [4 + 2] cycloaddition w ith inverse electron dem and tow ards several electron rich d ienop hiles yielding after successful d ep rotection the n ovel pyridine-, pyrindine-and isoqu inolin e-C -nu cleosid es 15, 18 and 21 o f 2 -d e o x y -a -D -r ib o se and 23, 25 and 27 o f 2-deoxy-/3-D -ribose. 
  Reference    Z. Naturforsch. 54b, 549 (1999) 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0549.pdf 
 Identifier    ZNB-1999-54b-0549 
 Volume    54 
85Author    Michael Schmittela, A. Ndrea Ganz3, WolfdieterA. Schenkb, Michael HagelbRequires cookie*
 Title    Synthesis and Coordination Properties of 6,6'-Dimesityl-2,2'-bipyridine  
 Abstract    a Institut für O rganische C h em ie der U niversität Würzburg, b Institut für A n organ isch e C h em ie der U niversität Würzburg, A m H ubland, D -97074 W ürzburg, G erm any 
  Reference    Z. Naturforsch. 54b, 559 (1999) 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0559.pdf 
 Identifier    ZNB-1999-54b-0559 
 Volume    54 
86Author    M. Ohindra, Seepersaud, Richard Bucala, Yousef Al-AbedRequires cookie*
 Title    A Polyhydroxylated Cyclopentene: A Useful Synthon toward the Synthesis of Carbocyclic D-Fructofuranoid  
 Abstract    The P icow er Institute for M edical R esearch, 350 C om m u nity D rive, D -A rab in o-and D -F ructofuranoid, P olyh ydroxylated C yclop en ten e. G ru bb's and Schrock's Catalyst A p olyh ydroxylated cyclop en ten e has b een syn th esized in five steps with an overall yield o f 61% , starting from 2,3,5-tri-O -benzyl-D -arab in ofuranose. 
  Reference    Z. Naturforsch. 54b, 565 (1999); received M arch 3 1999 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0565.pdf 
 Identifier    ZNB-1999-54b-0565 
 Volume    54 
87Author    Abdul-Khaliq Dardass3, Sadiqa Firdous, Zulfiqar Alib, Viqar Uddin, A. HmRequires cookie*
 Title    Alquds, a New Flavone Glycoside from Calamintha incana  
 Abstract    a D epartm ent o f Chem istry, U n iversity o f Karachi, K arachi-75270, Pakistan b International C enter for C hem ical Scien ces, H. E. J. R esearch Institute o f Chemistry, U niversity o f Karachi, K arachi- A lquds, C alam intha incana, L am iaceae A lquds, a new flavone glycosid e was isolated from the aerial parts o f C alam intha incana and identified on the basis o f spectral data (1-and 2 -D N M R . IR, U V) and com parative study. 
  Reference    Z. Naturforsch. 54b, 569 (1999); received N o v em b er 16 1998 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0569.pdf 
 Identifier    ZNB-1999-54b-0569 
 Volume    54 
88Author    Hans Liesenhoff, Wolfgang SundermeyerRequires cookie*
 Title    Chemische Reaktionen in Salzschmelzen, XXI [1]. Titan-vermittelte Synthese von Silanen in Chloroaluminat-Schmelzen Chemical Reactions in Molten Salts, XXI [I]. Titanium Mediated Synthesis of Silanes in Chloroaluminate Melts  
 Abstract    Fused Salts, Monosilane, Methylsilanes, Hydrosilylation, Chloroaluminate Silanes of technical interest as starting compounds for semiconducting materials or hydrosi­ lylation reactions, (CH3)xSiH4_x (x = 0, 1,2, 3), are obtained by direct hydrogenation of the corresponding chlorosilanes in the presence of various interstitial hydrides of transition metals (preferably of titanium), which are generated in situ in chloroaluminate melts, and aluminum as a halogen acceptor. 
