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Facet   section ZfN Section B:Volume 038  [X]
Facet   Publication Year 1983  [X]
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1983[X]
61Author    Boron, Arsenic Methoxotetrafluorotellurates, Vi, Walter Tötsch, Heinrich Aichinger, Fritz SladkyRequires cookie*
 Title    Bor-und Arsen-methoxotetrafluorotellurate(VI)  
 Abstract    Synthesis, Boron and Arsenic Methoxotetrafluorotellurates(VI), NMR Spectra The interaction of eis-and tfrans-HOTeRiOCHs with BG3 yields B(cis-and trans-0TeF40CH3)3. The ability of these compounds to transfer the CH30TeF40 entities has been demonstrated in reactions with ÄSF3, with the formation of As (eis-and trans-0TeF40CH3)3 respectively. All compounds have been characterized by NMR spectroscopy (125Te, 19F> 11B, iH). 
  Reference    Z. Naturforsch. 38b, 332—334 (1983); eingegangen am 25. November 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0332 
 Volume    38 
62Author    Rainer Mattes, Franz WaldmannRequires cookie*
 Title    Molekülstruktureii, Schwingungsspektren und Konformation der Thiooxalsäurederivate CH3S-CO-CONH2, CH3S-CS-CONH2, C2H50-C0-CSNH2 und K[OSC-CONH2] Molecular Structure, Vibrational Spectra and Conformation of the Thiooxalic Acid Derivatives CH3S-CO-CONH2, CH3S-CS-CONH2, C2H50-C0-CSNH2 and K[OSC-CONH2]  
 Abstract    The crystal structures ofCH3S-CO-CONH2 (1), CH3S-CS-CONH2 (2), C2H50-C0-CSNH2 (3) and K[OSC-CONH2] (4) have been determined by single crystal X-ray diffraction. The molecules 1, 2 and 3 are nearly planar and form centrosymmetric dimers by N H • • • O or N-H--S hydrogen bonds with the amidic oxygen or sulfur atom as acceptor atoms. The anion of 4 is not quite planar. The torsional angle around the C-C bond is 18.4°. The con-formations of the title compounds are E, Z' (1 and 2), Z, Z' (3) and Z (4). According to the vibrational spectra, which are discussed briefly, 1 and 3 retain their conformation also in solution. 
  Reference    Z. Naturforsch. 38b, 335—340 (1983); eingegangen am 5. November 1982 
  Published    1983 
  Keywords    Molecular Structure, Conformation, Vibrational Spectra, Thiooxalic Acid Derivatives 
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 Identifier    ZNB-1983-38b-0335 
 Volume    38 
63Author    Annegret LipkaRequires cookie*
 Title    Darstellung und Kristallstruktur des 2:3-Adduktes von Antimontrichlorid und 4-Phenylpyridin, 2 SbCl3 * 3 (CnH9N) Preparation and Crystal Structure of the 2:3 Adduct of Antimony Trichloride and 4-Phenylpyridine, 2SbCl3 * 3(CnH9N)  
 Abstract    A congruently melting phase of molar ratio 2:3 was identified in the system SbCl3/4-phenylpyridine. The structure consists of two different types of complex units: One SbCl3 molecule is bonded to one 4-phenylpyridine ligand only, whereas the other one forms a complex with two 4-phenylpyridine ligands. The SbCl3 unit in the 1:1 species is pyrami-dally shaped, whereas the SbCl3 unit in the 1:2 species displays a T-shaped geometry. The mean angle between the phenyl and pyridyl planes is 33.3°; mean bond lengths are <Sb-Cl> = 247.6 pm and <Sb-N> = 241.7 pm. 
  Reference    Z. Naturforsch. 38b, 341—346 (1983); eingegangen am 27. September 1982 
  Published    1983 
  Keywords    Antimony Trichloride, Crystal Structure, Stereochemistry 
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 Identifier    ZNB-1983-38b-0341 
 Volume    38 
64Author    HerbertW. Roesky, Pierre Schäfer, Mathias Noltemeyer, GeorgeM. SheldrickRequires cookie*
 Title    Zur Darstellung und Struktur des 1.3-Dichloro-5-N.N-dimethylamino-1.3-dithia-2.4.6-triazins Synthesis and Structure of l,3-Dichloro-5-N,N-dimethylamino-l,3-dithia-2,4,6-triazine  
 Abstract    The six membered ring of composition (CH3)2NCN3S2Cl2 8 a was prepared from N,N-dimethylguanidinhydrochloride and trithiadiazindichloride. 3 a was characterized on the basis of mass, 1 H, 13 C NMR spectra and X-ray structure analysis. Crystals of 3 a are monoclinic, space group P2i/c, with a — 660.3(6), b = 834.5(7), c = 1774.7(15) pm, ß = 112.83(6)° and Z = 4. The C2N unit lies approximately in the plane of the [-CNSNSN-] ring, with both Cl atoms on the same side of the ring. 
