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1986 (263)
101Author    Borislav Bogdanović, G. Udrun, K. Oppetsch, Carl Krüger, RichardM. YnottRequires cookie*
 Title    Magnesiumorganische Innerkomplexe, Teil II [1] Ethyl(dialkylaminoalkyl)-und Ethyl(4-alkoxybutyl)magnesium-Verbindungen Organomagnesium Inner Complexes, Part II [1] Ethyl(dialkylam inoalkyl)-and Ethyl(4-alkoxybutyl)magnesium Compounds  
 Abstract    The reaction o f bis(dialkylam inoalkyl)-and bis(4-alkoxybutyl)m agnesium inner com plexes with M gEt2 leads to the form ation of ethyl(dialkylam inoalkyl)-and ethyl(4-alkoxybutyl)m agnesium com pounds. The X -ray crystal structures o f ethyl(3-N ,N -dim ethylam inopropyl)m agnesium and ethyl(3-N -cyclohexyl-3-N -m ethylam inopropyl)m agnesium confirm that the com pounds are dim eric with the a-C -atom o f the chelating ligand bridging the magnesium atoms. The difference in reactivity of the M g —Et and M g—C"H2nX bonds (X = NR 'R ", O R) makes itself apparent in the reaction of these com plexes with ethylene: up to six ethylene m olecules are inserted, whereby in the case of the ethyl(4-alkoxybutyl)m agnesium com pounds insertion occurs preferentially into the M g—Et bond w hereas in the case o f the ethyl(dialkylam inoalkyl)m agne-sium com pounds both bonds are equally reactive. 
  Reference    Z. Naturforsch. 41b, 617 (1986); eingegangen am 21. N ovem ber 1985 
  Published    1986 
  Keywords    M agnesium, Inner C om plexes, Crystal Structures 
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 Identifier    ZNB-1986-41b-0617 
 Volume    41 
102Author    Wilhelm Kuchen, Wolfgang HönleRequires cookie*
 Title    Reaktionen koordinierter Liganden, III [1] Stabilisierung von Dimenthyldiphosphen und Menthylphosphiniden als Brückenliganden in Metallcarbonylkomplexen  
 Abstract    Diphosphene C om plexes, Phosphinidene C om plexes, Crystal Structure Reduction o f M entPBr2M (C O)5 1 (M = Cr, W) with magnesium in TH F yields the diphos­ phene com plex (C O)5M (M en t)P = P (M en t)M (C O)5 2 as the main product. In addition, a phos­ phinidene com plex, (C O)5M (M ent)P M (C O)5 (3) is also formed. The latter is obtained in larger am ounts, if the reaction is carried out in the presence o f M (C O)5TH F. The proposed structures are confirm ed by N M R and U V data as well as — in the case o f the chromium com pounds (2a, 3a) — by crystal structure analysis. Com pound 2a is obtained only as the frans-isomer. The P —P distance in 2a (204.0 pm) indicates a double bond which does not participate in the com ­ plex formation. The P —Cr distance in 3a (average: 230.3 pm) is within the low est range found for this elem ent com bination. R eaction o f 2a with L iA lH 4 yields the diphosphane com plex (C O)5C rM ent(H)P —P (H)M en tC r(C O)5 4 as a mixture o f "m eso" and "rac" diastereom ers. 
  Reference    Z. Naturforsch. 41b, 629—639 (1986); eingegangen am 13. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0629 
 Volume    41 
103Author    H. Ans-, Dietrich Stachel, H. Erm, Ann Poschenrieder, Hans BurghardRequires cookie*
 Title    Synthese von 5-Alkyliden-3-pyrrolin-2-onen Synthesis of 5-Alkylidene-3-pyrrolin-2-ones 5-A lkylidenetetram ic A cids, 5-Alkylidene-4-hydroxypyrrolidin-2-ones, 5-A lkylidenepyrrolin-2-ones, Reduction  
  Reference    Z. Naturforsch. 41b, 640 (1986); eingegangen am 6. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0640 
 Volume    41 
104Author    Erhard Jägers, Vinayagar Pasupathy, A. Nke, H. Ovenbitzer, Wolfgang Steglich-Requires cookie*
 Title    Suillin, ein charakteristischer Inhaltsstoff von Röhrlingen der Gattung Suillus (Boletales) Suillin, a Characteristic M etabolite from Boletes of the Genus Suillus (Boletales)  
 Abstract    Fruiting bodies o f several S u illu s species contain a colourless com pound, suillin, which is concentrated in the cuticle o f the pileus. Its structure has been established as4-acetoxy-3-geranyl-g eran yl-l,2 -dihydroxybenzene (1) by spectroscopic evidence, conversion into a cyclic carbonate 2 and synthesis o f its deacetyl derivative 3. 
