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1994 (283)
201Author    Requires cookie*
 Title    Darstellung, n B-, 13C-NMR-und Schwingungsspektren von Aminom ethylhexahydro-closo-hexaborat(l-), [B6H6(CH2N H 2)]~ sowie Kristallstrukturen von Cs[B6H6(CH2NH2)] und K[B6H6(CH2N H 2)]  
  Reference    Z. Naturforsch. 49b, 1267 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1267 
 Volume    49 
202Author    Bernward EngelenRequires cookie*
 Title    Kristallstruktur von M n S 03 * H20 , eine fastsymmetrische Schichtstruktur Crystal Structure of M n S 0 3 H20 , A Nearly Symmetrical Layer Structure  
 Abstract    M ärz 1994 X-Ray, Sulfites. H ydrates, M anganese, Pseudosym m etry The crystal structure of M n S 0 3 H 20 , space group P 2 xln, Z = 4. D t = 2.842(2) g e m '3, a = 4.843(3), b = 12.807(6), c = 5.762(4) Ä, ß = 90.39(4)° has b een determ in ed . M n S 0 3-H 20 crystallizes in a h ith erto unknow n structure type, which is closely related to th a t of o rth o -rhom bic M n S e 0 3 D 20 . C o ordination of Mn is octahedral involving O atom s from one w ater m oleculeo and four different sulfite ions. The M n -O distances range from 2.136(3) to 2.285(3)A . The S -O distances are 1.552(3), 1.556(3) and 1.482(3)!Ä . The M n 0 6 o ctah e d ra form layers parallel (010) by sharing four equato rial vertices. T he layers are co nnected by w eak hydrogen bonds and shifted laterally by 0.7 A from the a rran g em en t w ith m sym m etry, found in M n S e 0 3-D 20 . D ue to this shift, the w ater m olecule is asym m etrically b onded, as shown by b oth the O -H -O distances (2 .9 6 7 (4)-3 .8 3 4 (5)Ä) and the O D stretching m odes (2554 and 2576 cm ') of partly d eu terated samples. 
  Reference    Z. Naturforsch. 49b, 1272—1276 (1994); eingegangen am 17 
  Published    1994 
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 Identifier    ZNB-1994-49b-1272 
 Volume    49 
203Author    Ch Rabbow, Hk Müller-BuschbaumRequires cookie*
 Title    Zur Kenntnis eines Barium-Lanthanoid-Oxomanganats(IY,V): Ba3ErMn20 9  
 Abstract    In stitu t für A norgan isch e C hem ie d er C h ristian-A lbrechts-U niversität, O lsh au sen straß e 40.. M ärz 1994 B arium , R are E arth , M anganese, Oxide, Crystal S tructure H igh te m p e ra tu re reactions of B a C 0 3/M n 0 /E r20 3 (3 :1 :1) led to single crystals of B a3E rM n 20 9. The pro d u ct shows the structure of the hexagonal precious m etal oxides B a3L n R u 20 9, b u t crystallizes with orthorhom bic sym metry, space group C j 2-C m c 2 !, a = 5.823 A , b -10.099 A, c = 14.409 Ä; Z = 4. The crystal stru ctu re is characterized by E r 0 6 octah ed ra, M n2Oy face shared double o ctah edra and B a2+ w ithin cu b o ctah ed ral and an ticu b o ctah ed ral co ordination by O 2 -, respectively. In con trast to p recious m etal oxides the M n -M n distances inside the M n20 9 double o ctah e d ra are elongated. 
  Reference    Z. Naturforsch. 49b, 1277—1281 (1994); eingegangen am 17 
  Published    1994 
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 Identifier    ZNB-1994-49b-1277 
 Volume    49 
204Author    M. Artina Andratschke, Klaus-Jürgen Range, Claudia Weigl, Ulrike Schießl, Franz RauRequires cookie*
 Title    Die Kristallstruktur von T lZ n P 04 und T IZ nA s04 The Crystal Structure of T lZ n P 0 4 and T lZ n A s0 4  
  Reference    Z. Naturforsch. 49b, 1282 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1282 
 Volume    49 
205Author    U. Himmelreich, S. Huneck, G. B. Feige, H. T. LumbschRequires cookie*
 Title    Squamaron, ein Naphthochinon aus der Flechte Squamarina cartilaginea Squamarone, a Naphthoquinone from the Lichen Squamarina cartilaginea  
 Abstract    Squam arone, 2,6,8-T rihydroxy-3-m ethyl-7-ethyl-l,4-naphthoquinone, Squam arina cartilaginea, Lichen The structure of the orange pigm ent from the elucidated by N M R spectroscopical m eth o d s as 2. thoquinone. 