  Reference    Z. Naturforsch. 38b, 347—349 (1983); eingegangen am 16. September 1982 
  Published    1983 
  Keywords    Six Membered Ring, Carbon, Sulfur, Nitrogen, X-Ray Structure 
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 Identifier    ZNB-1983-38b-0347 
 Volume    38 
65Author    S. P. Perlepes, ThF. Zafiropoulos, A. G. Galinos, J. M. TsangarisRequires cookie*
 Title    Deprotonated Complexes of Bis(o-aminobenzenesulfonyl)ethylenediamine with Mn(II), Co(II), Ni(II) and Cu(II)  
 Abstract    The new complexes K2[ML2] (M = Mn, Cu), K2[ML2(H20)2] (M = Co, Ni), K2[Cu2L2(OH)2] and K2[Cu2L2(0H)2(H20)4], where LH2 = Bis(o-aminobenzenesulfonyl)ethylenediamine, have been prepared. Properties, X-ray powder patterns, molar conductance measurements, magnetic moments and spectral (IR, diffuse reflectance, visible in solution) data are discussed in terms of possible structural types and the nature of the bonding. Distorted octahedral geometries are proposed for the Mn(II), Co(II), Ni(II) and dimeric Cu(II) chelates in the solid state, while K2[CuL2] appears to have a distorted tetrahedral structure. The Mn(II) complex exhibits evidence of a polymeric configuration. The L 2 ~ anion acts as a bidentate N2 or tetradentate N4 ligand. 
  Reference    Z. Naturforsch. 38b, 350—356 (1983); received October 14 1982 
  Published    1983 
  Keywords    Bis(o-aminobenzenesulfonyl)ethylenediamine, Orthanilamide Complexes, Secondary Acid Sulfonylamide Groups, Copper(II), Subnormal Magnetic Moments 
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 Identifier    ZNB-1983-38b-0350 
 Volume    38 
66Author    DietrichK. Breitinger, Günter Petrikowski, Günter Liehr, Raymond SendelbeckRequires cookie*
 Title    Metallomethane, VI [1] Kristallstruktur von Tetrakis(chloroquecksilber)methan-Dimethylsulfoxid C(HgCl)4 (CH3)2SO Metallomethanes, VI [1] Crystal Structure of Tetrakis(chloromercuri)methane-Dimethylsulfoxide C(HgCl)4 * (CH3)2SO  
  Reference    Z. Naturforsch. 38b, 357—364 (1983); eingegangen am 9. November 1982 
  Published    1983 
  Keywords    Metallomethanes, Tetrakis(halomercuri )methanes, Tetrakis(chloromercuri) methane -Dimethylsulfoxide, Crystal Structure, Molecular Packing 
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 Identifier    ZNB-1983-38b-0357 
 Volume    38 
67Author    Herbert Trampisch, Wolfgang BeckRequires cookie*
 Title    Diphenylphosphino -a -aminosäurees ter als Liganden in Palladium(II)-und Platin(II)-Komplexen [1] Diphenylphosphino-a-Amino Acid Esters as Ligands in Palladium(II) and Platinum(II) Complexes [1]  
 Abstract    Aminophosphines, Diphenylphosphino-serine and -cysteine Methylester, Palladium(II) and Platinum(II) Complexes cis-Dichlorobis(chlorodiphenylphosphine)palladium-and platinum(II) react with N-alkyl-a-amino acid esters to give the complexes MCl2[Ph2PN(R)C(H)(R')C02Me]2 (M = Pd, Pt; R = CH2Ph, i-C3H7; R' = CH3, CH2Ph). With lysine ester dimeric, bis(chelate) com-plexes Ph2 Ph2 CI2M(;N(CH2)4C(H)(CO2R)N()MCI2 \p/ \p/ 
  Reference    Z. Naturforsch. 38b, 365—369 (1983); eingegangen am 3. November 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0365 
 Volume    38 
68Author    Franz Götzfried, Wolfgang BeckRequires cookie*
 Title    Reaktionen von S-Methylthiireniumsalzen mit nucleophilen Übergangsmetall-Komplexen [1] Reactions of S-Methylthiirenium Salts with Nucleophilic Transition Metal Complexes [1]  
 Abstract    l-Methyl-2,3-di-f-butyl-thiirenium-tetrafluoroborate, Metal Complexes, Nucleophilic Transition l-Methyl-2,3-di-«-butyl-thiirenium-tetrafluoroborate (1) reacts with K + [7r-C5H5(CO)3Mo] and (PPh3)4Pt to give [(7r-C5H5)(CO)2MoSCH3]2 and [(Ph3P)3PtSCH3]+BF4-, respectively. With 1 and (Ph3P)4Pd the phosphonium salt [Ph3PSCH3]+BF4-has been isolated. 