  Reference    Z. Naturforsch. 41b, 645 (1986); eingegangen am 9. Januar 1986 
  Published    1986 
  Keywords    Su illu s Species, B oletales, B asidiom ycetes, Suillin 
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 TEI-XML for    default:Reihe_B/41/ZNB-1986-41b-0645.pdf 
 Identifier    ZNB-1986-41b-0645 
 Volume    41 
105Author    Reinhold Tacke3, A. Nke Bentlage-Felten, H. Aryanto, Linoha, StephenM. AgdabRequires cookie*
 Title    Sila-Pharmaka, 34. Mitt. [1] Sila-Analoga des Triparanols und Ethamoxytriphetols: Synthese sowie pharmakologische und toxikologische Eigenschaften  
 Abstract    Starting from tetram ethoxysilane, sila-triparanol 4b and sila-ethamoxytriphetol 8b were synthesized by four-step syntheses. 4b and 8b exhibit a strong hypolipidem ic activity in mice after p.o. administration. W hereas 4b and its carbon analogue triparanol (4a) show a similar hypolipidem ic potency, 8b was found to be less potent than its carbon analogue etham oxy­ triphetol (8a). The silicon com pounds 4b and 8b are less toxic (repeated administration over a period o f 8 days) than the corresponding carbon analogues 4a and 8a, respectively. 
  Reference    Z. Naturforsch. 41b, 649 (1986); eingegangen am 11. Novem ber 1985 
  Published    1986 
  Keywords    Sila-Substitution, Triparanol, Etham oxytriphetol, H ypolipidem ic Activity Toxicological Properties 
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 Identifier    ZNB-1986-41b-0649 
 Volume    41 
106Author    H. Orst, W. Eber, G. Otelind Von Der Lippe, MagdalenaM. AtyjaRequires cookie*
 Title    Die oxidative Spaltung von Pseudobasen 2-a-alkylierter 2,3-CycIoaIkenopyridinium-Salze Oxidative Cleavage of Pseudobases from 2-a-A lkylated 2,3-Cycloalkenopyridinium Salts  
 Abstract    Cycloalka[b]pyridinium Salts, Hexacyanoferrate(III) O xidation, Pyridinones In contrast to former assumptions pyridinium salts with a tertiary 2-a-C -atom like 2 a and 16 are not oxidized to pyridinium-carbinol interm ediates during alkaline hexacyanoferrate(III) oxidation 
  Reference    Z. Naturforsch. 41b, 655—661 (1986); eingegangen am 9. D ezem ber 1985 
  Published    1986 
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 Identifier    ZNB-1986-41b-0655 
 Volume    41 
107Author    W. Olfdieter, A. SchenkRequires cookie*
 Title    N O T IZ E N Schwefeldioxid als Brückenligand zwischen zwei verschiedenen Metallatomen [1] Sulfur Dioxide as Bridging Ligand Between Two Different M etal Atom s [1]  
 Abstract    Bim etallic C om plexes, Sulphur D ioxide Bridge The com pound MoRhCl(M-dppm)2(C O)2(u-CO)(M-SC)2) (1) is ob­ tained from M oR hC l(/i-dppm)2(C O)4 and S 0 2. 1 is the first hetero-bim etallic com plex o f sulfur dioxide. 
  Reference    Z. Naturforsch. 41b, 663 (1986); eingegangen am 7. Februar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0663_n 
 Volume    41 
108Author    G. Erd Seemann, Karl HensenRequires cookie*
 Title    Das Phasendiagramm des Systems Aluminiumchlorid-Pyridiniumchlorid D eterm ination of the Phase Diagram Alum inium chloride-Pyridinium chloride  
 Abstract    A lum inium chloride, Pyridinium chloride, Phase Diagram A phase equilibrium study o f the system alumini-um chloride and pyridiniumchloride has been car­ ried out. The phase diagram of the system indicates the existence o f four congruently m elting com ­ pounds o f the molar ratio A lC l3/PyH C l 1:1, 1:2, 1:3, 2 :3 . 
