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1986 (263)
161Author    Hartm Ut Köpf, Thomas KlapötkeRequires cookie*
 Title    Synthese und spektroskopische Charakterisierung von Metallocen-chloro-selenophenolaten Synthesis and Spectroscopic C haracterization of M etallocene Chloro Selenophenolates  
 Abstract    Bis(/75-cyclopentadienyl)-chloro-selenophenolatotitanium (IV), Bis(?75-cyclopentadienyl)-chloro-selenophenolatozirconium (IV), Bis(//5-cyclopentadienyl)-chloro-selenophenolatohafnium (IV), Bis(^5-cyclopentadienyl)-chloro-selenophenolatotungsten(IV), Mass Spectra The metallocene chloro selenophenolates C p;M Cl(SeChH 5) (Cp = ^5-C5H 5; M = Ti, Z r, Hf, W) were prepared by reaction of Cp2MCl2 with equivalent am ounts of LiSeC6H 5, obtained from phenylselenol and «-butyllithium, and were characterized by 'H NM R, IR and MS data. The fragmentation behaviour of the Ti and W derivatives is elucidated by observing m etastable transi­ tions in the mass spectra. 
  Reference    Z. Naturforsch. 41b, 971—9 (1986); eingegangen am 18. April 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0971 
 Volume    41 
162Author    Joseph Grobe, Jürgen SzameitatRequires cookie*
 Title    Reaktive E =C (p—p);r-Systeme, X [1] Darstellung und Reaktivität von Perfluor-3-phosphapent-2-en (1) Preparation and Reactivity of Perfluoro-3-phosphapent-2-ene (1)  
 Abstract    Preparation o f F SC2P = C (F)C F 3, Cycloaddition to D ien es, 
  Reference    Z. Naturforsch. 41b, 974 (1986); eingegangen am 27. März 1986 
  Published    1986 
  Keywords    Chiral Phosphanes, Mass Spectra, NM R Spectra 
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 Identifier    ZNB-1986-41b-0974 
 Volume    41 
163Author    Gerhard Bremer3, Roland Boeseb, Mustafa Keddoa, Thomas Kruck3Requires cookie*
 Title    Dialkylchalkogenidverbrückte Carbonylzweikernkomplexe des Typs  
 Abstract    [M]2ER2 mit M = {CpMn(CO)2} und {Cr(CO)5}; E = S, Se, Te; R = Me oder R2 = (CH2)3 bzw. (CH2)4; Röntgenstrukturanalyse von [CpMn(CO)2]2S(CH2)3 Dialkylchalcogenide-Bridged Dinuclear Carbonyl Complexes of the Type [M]2ER2 with M = {CpMn(CO)2} and {Cr(CO)5}; E = S, Se, Te; R = Me or R2 = (CH2)3, (CH2)4; X-Ray-Structure Analysis of [CpMn(CO)2]2S(CH2)3 The reaction o f C pM n(C O)2T H F or C r(C O)sT H F with alkylchalcogenides E R 2 (E = S, Se, Te; R = M e or R 2 = (C H 2)3, (C H 2)4) in the molar ratio of 2:1 gives alkylchalcogenide-bridged dinuclear com plexes [C pM n(C O)2]2E R 2 and [C r(C O)5]2E R 2. The heteronuclear com plex C p (C O)2Mn — (u-SM e2) -C r (C O) 5 can be synthesized by reacting C pM n(C O)2SM e2 with C r(C O)5TH F. X-ray structure analysis o f the com pound [CpM n(CO)2]2S(C H 2) 3 dem onstrates the bridging character o f the alkylchalcogenides. 
  Reference    Z. Naturforsch. 41b, 981—986 (1986); eingegangen am 24. Februar/25. April 1986 
  Published    1986 
  Keywords    Synthesis, C halcogenide-Bridged Carbonyl C om plexes, X-Ray 
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 TEI-XML for    default:Reihe_B/41/ZNB-1986-41b-0981.pdf 
 Identifier    ZNB-1986-41b-0981 
 Volume    41 
164Author    A. E. Lavat, S. B. Etcheverry, E. J. BaranRequires cookie*
 Title    Kristallographisches und spektroskopisches Verhalten einiger gemischter Phosphat/Vanadat-Fluoroapatite Crystallographic and Spectroscopic Behaviour of Some Mixed Phosphate/Vanadate Fluoroapatites  
 Abstract    Crystallographic data for m ixed phosphate/vanadate fluoroapatites o f the type M 1o(P0 4)6_J(V 0 4)AF2 (with M = Ca, Sr, Ba and x = 1—3) have been obtained from X-ray powder data. The only structural effect observed is a continuous increase of unit cell dim ensions with increased vanadate incorporation. The IR and Raman spectra show that the V 0 43 incorporation has a negligible effect on the strength of the P —O bonds, although a small bond weakening for both tetrahedral oxoanions is observed as the unit cell volum e increases. The results are com par­ able to those reported earlier for similar mixed hydroxyapatites and suggest that the fluoroapatite lattice can be considered as a good "m odel" for the vertebrate hard tissues. 