  Reference    Z. Naturforsch. 38b, 370—372 (1983); eingegangen am 8. November 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0370 
 Volume    38 
69Author    Christian Burschka, Eyup Akgün, Ulf PindurRequires cookie*
 Title    Zur Struktur von (Pyrazolinonyl)-(hydroxypyrazolylium)methanperchloraten NMR-, IR-spektroskopische Studien und Kristallstruktur The Structure of (Pyrazohnonyl)-(hydroxypyrazolyhum)methaneperchlorates NMR, IR Spectroscopic Studies and Crystal Structure  
 Abstract    Spectroscopic Studies, Crystal Structure, (Pyrazolinonyl)-(hydroxypyrazolylium)methane Cations The structures of la-Id were investigated by spectroscopic methods and in the case of la in addition by X-ray diffraction, la, vicarious for the compounds 1, is stabilized in solution and in the crystal by an intramolecular hydrogen bond in an eight-membered ring. The IR and NMR spectra show that 1 exhibit a symmetrical structure. In the case of 1 a the molecular structure is affected by unsymmetrical packing and electrostatic effects in the crystal and is therefore approximated best between the forms I and II. 
  Reference    Z. Naturforsch. 38b, 373—377 (1983); eingegangen am 27. September 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0373 
 Volume    38 
70Author    Josef Metz, Georg Pawlowski, Michael HanackRequires cookie*
 Title    Lösliche Phthalocyaninatometalloxane, Dotierung und Leitfähigkeit Soluble Phthalocyaninatometaloxanes, Doping and Conductivity  
 Abstract    The polymeric //-oxo-(tetraalkylphthalocyaninato)-metal IVB derivatives la-d were synthesized by thermal condensation of the monomeric dihydroxo(tetraalkylphthalo-cyaninato)-metal IVB compounds 5 a-d. The high solubility of the metaloxanes la-d enables a homogeneous reaction with the dopant. The electrical conductivities of the undoped and doped compounds are reported. 
  Reference    Z. Naturforsch. 38b, 378—382 (1983); eingegangen am 9. November 1982 
  Published    1983 
  Keywords    Phthalocyanine, Doping, Conductivity, Polymer 
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 Identifier    ZNB-1983-38b-0378 
 Volume    38 
71Author    Franz Dallacker, Wim CoerverRequires cookie*
 Title    Derivate des Benzo  
 Abstract    [1.3]dioxols, 47 [1] Darstellung und Reaktionen des 4.8-Dimethoxy-bis[1.3]dioxolo[4.5]benzo-[1.2-d; 1.2 -f] [1.3]dioxepins Derivatives of 1,3-Benzodioxoles, 47 [1] Preparation and Reactions of 4,8-Dimethoxy-bis[l,3]dioxolo[4,5]benzo-[1,2-d; l',2'-f][l,3]dioxepine Dibenzo[d, f ][ 1,3]dioxepine, 4,8-Dimethoxy-bis[l,3]dioxolo[4,5]benzo[l,2-d; l',2'-f][l,3]dioxepine In 1957 some dibenzo[d,f][l,3]dioxepines were isolated from Cercospora kikuchii. We describe the preparation of 4,8-dimethoxy-bis[l,3]dioxolo[4,5]benzo[l,2-d; l',2'-f][l,3]-dioxepine (3). It shows a high Sß-reactivity. Bromination yields the monobromo-and dibromocompounds 3 a and 3 b. Treatment of 3 with copper(II) nitrate leads to the dinitro-compound 3c. With the same reagent 3a gives 3d. Reduction of 3d with hydrogen and Palladium as catalyst yields the mono-amine 3e under bromine loss. Under the same reduction conditions in acetic anhydride 3d and 3c yields 3f respectively 3g. The carboxylic acid 3i and the aldehyd 3h are prepared by bromine-lithium exchange from 3 a. In the same manner the dibromocompound 3 b is a suitable starting material to obtain the dicarboxylic acid 3k and the dialdehyd 3j. 3j undergoes easily a thiazolium catalysed oin-condensation, yielding the phenanthrenequinone 31. The cyclic anhydride 3 m can be prepared by heating 3 k in acetic anhydride. 