  Reference    Z. Naturforsch. 41b, 665—666 (1986); eingegangen am 21. Januar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0665_n 
 Volume    41 
109Author    Hartmut Köpf, Thomas KlapötkeRequires cookie*
 Title    Synthese und Konformationsstudien ringsubstituierter Titanocen-Dithiolen-Chelate Synthesis and Conform ational Studies of Ring-Substituted Titanocene Dithiolene Chelates  
 Abstract    Titanocene D ithiolen e C helates, D ithiolene Chelate Ring Conform ation, Bis(?7;'-m ethylcyclopentadienyl)-toluene-3,4-dithiolato-titanium (IV), ?/5-Cyclopentadienyl-?7:'-m ethylcyclopentadienyl-toluene-3,4-dithiolato-titanium (IV) The titanocene dithiolenato chelates Cp'2Ti(S2C6H 3C H 3-4) and C pCp'Ti(S2C6H 3CH 3-4) (Cp = 7/5-C5H 5, Cp' = 775-C5H 4C H 3) were prepared by reaction o f C p'2TiCl2 or CpCp'TiCl2 with equiva­ lent amounts o f l,2 -(L iS)2CftH 3C H 3-4. The structure and the conform ational mobility o f the ^"'-bonded and o f the chelating ligands o f the dithiolenato com plexes are discussed on the basis o f their tem perature-dependent 'H N M R spectra. The mass spectra show m etastable transitions for the fragmentation processes. 
  Reference    Z. Naturforsch. 41b, 667—670 (1986); eingegangen am 5. März 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0667 
 Volume    41 
110Author    FrauRequires cookie*
 Title    f/5-2,3-Dihydro-l,3-diborol-Komplexe des Rhodiums [1] A norganisch-C hem isches Institut der Universität, Im N euenheim er Feld 270, D -6900 H eidelberg  
 Abstract    2 ,3-D ih yd ro-l,3-d ib orole, Rhodium Sandwich Com plexes 
  Reference    Z. Naturforsch. 41b, 671 (1986); eingegangen am 2. Januar/25. Februar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0671 
 Volume    41 
111Author    Josef Hahn, Klaus Altenbach, FrauRequires cookie*
 Title    Ausgangsverbindungen zur Darstellung von Sulfanen H2S" und D 2S" mit definierter Kettenlänge Bis(methyldiphenylsilyl)-sulfanes: Starting Compounds for the Preparation of Sulfanes H 2S" and D 2S" of Definite Chain Length  
 Abstract    The silylsulfanes (M ePh2Si)2S", n — 2 —5 (la —d), have been prepared by reacting M ePh2SiSNa (2) with iodine or chlorosulfanes SmCl2, m = 1 -3 , in toluene solution. Com pounds l a —d, which 
  Reference    Z. Naturforsch. 41b, 675 (1986); eingegangen am 24. Januar 1986 
  Published    1986 
  Keywords    Bis(m ethyldiphenylsilyl)-sulfanes, Silylsulfanes, Sulfanes, D euterosulfanes 
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 Identifier    ZNB-1986-41b-0675 
 Volume    41 
112Author    R. Benn, P. W. Jolly, T. Joswig, R. Mynott, K.-P SchickRequires cookie*
 Title    Intermediates in the Palladium-Catalysed Reactions of 1,3-Dienes, Part 5 [1] Butadiene Complexes of Nickel, Palladium and Platinum  
 Abstract    Nickel-organo Com plex. Palladium-organo Complex, Platinum-organo Complex, Butadiene Complex A series of [M (R 2PC2H 4PR :)(butadiene)] complexes of Ni, Pd and Pt has been prepared and their structures investigated NM R-spectroscopically. The nickel and palladium complexes, irrespective of the substituents at phosphorus, contain a fluxional ?/2-bonded butadiene molecule. In the case of platinum the bonding mode is ligand dependent: an ^-arrangement is observed where R is tert-butyl or cyclohexyl while when R is isopropyl the butadiene adopts an rj', ^'-arrangement to give a platinacyclopentene derivative. 