  Reference    Z. Naturforsch. 41b, 987 (1986); eingegangen am 15. April 1986 
  Published    1986 
  Keywords    Mixed A patites, Crystal Data, IR Spectra, Raman Spectra 
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 Identifier    ZNB-1986-41b-0987 
 Volume    41 
165Author    Carlos Mujica, Dieter Weber, Hans-Georg Von SchneringRequires cookie*
 Title    Chemie und Strukturchemie der Phosphide und Polyphosphide  
 Abstract    , 41 [1] Synthese, Struktur und Eigenschaften neuer silyl-, germyl-und stannylsubstituierter Heptaphosphane(3) P7(MPh3)3 mit M = Si, Ge, Sn Chemistry and Structural Chemistry of Phosphides and Polyphosphides, 41 [1] Synthesis, Structure and Properties of New Silyl, Germyl and Stannyl Substituted Heptaphosphanes(3) P7(MPh3)3 with M = Si, Ge, Sn Silyl-, Germyl-and Stannyl-substituted H eptaphosphanes(3), 3,5,7-T riphenylm etalla[2.2.1.02'6]hepta-phosphanes, Structures, Raman Spectra, 31P NM R Spectra New derivatives P7(M Ph3) 3 (M = Si, G e, Sn) o f the heptaphosphanortricyclen cage were synthesized by reactions o f P7(SiM e,) 3 with com pounds CIMPh,. The driving force o f the reaction is the lower solubility o f the P7(M P h,) 3 com pounds. W hereas crystals of P7(SiM e3) 3 are enan-tiom orphs, the new com pounds P7(M Ph3) 3 crystallize as racemates. With decreasing M size, the nortricyclen cage P7 is slightly twisted about the 3-fold axis. The main P -P bond lengths in the cage follow the relation A (basal) — 221.8 pm > B (basal-equatorial) = 219.0 pm > C (equato-rial-apical) = 218.5 pm. The m ean bond lengths P —Si = 228.6 and P —Ge = 234.9 and P —Sn = 253.5 pm are slightly larger than the standard single bond distances. The IR absorptions show only very small M -dependent variations in the characteristic internal cage vibrations. Similar effects are recognized in the 3,P NM R chem ical shifts. 
  Reference    Z. Naturforsch. 41b, 991 (1986); eingegangen am 20. März 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0991 
 Volume    41 
166Author    P. Böttcher, W. FlammRequires cookie*
 Title    Die Kristallstruktur des Bis(tetrapropylammonium)heptasulfids [N(C3H7)4]2S7 The Crystal Structure of Bis(tetrapropylammonium)heptasulfide [N(C3H7)4]2S7  
 Abstract    Crystal Structure, Polychalcogenides Bis(tetrapropylam m onium)heptasulfide results from the reaction o f [(C3H 7) 4N ]Br and N a2S5 (molar ratio 4:1 to 2:1) in aqueous solution. The dark orange com pound crystallizes in the space group P2!/c, the lattice constants are (at —70 °C): a = 9.466(4) Ä , b = 11.013(3) Ä. c = 16.845(7) Ä , ß = 105.6(1)°. It contains unbranched chainlike S72 anions of all-trans-conioxma-tion. 