  Reference    Z. Naturforsch. 38b, 383—391 (1983); eingegangen am 31. Juli 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0383 
 Volume    38 
72Author    Franz Dallacker, Bodo Holtmann, Wim CoerverRequires cookie*
 Title    Derivate des 1.3-BenzdioxoIs, 48 [1] Darstellung und Reaktionen von substituierten 1.3-Benzdioxol-4.7-cliinonen Derivatives of 1,3-Benzdioxoles, 48 [1] Preparation and Reactions of l,3-Benzdioxole-4,7-quinones  
  Reference    Z. Naturforsch. 38b, 392—397 (1983); eingegangen am 6. Oktober 1982 
  Published    1983 
  Keywords    l, 3-Benzdioxol-4, 7-chinon, 6, 7-Dimethyl-naphtho[2, 3-d]-l, 3-dioxol-4, 9-chinon, 6-Hydroxy-naphtho[2, 3-d]-l, 3-dioxol-4, 9-chinon 
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 Identifier    ZNB-1983-38b-0392 
 Volume    38 
73Author    Thomas Kappe, Gertraud Korbuly, Erik PongratzRequires cookie*
 Title    Ylide von Heterocyclen, V [1] I-, N-und S-Ylide des 2-Pyrons und 2-Pyridons Ylides of Heterocycles, V [1] I-, N-and S-Ylides of 2-Pvrones and 2-Pyridones  
  Reference    Z. Naturforsch. 38b, 398 (1983) 
  Published    1983 
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 Identifier    ZNB-1983-38b-0398 
 Volume    38 
74Author    Brigitte Eisenmann, Hanna Jordan, Herbert SchäferRequires cookie*
 Title    Preparation and Crystal Structure of Ba6Sn2P6  
 Abstract    The new compound BaeSn2P6 crystallizes in the monoclinic system, space group P2i/c with lattice constants a = 883.7 ± 0.5 pm b = 1268.8 ± 0.8 pm c= 862.3 ± 0.5 pm ß = 114.42 ± 0.10°. The compound is isotypic to KeSn2Te6 and contains the Sn2P6 12_ -anions which are isosteric with the Sn2Te6 6_ -units. 
  Reference    Z. Naturforsch. 38b, 404—406 (1983); eingegangen am 4. November 1982 
  Published    1983 
  Keywords    Bariumhexaphosphidohypodistannate, Zintl Phase, Crystal Structure 
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 Identifier    ZNB-1983-38b-0404_n 
 Volume    38 
75Author    FrankH. Köhler, Norbert HertkornRequires cookie*
 Title    Direkte Lithiierung von  
 Abstract    BicycIo[3,2,l]octa-2.6-dien Direct Lithiation of Bicyclo[3,2,l]octa-2,6-diene Bicyclo[3,2,l]octa-2,6-diene, Metallation Bicyclo[3,2,l]octa-2,6-diene (1) has been lithiated directly with £-butyllithium/TMEDA at low temperature. After quenching with tri-methyltin chloride essentially two stannyl derivatives of 1 were obtained. The stannyl group did not bind to the allylic carbon of 1 as expected but to C-6 and C-7. This has been shown by means of elemental analysis, mass spectroscopy as well as iH, 13 C and U9 Sn NMR spectroscopy. 
  Reference    Z. Naturforsch. 38b, 407—408 (1983); eingegangen am 12. November 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0407_n 
 Volume    38 
76Author    W-CH., =. Allyl, Matthias Moll, Helmut Behrens, Hans-Jürgen Seibold, Peter MerbachRequires cookie*
 Title    Über Darstellung und Eigenschaften von Na[^ 3 -C3H5Fe(NO)(CO)CN] und ^ 3 -C3H5Fe(NO)(CO)CNMe Synthesis and Properties of Na[^3-C3H5Fe(NO)(CO)CN] and *2 3 -C3H5Fe(NO)(CO)CNMe (T? 3 -C3H5 = AUyl)  
 Abstract    The allyl iron complexes r? 3 -C3H5Fe(NO)(CO)L (L = CN", CNMe) can be obtained by the reaction of rj 3 -C3H5Fe(NO)(CO)2 with NaN(SiMe3)2 and subsequent methylation. 