  Reference    Z. Naturforsch. 49b, 1289—1291 (1994); eingegangen am 6. A pril 1994 
  Published    1994 
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 Identifier    ZNB-1994-49b-1289 
 Volume    49 
206Author    Uwe Himmelreich, Siegfried HuneckRequires cookie*
 Title    Haemophaein, ein Dibenzofuran aus der Flechte Phyllopsora haemophaea Haem ophaein, a Dibenzofuran from the Lichen Phyllopsora haemophaea  
 Abstract    6. A pril 1994 Lichens, P hyllopsora haem ophaea, H aem o p h aein , D ibenzofuran H aem oph aein , a m etab o lite of the lichen Phyllopsora haem ophaea has been structurally elucidated as l-(2',2'-dihydroxyheptyl)-3,6-dihydroxy-8-(2"-oxoheptyl)-dibenzofuran-2-carboxylic acid-9,2'-lactone. 
  Reference    Z. Naturforsch. 49b, 1292—1296 (1994); eingegangen am 
  Published    1994 
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 Identifier    ZNB-1994-49b-1292 
 Volume    49 
207Author    J.Ag G Falsone, F. Cateni, E. VrechRequires cookie*
 Title    Triacylglycerols, Fucosterol, Diacylglyceroglycolipids and Fucoxanthin from Fucus virsoides  
 Abstract    D ep artm en t of Pharm aceutical Sciences, U niversity of Trieste, P.zle E u ro p a 1,1-34127 Trieste L. Birkofer 
  Reference    Z. Naturforsch. 49b, 1297 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1297 
 Volume    49 
208Author    Requires cookie*
 Title    Asymmetrische  
 Abstract    Katalysen, 88 [1] Kinetik der Rh-katalysierten Hydrierung von (Z)-(«)-N-Acetylaminozimtsäure mit optisch aktiven Schalenphosphinen als Liganden Asymmetrie Catalysis, 88 [1] 
  Reference    Z. Naturforsch. 49b, 1305 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1305_n 
 Volume    49 
209Author    Rainer PöttgenRequires cookie*
 Title    Er2Au2Sn and other Ternary Rare Earth Metal Gold Stannides with Ordered Zr3A l2-Type Structure  
 Abstract    received M ay 20, 1994 R are E arth G old Tin, Interm etallic C om pounds, O rd ered Z r3A l2-Structure The ternary stannides R E 2A u2Sn (R E = Y, Dy, H o, E r, Tm , Lu) w ere p rep ared by arc-m elting of the elem en tal com ponents and su b seq u en t annealing at 800 °C. The stru ctu re of E r2A u2Sn (single crystal. X-ray, P 4 2/m nm , Z = 4, a = 778.2(2) pm , c = 739.6(3) pm , V = 0.4479 nm 3 and R = 0.026) is described as the tern ary ord ered version of the Z r3A l2-type structure, a su p erstru ctu re o f th e U 3Si2-type. It consists of tw o-dim ensionally infinite layers (A u2Sn)" which are sep arated by the erbium atom s. The structure is built up from slightly distorted [SnE r8] square prism s and [A uE r6] trigonal prism s which are condensed in all three directions. T hese fragm ents are derived from th e well know n A1B2 and CsCl-type structures. 
  Reference    Z. Naturforsch. 49b, 1309—1313 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1309 
 Volume    49 
210Author    Markus Wieber, Ralph HabersackRequires cookie*
 Title    Bis(triorganotelluronium)hexasulfide Bis(triorganotelluronium)hexasulfides  
 Abstract    T riorganotelluronium C om pounds, Polychalcogenides, H exasulfides, C rystal S tructure The reaction o f triorganotelluronium chlorides R 3TeCl (R = Me, Ph, 4 -fB u -C 6H 4) with N a2S v (jc = 4 -6) yields the corresponding b is(trio rg an o tellu ron iu m) hexasulfides (R 3Te)2S6 regardless of the em ployed sodium polysulfide or the size of the telluronium cation. All com pounds are therm ally stable and insensitive to m oisture o r air. (P h 3Te)2S6 was structurally characterized by X -ray crystallography (m onoclinic, space group P 2j/c). E ach tellurium atom is connected to both ends of the hexasulfide chain. 