  Reference    Z. Naturforsch. 41b, 1000—1004 (1986); eingegangen am 28. April 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1000 
 Volume    41 
167Author    WolfPeter Fehlhammer, Ulrike PlaiaRequires cookie*
 Title    Metallkomplexe funktioneller Isocyanide, XIII [1] Bis(oxazolidin-2-yIiden)-Komplexe von Mangan(I) und Nickel(II) Metal Complexes of Functional Isocyanides, XIII [1] Bis(oxazolidin-2-ylidene) Complexes of Manganese(I) and Nickel(II)  
 Abstract    The dicarbene com plexes, M nB r(C O)3(C N (H)C H ^C FI.O) 7 (1) and 
  Reference    Z. Naturforsch. 41b, 1005 (1986); eingegangen am 21. Februar 1986 
  Published    1986 
  Keywords    Organometallic Chemistry, Functionalized Isocyanides, Activation by Coordination Carbene C om plexes, X-Ray 
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 Identifier    ZNB-1986-41b-1005 
 Volume    41 
168Author    W. Calaminus, F. Vögtle, FaE M ErckRequires cookie*
 Title    Das Dispiro[5.1.5.1]tetradecan-Gerüst als Baustein für thermotrope Flüssigkristalle  
 Abstract    D isp iro[5.1.5.1 Jtetradecane U nit. Thermotropic Liquid Crystals Several 3 .1 1 -disubstituted dispiro[5.1.5.1]tetradecane-7,14-dions were prepared and the 
  Reference    Z. Naturforsch. 41b, 1011 (1986); eingegangen am 16. Januar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1011 
 Volume    41 
169Author    Henryk Zegota^, Nien Man, Dorothea Schuchmann, Clemens Schulz, Von SonntagRequires cookie*
 Title    Acetonylperoxyl Radicals, CH3C 0C H 20 2: A Study on the y-Radiolysis and Pulse Radiolysis of Acetone in Oxygenated Aqueous Solutions  
 Abstract    Pulse R adiolysis. A ceto n e, A cetonylperoxyl Radical, Superoxide Radical H ydroxyl radicals from the radiolysis o f N 20 / 0 2 (4:l)-saturated aqueous solutions o f acetone (10 3 m ol d m -3) react with the solute by H-abstraction thereby forming acetonyl radicals. A s shown by pulse radiolysis, the acetonyl radicals rapidly add oxygen (k = 3 x 109 dm 3m ol_1s _1) thereby forming acetonylperoxyl radicals which decay by second-order kinetics (2 k = 8 x 10* dm 3mol ' s -1). U nder steady-state radiolysis conditions (0.24 G y s "1) the products (G values in parentheses) are m ethylglyoxal (2.5). hydroxyacetone (0.5), form aldehyde (1 .6), acids (1 .7), carbon dioxide (0 .5), organic (hydro)peroxides (0.4), hydrogen peroxide (2 .2), and G (oxygen uptake) has been determ ined at 5.2. In the decay of the acetonylperoxyl radicals the m ajor process (slightly less than one half) leads in a concerted reaction to two m olecules o f m ethyl­ glyoxal and one m olecule o f hydrogen peroxide. The Russell m echanism which yields one m olecule o f m ethylglyoxal. hydroxyacetone and oxygen contributes about one fifth as does the breakdown into two m olecules o f form aldehyde, one m olecule o f oxygen and two acetyl radicals. Carbon dioxide, formaldehyde and acetic acid are among the products which result from the acetylperoxyl radicals formed upon oxygen addition to the acetyl radicals. A bout one tenth o f the organic peroxyl radicals is converted into hydroperoxides by OJ produced as a byproduct in the water radiolysis. 
  Reference    Z. Naturforsch. 41b, 1015—1022 (1986); received April 7 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1015 
 Volume    41 
170Author    WolfPeter Fehlhammer, Eberhard Bär, Borislav BoyadjievRequires cookie*
 Title    Chemie der Isoblausäure  
 Abstract    , II [1] Reaktionen von [M(CO)5CNH] (M = Cr, Mo, W) mit Aziridinen: Zyklische Diaminocarbenkomplexe Chemistry of Hydrogen Isocyanide, II [1] Reactions of [M(CO)5CNH] (M = Cr, Mo, W) with Aziridines: Cyclic Diaminocarbene Complexes The hydrogen isocyanide com plexes [M (C O)5CNH] (M = Cr, M o, W) have been treated with the aziridines R N C H R 'C H 2 (R = H, R' = H, Me, Et; R = M e, R' — H) to give im idazolidin-2-ylidene com plexes. The sam e type of ligand forms on addition of aziridine to the electrophilic isocyanide group in [FpC N Ph]+ in the presence of B r'. IR, 'H N M R , 13C N M R and mass spectra of the new com pounds are reported. 
  Reference    Z. Naturforsch. 41b, 1023—1027 (1986); eingegangen am 14. April 1986 
  Published    1986 
  Keywords    Functionalized Isocyanides, Reactions at Coordinated Ligands, Ring O pening and Closure, Carbene C om plexes 
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 Identifier    ZNB-1986-41b-1023 
 Volume    41 
171Author    Günter Schmid, Wilfried HusterRequires cookie*
 Title    Große Übergangsmetallcluster, IV [1, 2]  
 Abstract    The novel cluster com pounds R u55[P (/m -B u)3]12Cl20, Rh55(PPh3) 12Cl6 and Pt55[A s(rm -B u)3] 12C120 have been prepared by the reaction o f (R uC l3/P (rm -B u)3), (Ph3P)3RhCl and rra/75-[As(/m -Bu)3]2PtCl2, respectively, with B 2H 6 in TH F or benzene. D iborane reduces the m etal salts and serves to capture excess o f phosphine or arsine ligands. M olecular w eight determ i­ nations prove the cluster size. High resolution transmission electron microscopic investigations on the Ptss cluster show the expected full-shell cuboctahedron with 55 closest-packed platinum atom s. 31P N M R spectra prove the ligands to be very m obile. 