  Reference    Z. Naturforsch. 41b, 680—691 (1986); received D ecem ber 10 1985/February 5 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0680 
 Volume    41 
113Author    Thomas Krämer, Joachim SträhleRequires cookie*
 Title    Synthese, Eigenschaften und Struktur von Bipyridin-Halogeno-Komplexen des Cobalts Synthesis, Properties and Structure of Bipyridine H alogeno Complexes of Cobalt  
 Abstract    Bis(2,2'-bipyridine)dihalogeno C obalt(II), cis, trans Structure, Bis(2,2'-bipyridine)(4,4'-bipyridine) C obalt(II) Polymer The cobalt(II) 2,2'-bipyridine complexes C o(2,2'bpy)2X2 (X = Cl, Br, I) have been synthesized from the anhydrous halides and a stoichiometric am ount of 2,2'-bipyridine in acetonitrile. From the IR spectra a trans configuration is assumed for the chloro complex. For the brom o and iodo com pound an ionic form [C o(2,2'bpy)2X]X with a square pyram idal coordination of the Co atom is more likely. ds-[C o(2,2'bpy)2Cl2] • 1,5C 2H 4C12 was obtained from C o(2,2'bpy)2I2 in 1,2-di-chloroethane. It crystallizes with Z = 4 in the monoclinic space group P 2 x/n: a = 1379.4, b = 1325.9. c — 1423.9 pm, ß = 97.11°. Very long Co —Cl bond distances of 239.2 and 245.0 pm are observed, while the C o—N distances (213.8 to 217.4 pm) are of normal length. Reaction of C o(2.2'bpy)2I2 with 4,4'-bipyridine yields [C o(2,2'bpy)2(4,4'bpy)]2+ which is easily oxidized to give a polymeric complex that exhibits a conductivity of 10~6 S/cm. 
  Reference    Z. Naturforsch. 41b, 692 (1986); eingegangen am 28. F ebruar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0692 
 Volume    41 
114Author    Martin Haase, E. KlingebielRequires cookie*
 Title    Tris(silyl)sily 1-chlorsilane und P-halogenierte Silylphosphane Tris(silyl)silyl-chlorosilanes and P-Halogenated Silylphosphanes  
 Abstract    Tris(silyl)silyllithium, H alogenosilylphosphane, Silylhalogenophosphane, Silicon-Halogen Exchange Lithium -tris(trimethylsilyl)silan reacts with chlorosilanes to give therm ally stable com pounds (1—3). The chlorination of 3 leads to the formation of the silane (M e3Si)3SiSi(Cl)(CM e3)2 4. The reaction of tetram ethylpiperidinodihalogenophosphanes with (M e3Si)3SiLi results in th er­ mally stable compounds (M e3Si)3Si —P(H al)N (C M e2)2(C H 2)3, H al = F (5), Cl (6), (M e3Si)3Si—P(C l)N (C H M e2)2 (7) undergoes therm al rearrangem ent via a silicon-chlorine ex­ change reaction to give (M e3Si)2Si(C l)—P(SiMe3)N (C H M e2)2 (8). A byproduct — besides cyclic phosphanes -is the silylamine (M e3Si)2Si(Cl)N(CHM e2) (9). The form ation of (9) can be ex­ plained via the elimination of the phosphinidene M e3SiP. 
  Reference    Z. Naturforsch. 41b, 697—701 (1986); eingegangen am 21. Februar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0697 
 Volume    41 
115Author    WolfgangH. Eininger, R. Olf Stucka, Günter NagorsenRequires cookie*
 Title    Ein neues Silicat-Anion: [Si(NCS)6]2 A N ew Silicate Anion: [Si(N C S)6]2  
  Reference    Z. Naturforsch. 41b, 702—707 (1986); eingegangen am 7. Februar 1986 
  Published    1986 
  Keywords    New H exacoordinated Anionic Silicon Complex, H exaisothiocyanatosilicate, Synthesis, IR Spectra, X-Ray Spectra 
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 Identifier    ZNB-1986-41b-0702 
 Volume    41 
116Author    Ekkehard Lindner, Abraham Kandenkulathu, D. Varughese, Ieter Hübner, Otto Eberle, Bernd SchillingRequires cookie*
 Title    Biologisch aktive 1,2,4-triazol-und imidazolhaltige phosphorylierte Alkohole Biologically A ctive 1,2,4-Triazole and Imidazole Containing Phosphorylated A lcohols  
 Abstract    The addition of the secondary phosphane chalkogenides H P (E)R 2 (E = O , S) to the 1,2,4-triazole or imidazole containing ketones R 'C 6H 4—C (O)—C H R 2—X (2, 3) [X = C2H 2N3 (2), C3H 3N2 (3)] results in the form ation of the phosphorylated alcohols R2P(E) —C (O H)C 6H 4R '-C H R : —X (4, 5). 4, 5 are fungicides with partially high activity. Their structures are discussed on the basis of the IR and NM R spectra. 
