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Facet section ZfN Section B:Volume 038 [X]
Facet Publication Year 1983 [X]

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61	Author	Boron, Arsenic Methoxotetrafluorotellurates, Vi, Walter Tötsch, Heinrich Aichinger, Fritz Sladky	Requires cookie*
	Title	Bor-und Arsen-methoxotetrafluorotellurate(VI)
	Abstract	Synthesis, Boron and Arsenic Methoxotetrafluorotellurates(VI), NMR Spectra The interaction of eis-and tfrans-HOTeRiOCHs with BG3 yields B(cis-and trans-0TeF40CH3)3. The ability of these compounds to transfer the CH30TeF40 entities has been demonstrated in reactions with ÄSF3, with the formation of As (eis-and trans-0TeF40CH3)3 respectively. All compounds have been characterized by NMR spectroscopy (125Te, 19F> 11B, iH).
	Reference	Z. Naturforsch. 38b, 332—334 (1983); eingegangen am 25. November 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0332
	Volume	38

62	Author	Rainer Mattes, Franz Waldmann	Requires cookie*
	Title	Molekülstruktureii, Schwingungsspektren und Konformation der Thiooxalsäurederivate CH3S-CO-CONH2, CH3S-CS-CONH2, C2H50-C0-CSNH2 und K[OSC-CONH2] Molecular Structure, Vibrational Spectra and Conformation of the Thiooxalic Acid Derivatives CH3S-CO-CONH2, CH3S-CS-CONH2, C2H50-C0-CSNH2 and K[OSC-CONH2]
	Abstract	The crystal structures ofCH3S-CO-CONH2 (1), CH3S-CS-CONH2 (2), C2H50-C0-CSNH2 (3) and K[OSC-CONH2] (4) have been determined by single crystal X-ray diffraction. The molecules 1, 2 and 3 are nearly planar and form centrosymmetric dimers by N H • • • O or N-H--S hydrogen bonds with the amidic oxygen or sulfur atom as acceptor atoms. The anion of 4 is not quite planar. The torsional angle around the C-C bond is 18.4°. The con-formations of the title compounds are E, Z' (1 and 2), Z, Z' (3) and Z (4). According to the vibrational spectra, which are discussed briefly, 1 and 3 retain their conformation also in solution.
	Reference	Z. Naturforsch. 38b, 335—340 (1983); eingegangen am 5. November 1982
	Published	1983
	Keywords	Molecular Structure, Conformation, Vibrational Spectra, Thiooxalic Acid Derivatives
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	TEI-XML for	default:Reihe_B/38/ZNB-1983-38b-0335.pdf
	Identifier	ZNB-1983-38b-0335
	Volume	38

63	Author	Annegret Lipka	Requires cookie*
	Title	Darstellung und Kristallstruktur des 2:3-Adduktes von Antimontrichlorid und 4-Phenylpyridin, 2 SbCl3 * 3 (CnH9N) Preparation and Crystal Structure of the 2:3 Adduct of Antimony Trichloride and 4-Phenylpyridine, 2SbCl3 * 3(CnH9N)
	Abstract	A congruently melting phase of molar ratio 2:3 was identified in the system SbCl3/4-phenylpyridine. The structure consists of two different types of complex units: One SbCl3 molecule is bonded to one 4-phenylpyridine ligand only, whereas the other one forms a complex with two 4-phenylpyridine ligands. The SbCl3 unit in the 1:1 species is pyrami-dally shaped, whereas the SbCl3 unit in the 1:2 species displays a T-shaped geometry. The mean angle between the phenyl and pyridyl planes is 33.3°; mean bond lengths are <Sb-Cl> = 247.6 pm and <Sb-N> = 241.7 pm.
	Reference	Z. Naturforsch. 38b, 341—346 (1983); eingegangen am 27. September 1982
	Published	1983
	Keywords	Antimony Trichloride, Crystal Structure, Stereochemistry
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	Identifier	ZNB-1983-38b-0341
	Volume	38