  Reference    Z. Naturforsch. 41b, 1028 (1986); eingegangen am 30. April 1986 
  Published    1986 
  Keywords    -, Rh55-und Pt55-Cluster Large Transition Metal Clusters, IV [1, 2] Ru55-, Rh55-and Pt55-Clusters Clusters, R u55, R h55, Pt55, Transition M etal Clusters 
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 Identifier    ZNB-1986-41b-1028 
 Volume    41 
172Author    Viqar Uddin, Ahmad, Shoih Arif, Aziz-Ur-Rahman Amber, M. Ajmal, NasirH E J, K.Usman GhaniRequires cookie*
 Title    A New Alkaloid from Root Bark of Capparis decidua  
 Abstract    Spermidine A lkaloid, Capparis decidua A new spermidine alkaloid, capparisine (1) has been isolated from the alcoholic extract o f the root bark of Capparis decidua, and its structure was elucidated by spectral studies. 
  Reference    Z. Naturforsch. 41b, 1033—1035 (1986); received February 20 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1033 
 Volume    41 
173Author    Bernd Kohne, Klaus Praefcke, Jan BillardRequires cookie*
 Title    Uber die drei discotischen Mesophasen der scj//o-Inosithexaester [1] On the Three Discotic Mesophases of scy//o-Inositol Hexaesters [1]  
 Abstract    scy/Zo-Inositol, Cyclohexane D erivatives, D iscogens o f a Natural Product, D iscotic M esophases D". D ,, D E 
  Reference    Z. Naturforsch. 41b, 1036—1044 (1986); eingegangen am 2. Dezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-1036 
 Volume    41 
174Author    Dieter Hellwinkel, HeinrichGeorg Gaa, Reiner GottfriedRequires cookie*
 Title    Inverse Triphenylmethylium-Farbstoffe Inverse Triphenylmethylium Dyes  
  Reference    Z. Naturforsch. 41b, 1045—1060 (1986); eingegangen am 17. A pril 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1045 
 Volume    41 
175Author    Ulf Thewalt, Konrad Holl, Udo Demant, Ulrich Müller, Kurt DehnickeRequires cookie*
 Title    Untersuchungen zur möglichen Existenz des S4N4@-Radikalkations und die Kristallstruktur von S4N4H[FeCl4] Investigations Concerning the Possible Existence of the S4N4® Radical Cation and the Crystal Structure of S4N4H[FeCl4]  
 Abstract    Brom ination o f S4N 4 Cl[FeCl4], Preparation o f S4N 4 H [FeX 4] (X = Cl, Br), IR Spectra, Crystal Structure of S4N4H[FeCI4] S4N 4 H [FeC l4] as well as S4N 4 D [F eC l4] were prepared in C H 2C12 by reaction o f S4N 4 with FeC l3 and C H 3C O O H and CH 3C O O D , respectively. Bromination o f S4N 4C l[FeCl4] with M e3SiBr in C H 2 C12 yields S4N 4 H[FeBr4]; in this reaction, S4N 4 Br® is presumably formed initially; it then decom p oses by elimination o f bromine and formation of the S4N 4® radical cation; the latter reacts with the solvent, yielding the S4N 4 H® cation. Brom ination of S3N 2C l[FeCl4] with M e3SiBr affords S6N 4 [FeBr4]2. The IR spectra o f the com pounds are discussed. The crystal structure o f S4N 4 H [FeC l4] was determined by X-ray diffraction (1210 observed reflexions, R = 0.035). Crystal data: a = 803.8, b — 1003.9, c = 1507.7 pm, ß = 104.52°, Z = 4, space group P 2,/c. 