  Reference    Z. Naturforsch. 41b, 708—717 (1986); eingegangen am 31. Januar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0708 
 Volume    41 
117Author    Lutz Dahlenburg, Constanze Prengel, Nils HöckRequires cookie*
 Title    Oligophosphan-Liganden, XX [1] Reduktion von C 0 2 am Trisphosphanrhodium(I)-Komplex RhCl[f-BuP(CH2CH2CH2PMe2)2] Oligophosphine Ligands, X X [1] Reduction of Carbon D ioxide by the Trisphosphinerhodium (I) Complex RhCl[r-BuP(CH2CH2CH2PM e2)2]  
  Reference    Z. Naturforsch. 41b, 718—721 (1986); eingegangen am 28. Februar 1986 
  Published    1986 
  Keywords    C arbon Dioxide, Bis(3-dim ethylphosphinopropyl)fm -butylphosphine, Rhodium Complexes, NMR Spectra, X-Ray 
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 Identifier    ZNB-1986-41b-0718 
 Volume    41 
118Author    CorneliusG. Kreiter, EduardM. Ichels, Jürgen KaubRequires cookie*
 Title    Chrom(O)-und Molybdän(0)-Komplexe von ll-Isopropyliden-bicyclo[4.4.1]undeca-2,4,8-trienen Chromium(O) and Molybdenum(O) Com plexes of 1 l-Isopropylidene-bicyclo[4.4. l]undeca-2,4,8-trienes  
 Abstract    Bicyclic T etraenes. A m bidentate 6-Electron Ligands ll-Isopropylidene-bicyclo[4.4. l]undeca-2.4,8-triene (IB U , 1A) and five alkyl substituted de­ rivatives (1 B—IF) contain a conjugated diene unit and two isolated CC-double bonds, one exocyclic and one incorporated into the bicyclus, each suited for complexation to transition metals. With [C r(CO)3(C H 3CN)3] (2) 1 A -1 F form [C r(CO)3(?76-IBU)] complexes (3 A -3 F) , in which the IBU ligands are coordinated to the chromium via the diene unit and the exocyclic CC-double bond. The corresponding [M o(C O)3(t;6-IBU)] complexes (5 A —5F) are obtained from the reactions of [M o(CO),(diglyme)] (4) with 1 A —IF . In addition, the isomeric [Mo(CO),(?76-IBU)] complexes (6 A —6D) are form ed, in which the IBU ligands are bound to molybdenum via the three cyclic CC-double bonds. The complexes 3 A —3F, 5 A —5F and 6 A —6D were studied by IR and N M R spectroscopy ('H , 13C) and characterized by C, H elem ental analyses. The crystal and molecular structure of 1A was determ ined by X-ray structure analysis. 
  Reference    Z. Naturforsch. 41b, 722—730 (1986); eingegangen am 10. März 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0722 
 Volume    41 
119Author    JulianeW. Olf, D. Ieter, Weber, H. Ans-G, Von Eorg, SchneringRequires cookie*
 Title    Rubidium-diarsasilicat(IV) Rb2SiAs2, ein Derivat der SiS2-Struktur Rubidium Diarsasilicate(IV) R b2SiA s2, a D erivative of the SiS2 Structure Type  
 Abstract    Rubidium D iarsasilicate(IV), P reparation, Structure R b2SiAs2 was found as a byproduct in the course of the RbAs synthesis in a quartz container. The direct synthesis from the elem ents yields pure sam ples within 5 h at 925 K. R b2SiAs2 forms transparent red needle-shaped crystals which split to bunches of golden, reflecting fibres. The compound is sensitive against m oisture. R b2SiAs2 is isotypic to K2SiP2 with a polyanionic chain [SiAs2]2~ of edge-connected tetrahedra (isostructural and isoelectronic to SiS2) formed in a dis­ torted cubic closed packed As arrangem ent, and with R b in the octahedral holes (Ibam , No. 72; a = 726.6(5), b = 1377.1(6), c -638.9(3) pm; Z = 4; S i-A s = 238.1 pm ; A s -S i -A s = 95.7° and Si—A s—Si = 84.3° in the four m em bered Si2A s2 rings). 
  Reference    Z. Naturforsch. 41b, 731—735 (1986); eingegangen am 24. Februar 1986 
  Published    1986 
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 Identifier    ZNB-1986-41b-0731 
 Volume    41 
120Author    Requires cookie*
 Title    Calamitische Flüssigkristalle: Beziehung zwischen Molekülstruktur und Mesogenität, trans-und ds-l,3,5,7-TetraoxadecaIin-Derivate [1,2]  
  Reference    Z. Naturforsch. 41b, 736 (1986) 
  Published    1986 
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 Identifier    ZNB-1986-41b-0736 
 Volume    41 
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