64	Author	HerbertW. Roesky, Pierre Schäfer, Mathias Noltemeyer, GeorgeM. Sheldrick	Requires cookie*
	Title	Zur Darstellung und Struktur des 1.3-Dichloro-5-N.N-dimethylamino-1.3-dithia-2.4.6-triazins Synthesis and Structure of l,3-Dichloro-5-N,N-dimethylamino-l,3-dithia-2,4,6-triazine
	Abstract	The six membered ring of composition (CH3)2NCN3S2Cl2 8 a was prepared from N,N-dimethylguanidinhydrochloride and trithiadiazindichloride. 3 a was characterized on the basis of mass, 1 H, 13 C NMR spectra and X-ray structure analysis. Crystals of 3 a are monoclinic, space group P2i/c, with a — 660.3(6), b = 834.5(7), c = 1774.7(15) pm, ß = 112.83(6)° and Z = 4. The C2N unit lies approximately in the plane of the [-CNSNSN-] ring, with both Cl atoms on the same side of the ring.
	Reference	Z. Naturforsch. 38b, 347—349 (1983); eingegangen am 16. September 1982
	Published	1983
	Keywords	Six Membered Ring, Carbon, Sulfur, Nitrogen, X-Ray Structure
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	Identifier	ZNB-1983-38b-0347
	Volume	38

65	Author	S. P. Perlepes, ThF. Zafiropoulos, A. G. Galinos, J. M. Tsangaris	Requires cookie*
	Title	Deprotonated Complexes of Bis(o-aminobenzenesulfonyl)ethylenediamine with Mn(II), Co(II), Ni(II) and Cu(II)
	Abstract	The new complexes K2[ML2] (M = Mn, Cu), K2[ML2(H20)2] (M = Co, Ni), K2[Cu2L2(OH)2] and K2[Cu2L2(0H)2(H20)4], where LH2 = Bis(o-aminobenzenesulfonyl)ethylenediamine, have been prepared. Properties, X-ray powder patterns, molar conductance measurements, magnetic moments and spectral (IR, diffuse reflectance, visible in solution) data are discussed in terms of possible structural types and the nature of the bonding. Distorted octahedral geometries are proposed for the Mn(II), Co(II), Ni(II) and dimeric Cu(II) chelates in the solid state, while K2[CuL2] appears to have a distorted tetrahedral structure. The Mn(II) complex exhibits evidence of a polymeric configuration. The L 2 ~ anion acts as a bidentate N2 or tetradentate N4 ligand.
	Reference	Z. Naturforsch. 38b, 350—356 (1983); received October 14 1982
	Published	1983
	Keywords	Bis(o-aminobenzenesulfonyl)ethylenediamine, Orthanilamide Complexes, Secondary Acid Sulfonylamide Groups, Copper(II), Subnormal Magnetic Moments
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	Identifier	ZNB-1983-38b-0350
	Volume	38

66	Author	DietrichK. Breitinger, Günter Petrikowski, Günter Liehr, Raymond Sendelbeck	Requires cookie*
	Title	Metallomethane, VI [1] Kristallstruktur von Tetrakis(chloroquecksilber)methan-Dimethylsulfoxid C(HgCl)4 (CH3)2SO Metallomethanes, VI [1] Crystal Structure of Tetrakis(chloromercuri)methane-Dimethylsulfoxide C(HgCl)4 * (CH3)2SO
	Reference	Z. Naturforsch. 38b, 357—364 (1983); eingegangen am 9. November 1982
	Published	1983
	Keywords	Metallomethanes, Tetrakis(halomercuri )methanes, Tetrakis(chloromercuri) methane -Dimethylsulfoxide, Crystal Structure, Molecular Packing
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	Identifier	ZNB-1983-38b-0357
	Volume	38

67	Author	Herbert Trampisch, Wolfgang Beck	Requires cookie*
	Title	Diphenylphosphino -a -aminosäurees ter als Liganden in Palladium(II)-und Platin(II)-Komplexen [1] Diphenylphosphino-a-Amino Acid Esters as Ligands in Palladium(II) and Platinum(II) Complexes [1]
	Abstract	Aminophosphines, Diphenylphosphino-serine and -cysteine Methylester, Palladium(II) and Platinum(II) Complexes cis-Dichlorobis(chlorodiphenylphosphine)palladium-and platinum(II) react with N-alkyl-a-amino acid esters to give the complexes MCl2[Ph2PN(R)C(H)(R')C02Me]2 (M = Pd, Pt; R = CH2Ph, i-C3H7; R' = CH3, CH2Ph). With lysine ester dimeric, bis(chelate) com-plexes Ph2 Ph2 CI2M(;N(CH2)4C(H)(CO2R)N()MCI2 \p/ \p/
	Reference	Z. Naturforsch. 38b, 365—369 (1983); eingegangen am 3. November 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0365
	Volume	38