  Reference    Z. Naturforsch. 41b, 1061 (1986); eingegangen am 7. Mai 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1061 
 Volume    41 
176Author    S. S. Kumaravel, S. S. Krishnamurthy, B. R. Vincent, T. S. CameronRequires cookie*
 Title    Assignment of 31P Chemical Shifts to Isomers of 2,3-Dialkoxy-A3-diazadiphosphetidines — Crystal and Molecular Structure of rrflMs-[PhNP(OCH2CF3)]2  
 Abstract    Trifluoroethoxydiazadiphosphetidine, cis-trans Isom erisation, Crystal Structure, 31 P N M R Spectra G eom etrical isom ers of /.3-diazadiphosphetidines show large differences in their 31P chem ical shifts. Trifluoroethoxylation o f rä-(P h N P C l) 2 gives only the 'low-field' isom er initially, for which the crystal structure is determ ined. The compound crystallises in the triclinic space group P 1 with a = 9 .6 2 4 (4).6 = 1 0 .107(4),c = 11.140(7) Ä ; a = 105.65(4),ß = 1 10.59(4),y = 93 .8 2 (3)°;a n d Z = 2. The structure was solved by direct m ethods and refined to R = 0.045. The alkoxy groups are trans to each other. On standing in solution. rra/J5 -[PhN P(O C H 2 CF3) ] 2 transforms slowly and almost com pletely into its cis analogue with a high field 31P chemical shift. 
  Reference    Z. Naturforsch. 41b, 1067—1070 (1986); received May 5. 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1067 
 Volume    41 
177Author    M. Veith, R. RosierRequires cookie*
 Title    Alkoxistannate, II [1] Tri(te/*-butoxi)alkalistannate(II): Darstellung und Strukturen Alkoxistannate, II [1] Tri(rerr-butoxi)alkalistannates(II): Synthesis and Structures  
 Abstract    Tri(terf-butoxi)alkalistannates (M (O rBu)3Sn, M = Li, Na, K, Rb, Cs) are obtained by reaction of alkali-fert-butanolates with tindi-terf-butoxide. If M equals Li or Na (1, 2) molecular com ­ 
  Reference    Z. Naturforsch. 41b, 1071 (1986); eingegangen am 12. F eb ru ar/17. März 1986 
  Published    1986 
  Keywords    Synthesis, Polycyclic C om pounds, Crystal Structure, M olecular Structure, X -R ay 
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 Identifier    ZNB-1986-41b-1071 
 Volume    41 
178Author    F. E. Senftle+, D. B. WrightRequires cookie*
 Title    Synthesis of Au2S and Au2S3 Using H2S, Short-Chain and Ring-Structured Sulfur as Sulfur Sources  
 Abstract    Gold Sulfide, A llotropes o f Sulfur; G old Sulfate, co-Sulfur To determine which o f the two known gold sulfides (containing either m ono-or trivalent gold) are formed by reacting trivalent gold with differnt allotropes o f sulfur, experim ents were made using three different sources o f sulfur. W hen trivalent gold in the form of A u 2 (S 0 4) 3 in concen­ trated acid is reacted with electrolytically form ed short-chain sulfur, m onovalent gold sulfide (A u 2S) is formed. If hydrogen sulfide gas reacts with the sam e solution, trivalent gold sulfide (A u 2S3) is produced. A lternatively, if ordinary a-sulfur (ring structure) is used, a 50/50 mixture of A u 2S and A u 2S3 is formed. The synthesis procedure for the two gold sulfides is substantially simpler than previously reported m ethods o f preparation. 
  Reference    Z. Naturforsch. 41b, 1081 (1986); received December 12 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-1081 
 Volume    41 
179Author    Fritz Preuss, Harald Noichl, Jürgen KaubRequires cookie*
 Title    Darstellung und Struktur der terr-Butyliminovanadiuni(V)-Verbindungen 'C4H9N =V (S R )3 (R = 'C4H9, SiPh3)  
 Abstract    Synthesis and Molecular Structure of rerf-Butyliminovanadium(V) Compounds 'C4H9N=V(SR)3 (R = 'C4H9, SiPh3) Thiolato Im inovanadium (V) Com pounds. Preparation. X-Ray D ata, MV NM R Spectra 
  Reference    Z. Naturforsch. 41b, 1085—1 (1986); eingegangen am 4. April 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1085 
 Volume    41 
180Author    CarlH. Abben, A. Nton, M. Eller, M. Athias, Noltemeyer, GeorgeM. SheldrickRequires cookie*
 Title    Synthese, Molekül-und Kristallstruktur von 3-(2,6-Dimethylphenylamino)-4,5-diethyl-l,2,3-diselenaborol  
 Abstract    Synthesis, M olecular and Crystal Structure of 3-(2,6-D im ethylphenylam ino)-4,5-diethyl-1,2,3-diselenaborole 1,2,3-D iselen aborole D erivatives, M olecular and Crystal Structure The title com pound, isolated from the reaction of 3-iodo-4,5-diethyl-l,2,3-diselenaborol with 
  Reference    Z. Naturforsch. 41b, 1093—1095 (1986); eingegangen am 6. Juni 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-1093 
 Volume    41 
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