  Reference    Z. Naturforsch. 38b, 409—410 (1983); eingegangen am 23. Dezember 1982 
  Published    1983 
  Keywords    Allyl Nitrosyl Carbonyl, Cyano, Isonitrile Iron Complexes 
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 Identifier    ZNB-1983-38b-0409 
 Volume    38 
77Author    Matthias Moll, Helmut Behrens, Karl-Heinz Trümmer, Peter MerbachRequires cookie*
 Title    Über neue Cyano-nitrosylmanganate und Isonitril-nitrosyl-Komplexe des Mangans On New Cyano Nitrosyl Manganates and Isonitrile Nitrosyl Complexes of Manganese  
 Abstract    The anionic cyano nitrosyl manganates [Mn(NO)(CO)3CN] _ and [Mn(NO)3CN]~ are formed by the reactions of Mn(NO)(CO)4 andMn(NO)3CO with NaN(SiMe3)2. The alkyla-tion of these anions with [R30]BF4 (R = Me, Et) leads to the corresponding isonitrile complexes Mn(NO)(CO)3CNR and Mn(NO)3CNR. IR, mass and 13 C NMR spectra indicate trigonal-bipyramidal coordination for nitrosyl tricarbonyl derivatives, with three CO ligands in facial positions and NO in the equatorial plane. Based on the temperature de-pendent 13 C NMR spectra of Mn(NO)(CO)3CNR and Mn(NO)(CO)4 the fluctional behaviour of these compounds could be demonstrated with /1G+ values of 48 kJ/mol or less for the CO exchange. 
  Reference    Z. Naturforsch. 38b, 411—416 (1983); eingegangen am 23. Dezember 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0411 
 Volume    38 
78Author    Ekkehard Lindner, Hartwig Rauleder, Wolfgang HillerRequires cookie*
 Title    Neuartige basische Liganden für die homogenkatalytische Homologisierung von Methanol zu Ethanol, I Synthese basischer, dreizähniger P-N-haltiger Chelatliganden und deren Verhalten gegenüber Carbonylverbindungen von Metallen der VI. Nebengruppe Novel Basic Ligands for the Homogeneous Catalytic Homologation of Methanol to Ethanol, I Synthesis of Basic Tridentate P-N Containing Chelate Ligands and their Behaviour Towards Carbonyl Compounds of Group VI Metals  
 Abstract    Tridentate P-N-Ligands PhP(XC5H4N)2, Chelate Complexes of Cr, Mo, W, Structure of (OC)3W[PhP(NHC5H4N)2], NMR Spectra 
  Reference    Z. Naturforsch. 38b, 417—425 (1983); eingegangen am 16. Dezember 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0417 
 Volume    38 
79Author    Arndt Simon, -A, Karl Peters, Eva-Maria Peters, Harry HahnRequires cookie*
 Title    Verfeinerung der Kristallstruktur von Tripalladium-di-tetrathiophospliat Pd3(PS4)2 Refinement of the Crystal Structure of Tripalladium-di-tetrathiophosphate Pda(PS4)2  
 Abstract    Tetrathiophosphate, X-Ray The structure of the title compound has been determined by X-ray crystallography. The title compound is synthesized from the elements at 600 °C. Its crystal structure, derived from powder data [3] is refined by single crystal diffractometer data. The structure is trigonal (P"3ml, o, = 684.1(1), c = 724.4(1) pm); Pd 2+ cations and PS4 3 -anions form a network with an anti-Claudetite (AS2O3) type structure. The PS4 units are distinctly distorted from ideal tetrahedral symmetry. The Pd atoms have a planar environment of 4 S atoms. 
  Reference    Z. Naturforsch. 38b, 426—427 (1983); eingegangen am 15. Dezember 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0426 
 Volume    38 
80Author    Marianne Baudler, Yusuf Aktalay, Karin Kazmierczak, Josef HahnRequires cookie*
 Title    Beiträge zur Chemie des Phosphors, 125 [1, 2]  
 Abstract    Synthese und Struktur der Triorganyl-nonaphosphane(3) P9(i-Pr)3 und P9(t-Bu)3 Contributions to the Chemistry of Phosphorus, 125 [1, 2] Synthesis and Structure of the Triorganyl-nonaphosphanes(3) P9(i-Pr)3 and Pg(£-Bu)3 Triisopropyl -nonaphosphane (3), Tri -£er£-butyl -nonapliosphane (3), Nonaphosphane (3), 5,8,9-Triorganyl-tetracyclo[4.3.0.0 2 > 4 .0 3 ' 7 ]nonaphosphanes, Polycyclic Phosphanes 
  Reference    Z. Naturforsch. 38b, 428—433 (1983); eingegangen am 16. Dezember 1982 
  Published    1983 
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 Identifier    ZNB-1983-38b-0428 
 Volume    38 
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