  Reference    Z. Naturforsch. 54b, 573—576 (1999); eingegangen am 28. Dezember 1998 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0573.pdf 
 Identifier    ZNB-1999-54b-0573 
 Volume    54 
89Author    Heike Quellhorst, Andreas Wilkening, Nicola Söger, Michael BinnewiesRequires cookie*
 Title    Hydrolytische Bildung von Perchlorsiloxanen Formation of Chlorosiloxanes by Hydrolysis  
 Abstract    Chlorosiloxanes, Hydrolytic Formation, Chlorosilanoles During the reaction of Si2OCl6 with H20 in the gas phase the intermediate Si2OCl5OH has been observed by mass-spectrometry. Reactive intermediates like this are responsible for the formation of higher chlorosilanes by slow hydrolysis reactions of chlorosilanes and -siloxanes. Reaction products of inter-and intramolecular condensation reactions have been observed by GC-MS-methods. 
  Reference    Z. Naturforsch. 54b, 577—582 (1999); eingegangen am 18. Februar 1999 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0577.pdf 
 Identifier    ZNB-1999-54b-0577 
 Volume    54 
90Author    Carola Stoll3, Ingo-Peter Lorenza, Kurt Polbom, ErichFriedrich Paulus0Requires cookie*
 Title    Umsetzung von Cyclopentadienylmetallcarbonylen mit Thionylhalogeniden -Neue Synthese halogenoverbrückter Cp*Co-Komplexe Reaction o f Cyclopentadienyl Metal Carbonyles with Thionylhalides -New Synthesis o f Halogeno-Bridged Cp*Co Complexes  
 Abstract    The reaction of Cp*Co(CO)2 with thionylchloride in hexane affords the doubly bridged dimer (Cp*CoCl2)2. Whereas the same reaction in more polar solvents such as CH2C12 or thf gives the triply bridged dinuclear cations in the salt [(Cp*Co)2(^-C l)3]2 [Co2Cl6], no influence of the solvent is observed in the reaction of Cp*Co(CO)2 with thionylbromide, which results in the formation of the neutral dimer (Cp*CoBr2)2. The X-ray structure analysis of (Cp*CoBr2)2 shows two edge-sharing octahedra, while that of [(Cp*Co)2(^-C l)3]2[Co2Cl6] shows two face-sharing octahedra in the cation and two edge-sharing tetrahedra in the anion. 
  Reference    Z. Naturforsch. 54b, 583—590 (1999); eingegangen am 23. Dezember 1998 
  Published    1999 
  Keywords    Thionylhalides, Halogeno Bridges, Pentamethylcylopentadienylcobalt Complexes, Chlorination, X-Ray Data 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0583.pdf 
 Identifier    ZNB-1999-54b-0583 
 Volume    54 
91Author    Andrea Noll, Susanne Rabe, Ulrich MüllerRequires cookie*
 Title    Die Oxochlorovanadate PPh4[VOCl3OH], PPh4[VOCl4], (PPh4 )2 [VOCl4 ]*2 CH3CN und (P P l^ tV O C ^ M C I^ C N mit auffälligen Abweichungen von der quadratisch-pyramidalen Anionenstruktur The Oxochlorovanadates PPh4 [VOCl3OH], PPh4 [VOCl4], (PPh4 )2 [VOCl4]-2CH3 CN, and (PPh4)2[VOCl4]-4CH3CN with Remarkable Deviations from the Square-Pyramidal Anion Structure  
 Abstract    Trichloro-hydroxo-oxo-vanadate(V), Tetrachloro-oxo-vanadate(IV), Tetrachloro-oxo-vanadate(V), Crystal Structure Starting from vanadium which was not free of oxide, VC14 was prepared; its reaction with PPh4Cl in the presence of K2S5 in dichloromethane yielded PPh4[VOCl3OH]. From V 2S5, PPh4Cl and S2C12 in acetonitrile, sulfur crystallized first, then PPh4[VOCl4], and then (PPh4)2[VOCl4]-4CH3CN. Upon standing with the mother liquor at -18°C , the latter was con­ verted to (PPh4)2[VOCl4]-2CH3CN. According