68	Author	Franz Götzfried, Wolfgang Beck	Requires cookie*
	Title	Reaktionen von S-Methylthiireniumsalzen mit nucleophilen Übergangsmetall-Komplexen [1] Reactions of S-Methylthiirenium Salts with Nucleophilic Transition Metal Complexes [1]
	Abstract	l-Methyl-2,3-di-f-butyl-thiirenium-tetrafluoroborate, Metal Complexes, Nucleophilic Transition l-Methyl-2,3-di-«-butyl-thiirenium-tetrafluoroborate (1) reacts with K + [7r-C5H5(CO)3Mo] and (PPh3)4Pt to give [(7r-C5H5)(CO)2MoSCH3]2 and [(Ph3P)3PtSCH3]+BF4-, respectively. With 1 and (Ph3P)4Pd the phosphonium salt [Ph3PSCH3]+BF4-has been isolated.
	Reference	Z. Naturforsch. 38b, 370—372 (1983); eingegangen am 8. November 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0370
	Volume	38

69	Author	Christian Burschka, Eyup Akgün, Ulf Pindur	Requires cookie*
	Title	Zur Struktur von (Pyrazolinonyl)-(hydroxypyrazolylium)methanperchloraten NMR-, IR-spektroskopische Studien und Kristallstruktur The Structure of (Pyrazohnonyl)-(hydroxypyrazolyhum)methaneperchlorates NMR, IR Spectroscopic Studies and Crystal Structure
	Abstract	Spectroscopic Studies, Crystal Structure, (Pyrazolinonyl)-(hydroxypyrazolylium)methane Cations The structures of la-Id were investigated by spectroscopic methods and in the case of la in addition by X-ray diffraction, la, vicarious for the compounds 1, is stabilized in solution and in the crystal by an intramolecular hydrogen bond in an eight-membered ring. The IR and NMR spectra show that 1 exhibit a symmetrical structure. In the case of 1 a the molecular structure is affected by unsymmetrical packing and electrostatic effects in the crystal and is therefore approximated best between the forms I and II.
	Reference	Z. Naturforsch. 38b, 373—377 (1983); eingegangen am 27. September 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0373
	Volume	38

70	Author	Josef Metz, Georg Pawlowski, Michael Hanack	Requires cookie*
	Title	Lösliche Phthalocyaninatometalloxane, Dotierung und Leitfähigkeit Soluble Phthalocyaninatometaloxanes, Doping and Conductivity
	Abstract	The polymeric //-oxo-(tetraalkylphthalocyaninato)-metal IVB derivatives la-d were synthesized by thermal condensation of the monomeric dihydroxo(tetraalkylphthalo-cyaninato)-metal IVB compounds 5 a-d. The high solubility of the metaloxanes la-d enables a homogeneous reaction with the dopant. The electrical conductivities of the undoped and doped compounds are reported.
	Reference	Z. Naturforsch. 38b, 378—382 (1983); eingegangen am 9. November 1982
	Published	1983
	Keywords	Phthalocyanine, Doping, Conductivity, Polymer
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	Identifier	ZNB-1983-38b-0378
	Volume	38