  Reference    Z. Naturforsch. 49b, 1314—1318 (1994); eingegangen am 24. M ai 1994 
  Published    1994 
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 Identifier    ZNB-1994-49b-1314 
 Volume    49 
211Author    Abdel-Fattah ShihadaRequires cookie*
 Title    Synthesis and Vibrational and Mass Spectra of Ph3S n 0 2PM e2, Ph3S n 0 2PMePh and Ph3S n 0 2PPh2  
 Abstract    D e p artm en t of Chem istry, Faculty of Science, U n ited A ra b E m irates U niversity, A l-A in, P.O. Box: 17551, U nited A rab E m irates Z. N aturforsch. 49b, 1319-1323 (1994); received M arch 16, 1994 IR Spectra, R am an Spectra, Mass Spectra, T riphenyltin D im eth y lp h o sp h in ate T he reactions of (P h 3Sn)20 with P hM eP O C l and w ith P h2P O C l lead to P h 3S n 0 2PM ePh and P h 3S n 0 2PPh2, respectively. Ph3S n 0 2P M e2 has b een p re p a red from the reactio n of (P h 3S n)20 and M e2P 0 2H in toluene. The IR and R am an spectra o f Ph3S n 0 2PM e2, P h 3S nÖ 2PM ePh and P h3S n 0 2P P h2 are found to be consistent w ith polym eric stru ctu res with p entacoordinated tin atom s. The E l mass spectra indicate th a t the principal fragm entation processes of Ph3S n 0 2P R R ' (R R ' = M e2, M ePh, P h2) a p p ear to occur by loss o f phenyl radicals from tin and by elim ination of th e en tire d io rg an o p h o sp h inate group. 
  Reference    Z. Naturforsch. 49b, 1319 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1319 
 Volume    49 
212Author    E. Ndre Kövári, Roland KrämerRequires cookie*
 Title    Metallkomplexe 6,6'-Dialkinyl-substituierter 2,2'-Bipyridin  
 Abstract    Liganden: Synthese und Struktur von [{6,6'-(CH3CH2CH2C = C)2bpy}Cu(Cl)(^-Cl)]2 Metal Complexes of 6 ,6 '-Dialkynyl-Substituted 2,2'-Bipyridine Ligands: Synthesis and Structure of [{6 ,6 '-(C H 3 CH2CH2C = C)2bpy}Cu(Cl)(a-Cl)] 2 The bipyridyldiacetylene 6,6'-(C H 3CH2CH2C = C)2bpy (1) was prepared by palladium catalyzed C -C -cou p lin g reaction of 6,6'-dibromo-2,2'-bipyridine with pentyne. Reaction of 1 with anhydrous CuCl2 in acetonitrile gave the dimeric, chloro-bridged complex (1)C u(C1)(m-C1)2Cu(C1)(1) (2), which was characterized by X-ray crystallography. The copper atoms in 2 are square-pyramidally coordinated with normal in-plane C u -N and C u -C l bond distances and one longer, apical bond to the second bipyridyl nitrogen atom. The influence of steric hindrance o f the bipyridyl 6,6'-substituents on the structure o f the complex is discussed. 
  Reference    Z. Naturforsch. 49b, 1324—1328 (1994); eingegangen am 9. Mai 1994 
  Published    1994 
  Keywords    Copper Bipyridine Complexes, Bipyridylacetylenes, X-Ray 
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 Identifier    ZNB-1994-49b-1324 
 Volume    49 
213Author    F.-D Martin, Hk Müller-BuschbaumRequires cookie*
 Title    Synthese und Kristallstruktur von NaM g1?64Cu0 ,36^3^10 Synthesis and Crystal Structure of NaM glt64Cuoi36V 3 0 1o  
 Abstract    Single crystals of NaMg] 64Cu().36V 3O 10 have been prepared by heating mixtures of Na2C 0 3, M gC 03, CuO and V 20 5 above the melting point. The yellow crystals show triclinic symmetry, space group Cj-PT, a = 6.726(8), b = 6.743(7), c = 9.625(2) Ä , a = 100.705(9), ß -104.57(1), y = 101.700(9)°, Z = 2. N aM g164Cu0.36V 3O 10 represents a new structure type showing V 3O 10 groups, a statistical distribution of Mg2+ and Cu2+ on two point positions, and N a+ in an irregular coordination. 