to its X-ray crystal structure determination, PPh4[VOCl3OH] (space group Pbca, a = 1105.5, b = 1920.8, c = 2242.8 pm, Z -8) has near­ ly square-pyramidal anions that are associated to chains by 0-H --C1 bridges. PPh4[VOCl4] is isotypic with AsPh4[VOCl4] and has strictly square-pyramidal anions (space group P4/n, a = 1254.0, c = 765.0 pm, Z = 2). In (PPh4)2[VOCl4]-4CH3CN (space group P T, a = 1281.3, b = 1276.6, c = 1841.5 pm, a = 84.11°, ß = 83.96, 7 = 64.31°, Z = 2) the square pyramid of the VOCl42-ion is distorted towards a trigonal-bipyramidal shape (C2v symmetry) ha­ ving trans-C 1VC1 angles of 145.88° and 156.87° and 0=V-C1 angles of 107° and 101.6°. In (PPh4)2[VOCl4]-2CH3CN (space group P \ a = 1017.1, b = 1029.3, c = 2416.0, a = 77.74°, ß = 79.99°, 7 = 78.94°, Z = 2), the VOCl4_~ structure is even closer to trigonal-bipyramidal, with trans-C1VC1 angles of 133.25° and 165.80° and 0=V-C1 angles of 113.3° and 97°. 
  Reference    Z. Naturforsch. 54b, 591—596 (1999); eingegangen am 23. November 1998 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0591.pdf 
 Identifier    ZNB-1999-54b-0591 
 Volume    54 
92Author    Lars Ihloa, Reinhard Stößerb, W. Ulf Hofbauer0, R. Olf Böttcherd, Reinhard Kirmse3Requires cookie*
 Title    S-, X-, Q-und W-Band-Pulver-EPR-Untersuchungen an Tetra-« -butylammonium-bis( 1,2-dicyanoethen-1,2-dithiolato)aurat(II), [(n-C4H9)4N]2[Aun(mnt)2] S, X, Q and W Band Powder-EPR Investigations on Tetra-«-butylammonium- bis(l,2-dicyanoethylene-l,2-dithiolato)aurate(II), [(«-C4 H9)4N ]2[Aun(mnt)2]  
 Abstract    Powder-EPR studies at T = 295 K and T = 12 K on the unstable gold(II) complex [(n-C4H9)4N ]2[AuII(mnt)2] diamagnetically diluted by the corresponding Ni" complex are reported. Due to (i) the small anisotropy of the g and the I J7Au hyperfine tensor AAu, and (ii) the large 197 Au quadrupole interaction the powder spectra possess a very complex pattern. Using different EPR frequencies -S band (2.4 GHz), X band (9.5 GHz), Q band (35 GHz) and W band (94 GHz) -the spectra could be analyzed successfully. All spectra were simulated with a computer program which diagonalizes the spin-Hamiltonian matrix exactly. 
  Reference    Z. Naturforsch. 54b, 597—602 (1999); eingegangen am 2. März 1999 
  Published    1999 
  Keywords    Gold(II) Complexes, Dithiolenes, Powder-EPR 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0597.pdf 
 Identifier    ZNB-1999-54b-0597 
 Volume    54 
93Author    Heinrich Nöth, Ralf WaldhörRequires cookie*
 Title    Unerwartete Reaktionsprodukte bei der Umsetzung von Mesitylmagnesiumbromid mit Arsentribromid Unexpected Products from the Reaction o f Mesitylmagnesium Bromide and Arsenic Tribromide  
 Abstract    Dimesitylarsenic Bromide, Enneabromotriarsenate(III), Magnesium-tetrakis(acetonitrile)-bis(tetrahydrofuran) Cation, X-Ray Data Irrespective of the ratio of the reactands AsBr3 and mesMgBr (mes = mesityl), two pro­ ducts are formed in THF solution: dimesitylarsenic bromide and a magnesium bromoarsenate of composition M gAs5B r|7 • n THF. The latter, on crystallization from acetonitrile, yields [Mg(NCMe)4(THF)2][As3B rn ]. The anion of this salt can be described as derived from three face sharing AsBr6 octahedra. The lone pair of electrons at the As atoms is stereochemically not active. 
  Reference    Z. Naturforsch. 54b, 603—608 (1999); eingegangen am 9. Dezember 1998 
  Published    1999 
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 Identifier    ZNB-1999-54b-0603 
 Volume    54 
94Author    Robert Tripolt, Siegfried Schmuck, Edgar NachbaurRequires cookie*
 Title    .3.5-Triazin-2,4,6-trisulfenyltrichlorid: Synthese, Eigenschaften und Reaktionsverhalten 1.3.5-Triazine-2,4,6-trisulfenyltrichloride: Synthesis, Properties and Reactions  
 Abstract    Various routes and improved experimental conditions for the synthesis o f 1,3,5-triazine-2,4,6-trisulfenyltrichloride are reported and its reaction with water, alcohols, ammonia, and acetone investigated. The formation o f the monomeric pseudohalogen halide NCS-C1 by degradation o f the title compound under mass-spectrometry conditions has been observed. 
  Reference    Z. Naturforsch. 54b, 609 (1999); eingegangen am 29. Dezember 1998 
  Published    1999 
  Keywords    Sulfenyl Chloride, Sulfenic Acid, Sulfenate Ester, Sulfenamide 
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 Identifier    ZNB-1999-54b-0609 
 Volume    54 
95Author    H. Oppermann, A. MorgensternRequires cookie*
 Title    Verdampfungsverhalten von Lanthantrihalogeniden Evaporation Behaviour o f Lanthanum Trihalides  
 Abstract    The evaporation of LaCl3, LaBr3 and Lal3 was investigated in closed tubes under argon atmosphere and correlated with data in the literature. The enthalpies and entropies of evaporation were derived from the temperature functions of pressure: -AH°(v, LaCl3, T) = 48,5 ± 2 kcal/mol, Z\S°(v, LaCl3, T) = 22,0 ± 3 cal/K-mol _AH°(v, LaBr3, T) = 48,0 ± 2 kcal/mol, Z\S°(v, LaBr3, T) = 24,0 ± 2 cal/K-mol J H ° (v , L al3, T) = 49,5 ± 2 kcal/mol, Z\S°(v, L al3, T) = 29,0 ± 2 cal/K-mol 
  Reference    Z. Naturforsch. 54b, 617—623 (1999); eingegangen am 11. Februar 1999 
  Published    1999 
  Keywords    Lanthanum Trihalides, Evaporation, Enthalpy, Entropy 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0617.pdf 
 Identifier    ZNB-1999-54b-0617 
 Volume    54 
96Author    Lutz Ruwischa, Ralf Riedel3, Uwe Klingebielb, Mathias NoltemRequires cookie*
 Title    Synthese und Molekülstruktur des [a-(Dichlormethylsilyl)ethyl]- dichlorboran-dimethylsulfid Synthesis and Molecular Structure o f [a-(Dichlorom ethylsilyl)ethyl]- dichloroborane-dimethylsulfide  
 Abstract    Silicon, Silylethyl-boranedimethylsulfide, Crystal Structure [o-(Dichloromethylsilyl)ethyl]-dichloroborane-dimethylsulfide has been synthesized by the reaction of dichloromethylvinylsilane with dichloroborane-dimethylsulfide and its molecular structure determined by single crystal X-ray diffraction and by spectroscopic methods. Follo­ wing the Markovnikov rule, a chiral methine group is formed as a bridge between silicon and boron. 