  Reference    Z. Naturforsch. 49b, 1329—1333 (1994); eingegangen am 6. Mai 1994 
  Published    1994 
  Keywords    Sodium Magnesium, Copper, Vanadium Oxide, Crystal Structure 
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 Identifier    ZNB-1994-49b-1329 
 Volume    49 
214Author    Hendrik Möller, Ellen Suchanek, HeinzDieter Lutz, Werner PaulusRequires cookie*
 Title    Neutronenbeugungs-Untersuchung von M g(I03)2*4H 20 -Einkristallen Neutron Diffraction Studies on M g (I0 3 )2 -4H 20 Single Crystals  
 Abstract    The crystal structure of M g (I 0 3)2-4 H 20 has been determined by neutron single crystal diffraction (P2j/c, Z = 2, R = 2,2% on the basis of 1107 observed reflections). M g (I 0 3)2-4 H 20 forms a layered structure built up of octahedral M g(H 20) 4(I 0 3)2 units linked by hydrogen bonds. The two crystallographically different water m olecules are in­ volved in asymmetric, nearly linear hydrogen bonds to adjacent iodate ions (vOD of matrix isolated HDO: 2480, 2475, 2425 und 2412 cm -1, IR spectroscopic data, 90 K). The strength of the hydrogen bonds as well as that of other iodate hydrates is discussed in terms o f both the synergetic effect and Brown's bond valences. 
  Reference    Z. Naturforsch. 49b, 1334—1338 (1994); eingegangen am 2. Mai 1994 
  Published    1994 
  Keywords    Magnesium Iodate Tetrahydrate, Crystal Structure, Neutron Diffraction Studies, Hydrogen Bonds 
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 Identifier    ZNB-1994-49b-1334 
 Volume    49 
215Author    Requires cookie*
 Title    Elektronentransfer und Ionenpaar-Bildung, 34 [ 1 -3 ] Einkristallstruktur des Solvens-separierten Radikalionenpaares [9,9'-Bianthryle ][N ae (DM E)3]  
  Reference    Z. Naturforsch. 49b, 1339 (1994) 
  Published    1994 
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 Identifier    ZNB-1994-49b-1339 
 Volume    49 
216Author    Christoph Riidinger, Holger Beruda, H. Ubert SchmidbaurRequires cookie*
 Title    Synthesis and Molecular Structure of Silylated Ethenes and Acetylenes  
 Abstract    Disilylacetylene (1) has been obtained from LiA lH 4 reduction of bis(trichlorosilyl)ace-tylene (2) and bis[(trifluoromethylsulfonyloxy)silyl]acetylene (4). The catalytic hydrosilyl-ation of 2 with HSiCl3 affords tris(trichlorosilyl)ethene (5) and l.l,2-tris(trichlorosilyl)ethane (6). The synthesis of 6, fra/«-bis(trichlorosilyl)ethene (8) and l,l-bis(trichlorosilyl)ethene (9) has been accomplished by hydrosilylation of trichlorosilylacetylene (7) which was synthesized by the reaction of trichloro(trifluoromethylsulfonyloxy)silane with sodium acetylide. R e­ 
  Reference    Z. Naturforsch. 49b, 1348—1360 (1994); received May 20 1994 
  Published    1994 
  Keywords    Silanes, Trichlorosilanes, Polysilylethenes, Carbon H alogenated Silylolefines 
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 Identifier    ZNB-1994-49b-1348 
 Volume    49 
217Author    M. Anfred Fild, PeterG. Jones, Karsten Ruhnau, Carsten ThöneRequires cookie*
 Title    Darstellung und Strukturen von 2,2,4,4-Tctrafluor-l,3-diphosphctancn und -1,3-diphosphetan-disulfiden Synthesis and Structures of 2,2,4,4-Tetrafluoro-l,3-diphosphetanes and of -1,3-diphosphetane Disulfides  
 Abstract    A simple route to 1,3-diphosphetanes [RPCF2]2 [R = Ph, Me, Bu'] is described. The phos-phaalkene intermediates RP=CF2, as well as the corresponding disulfides [R (S)PC F2]2 have been characterized. The crystal structures of [PhPCF2]2, and of the sulfides [Ph(S)PCF2]2 and [Bu'(S)PCF2]2 are reported. 