  Reference    Z. Naturforsch. 54b, 624—626 (1999); eingegangen am 23. November 1998 
  Published    1999 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0624.pdf 
 Identifier    ZNB-1999-54b-0624 
 Volume    54 
97Author    MikeR. Kopp, Thomas Kräuter, Anahita Dashti-Mommertz, Bernhard NeumüllerRequires cookie*
 Title    Organogallitimamide: Synthese und Kristallstrukturen von [IPr2GaN(H/Bu]2 und [Mes(Cl)GaN(H)'Bu]2 Organogallium Amides: Synthesis and Crystal Structures o f ['Pr-,GaN(H)'Bu]-, and [Mes(Cl)GaN(H)'Bu]2  
 Abstract    ['Pr2GaN(H)'Bu]2 (1) and [Mes(Cl)GaN(H)'Bu]2 (2) can be synthesized by the metathesis reaction of 'Pr2GaCl and MesGaCl2 with one equivalent of LiN(H)'Bu, respectively. 1 and 2 were characterized by NMR, IR and MS techniques as well as by X-ray structure analyses. 1 and 2 consist of centrosymmetric dimeric molecules with a G a2N2 skeleton. According to cryoscopic measurements in benzene, both amides 
  Reference    Z. Naturforsch. 54b, 627—631 (1999); eingegangen am 8. Januar 1999 
  Published    1999 
  Keywords    Gallium Compounds, Organogallium Amides, Crystal Structure 
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 Identifier    ZNB-1999-54b-0627 
 Volume    54 
98Author    Hans Möhrle, Georg KellerRequires cookie*
 Title    a-Dicarbonylmonoxime als Nucleophile und Nachbargruppen a-Dicarbonylm onoxim es as Nucleophiles and Neighbour Groups  
 Abstract    The Q-dicarbonylmonooximes 1 and 11 do not react as simple "CH-acidic-compounds" in the Mannich condensation. In a concerted reaction with aminals in absolute dioxane they give rise to the products 4a -e and 12a -e with better practicability and much higher yields compared with the conventional method. The Mannich bases with a cyclic amine part show in the dehydrogenation, using mercury-EDTA, a neighbouring group participation of the oxime in type 4 and of the oxime or amide function in 12 yielding cyclized products. For the reaction a plausible mechanism is proposed. 
  Reference    Z. Naturforsch. 54b, 632—642 (1999); eingegangen am 27. Januar 1999 
  Published    1999 
  Keywords    Aminal, C-Aminomethylation, Mercury(II)-EDTA Dehydrogenation, Intramolecular Cyclization 
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 Identifier    ZNB-1999-54b-0632 
 Volume    54 
99Author    Karna Wijaya, Oliver Moers, Blaschette Arm, PeterG. JonesRequires cookie*
 Title    Polysulfonylamine, CXII [1] Neues aus der Festkörperchemie der 2-Pyridone: Isolierung und Röntgenstrukturen von Bis(2-pyridon)hydrogen(I)-und Bis(6-methyl-2-pyridon)hydrogen(I)-dimesylamid Polysulfonylamines, CXII [1] A Novel Solid-State Aspect of 2-Pyridones: Isolation and X-Ray Structures of Bis(2-pyridone)hydrogen(I) and Bis(6-methyl-2-pyridone)hydrogen(I) Dimesylamides  
 Abstract    The compounds (2-pyridone)2H +(M e S 0 2)2N~ (1, monoclinic, space group V ljn) and ( 
  Reference    Z. Naturforsch. 54b, 643 (1999); eingegangen am 11. Januar 1999 
  Published    1999 
  Keywords    2-Pyridones, 2-Hydroxypyridines, Dimesylamide, Hom oconjugate Cations, Crystal Structure 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0643.pdf 
 Identifier    ZNB-1999-54b-0643 
 Volume    54 
100Author    Friedhelm Balkenhohl, Joachim PaustRequires cookie*
 Title    A Short and Productive Synthesis of Racemic a-Lipoic Acid  
  Reference    Z. Naturforsch. 54b, 649 (1999); received Decem ber 4 1999 
  Published    1999 
  Keywords    Lipoic A cid, Radical Induced C-C-Bond Formation, Baeyer-Villiger Oxidation, Ether Cleavage, Isothiuronium Salts 
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 TEI-XML for    default:Reihe_B/54/ZNB-1999-54b-0649.pdf 
 Identifier    ZNB-1999-54b-0649 
 Volume    54 
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