  Reference    Z. Naturforsch. 49b, 1361—1367 (1994); eingegangen am 6. Juni 1994 
  Published    1994 
  Keywords    Phosphaalkenes, 1, 3-Diphosphetanes, 1, 3-Diphosphetane Disulfides, NM R Spectra, Crystal Structure 
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 Identifier    ZNB-1994-49b-1361 
 Volume    49 
218Author    YueQing Zheng, Arnold AdamRequires cookie*
 Title    Ein neues Carbonat mit Baylissit-Struktur: Rb2[M g(C 03)2(H 20 )4] A New Carbonate with Baylissite Structure: Rb2 [Mg(C0 3 )2(H 2 0 )4]  
 Abstract    The new complex carbonate Rb2[M g (C 0 3)2(HoC))4] crystallizes in the Baylissite-tvpe structure with a = 1130,4(3), b = 641,9(1), c = 703,3(2) pm, ß = 99,62(1)°, V EZ = 503,2(2), space group P2l/n (No. 14) and Z = 2. In comparison with the isostructural potassium compound the cell dimensions increase in b-and c-and decrease in ö-direction. This effect depends on the greater coordination number of Rb+ and the rigidity of strong hydrogen bonds. The carbonate anion exhibits significant deviations from D 3h-symmetry (C -O : 127,1(5)-130,2(5) pm, Z_ O -C -O : 117.9(4)-121,1(3)°). 
  Reference    Z. Naturforsch. 49b, 1368—1372 (1994); eingegangen am 25. April 1994 
  Published    1994 
  Keywords    M etal-Carbonato-Complex, Baylissite Type, Synthesis, Crystal Structure 
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 Identifier    ZNB-1994-49b-1368 
 Volume    49 
219Author    Stefan Peschel, Dietrich BabelRequires cookie*
 Title    Zur Kristallstruktur der Cyanoelpasolithe [N(CH3)4]2CsCo(CN)6 und [H3NCH3]2NaFe(CN)6 Concerning the Crystal Structures of the Cyano-Elpasolites [N(CH3 )4]2CsCo(CN) 6 and [H3NCH3]2NaFe(CN) 6  
 Abstract    Single crystals of the cyano com plexes [N (C H 3)4]2C sC o(C N)6 and [H3NCH 3]2N aFe(C N)6 were prepared and their structures determined by X-ray methods. The cobalt compound is monoclinic, a -885.5(1), b = 892.6(2), c = 1259.9(5) pm, ß = 90.29(4)°, space group 12Im, Z = 2; R l = 0.048 for 861 independent reflections. The resulting average distances in the nearly undistorted octahedra are C o -C = 189.8, C -N = 114.1, C s -N = 325.6 pm. The iron compound exhibits a cubic elpasolite type structure, a = 1105.2(1) pm, space group Fm 3m , Z = 4; R l = 0.040 for 127 independent reflections; F e -C = 193.4(6), N a -N = 247.7(8) pm. The orientation of the librating tetramethyl-ammonium group within the cages of the cobalt compound and the disorder of the monomethyl-ammonium cation around the special site (1/4, 1/4, 1/4) of the iron complex are discussed. 
  Reference    Z. Naturforsch. 49b, 1373—1380 (1994); eingegangen am 31. März 1994 
  Published    1994 
  Keywords    Hexacyanometallates(III), Crystal Structure, Elpasolite 
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 Identifier    ZNB-1994-49b-1373 
 Volume    49 
220Author    Stefan Horstmann, Wolfgang SchnickRequires cookie*
 Title    Synthese, Kristallstruktur und Eigenschaften von Tetraaminophosphoniumiodid [P(NH2)4]I Synthesis, Crystal Structure, and Properties of Tetraaminophosphonium Iodide [P(NH2)4]I  
 Abstract    The title compound has been prepared starting from phosphorothionic triamide SP(N H 2)3 by methylation of the sulfur atom and subsequent ammonolysis reaction in dry acetonitrile and dichloromethane, respectively, both at room temperature. Suitable single crystals are obtained from an acetonitrile solution in a temperature gradient between 70 °C and room temperature. The crystal structure o f [P(N H 2)4]I has been determined by single crystal X-ray methods (P 4!nbm\ a = 842.6(2), c = 486.7(2) pm, Z = 2). In the solid [P(NH2)4]+-and I~-ions are found with significant N -H -I -h y d r o g e n bonding interactions between anions and cations (H —I: 276.4 pm). The P -N -b o n d length in the cation (160.7(2) pm) represents the shortest P -N H 2 bond distance reported to date indicating a significant electrostatic strengthening. The condensation behaviour of [P(N H 2)4]I in solution and in the solid has been investigated. 
  Reference    Z. Naturforsch. 49b, 1381—1386 (1994); eingegangen am 5. Mai 1994 
  Published    1994 
  Keywords    Tetraaminophosphonium Salt, Synthesis, Crystal Structure, Hydrogen Bonding, Condensation Reactions 
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 Identifier    ZNB-1994-49b-1381 
 Volume    49 
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