71	Author	Franz Dallacker, Wim Coerver	Requires cookie*
	Title	Derivate des Benzo
	Abstract	[1.3]dioxols, 47 [1] Darstellung und Reaktionen des 4.8-Dimethoxy-bis[1.3]dioxolo[4.5]benzo-[1.2-d; 1.2 -f] [1.3]dioxepins Derivatives of 1,3-Benzodioxoles, 47 [1] Preparation and Reactions of 4,8-Dimethoxy-bis[l,3]dioxolo[4,5]benzo-[1,2-d; l',2'-f][l,3]dioxepine Dibenzo[d, f ][ 1,3]dioxepine, 4,8-Dimethoxy-bis[l,3]dioxolo[4,5]benzo[l,2-d; l',2'-f][l,3]dioxepine In 1957 some dibenzo[d,f][l,3]dioxepines were isolated from Cercospora kikuchii. We describe the preparation of 4,8-dimethoxy-bis[l,3]dioxolo[4,5]benzo[l,2-d; l',2'-f][l,3]-dioxepine (3). It shows a high Sß-reactivity. Bromination yields the monobromo-and dibromocompounds 3 a and 3 b. Treatment of 3 with copper(II) nitrate leads to the dinitro-compound 3c. With the same reagent 3a gives 3d. Reduction of 3d with hydrogen and Palladium as catalyst yields the mono-amine 3e under bromine loss. Under the same reduction conditions in acetic anhydride 3d and 3c yields 3f respectively 3g. The carboxylic acid 3i and the aldehyd 3h are prepared by bromine-lithium exchange from 3 a. In the same manner the dibromocompound 3 b is a suitable starting material to obtain the dicarboxylic acid 3k and the dialdehyd 3j. 3j undergoes easily a thiazolium catalysed oin-condensation, yielding the phenanthrenequinone 31. The cyclic anhydride 3 m can be prepared by heating 3 k in acetic anhydride.
	Reference	Z. Naturforsch. 38b, 383—391 (1983); eingegangen am 31. Juli 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0383
	Volume	38

72	Author	Franz Dallacker, Bodo Holtmann, Wim Coerver	Requires cookie*
	Title	Derivate des 1.3-BenzdioxoIs, 48 [1] Darstellung und Reaktionen von substituierten 1.3-Benzdioxol-4.7-cliinonen Derivatives of 1,3-Benzdioxoles, 48 [1] Preparation and Reactions of l,3-Benzdioxole-4,7-quinones
	Reference	Z. Naturforsch. 38b, 392—397 (1983); eingegangen am 6. Oktober 1982
	Published	1983
	Keywords	l, 3-Benzdioxol-4, 7-chinon, 6, 7-Dimethyl-naphtho[2, 3-d]-l, 3-dioxol-4, 9-chinon, 6-Hydroxy-naphtho[2, 3-d]-l, 3-dioxol-4, 9-chinon
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	Identifier	ZNB-1983-38b-0392
	Volume	38

73	Author	Thomas Kappe, Gertraud Korbuly, Erik Pongratz	Requires cookie*
	Title	Ylide von Heterocyclen, V [1] I-, N-und S-Ylide des 2-Pyrons und 2-Pyridons Ylides of Heterocycles, V [1] I-, N-and S-Ylides of 2-Pvrones and 2-Pyridones
	Reference	Z. Naturforsch. 38b, 398 (1983)
	Published	1983
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	Identifier	ZNB-1983-38b-0398
	Volume	38

74	Author	Brigitte Eisenmann, Hanna Jordan, Herbert Schäfer	Requires cookie*
	Title	Preparation and Crystal Structure of Ba6Sn2P6
	Abstract	The new compound BaeSn2P6 crystallizes in the monoclinic system, space group P2i/c with lattice constants a = 883.7 ± 0.5 pm b = 1268.8 ± 0.8 pm c= 862.3 ± 0.5 pm ß = 114.42 ± 0.10°. The compound is isotypic to KeSn2Te6 and contains the Sn2P6 12_ -anions which are isosteric with the Sn2Te6 6_ -units.
	Reference	Z. Naturforsch. 38b, 404—406 (1983); eingegangen am 4. November 1982
	Published	1983
	Keywords	Bariumhexaphosphidohypodistannate, Zintl Phase, Crystal Structure
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	Identifier	ZNB-1983-38b-0404_n
	Volume	38

75	Author	FrankH. Köhler, Norbert Hertkorn	Requires cookie*
	Title	Direkte Lithiierung von
	Abstract	BicycIo[3,2,l]octa-2.6-dien Direct Lithiation of Bicyclo[3,2,l]octa-2,6-diene Bicyclo[3,2,l]octa-2,6-diene, Metallation Bicyclo[3,2,l]octa-2,6-diene (1) has been lithiated directly with £-butyllithium/TMEDA at low temperature. After quenching with tri-methyltin chloride essentially two stannyl derivatives of 1 were obtained. The stannyl group did not bind to the allylic carbon of 1 as expected but to C-6 and C-7. This has been shown by means of elemental analysis, mass spectroscopy as well as iH, 13 C and U9 Sn NMR spectroscopy.
	Reference	Z. Naturforsch. 38b, 407—408 (1983); eingegangen am 12. November 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0407_n
	Volume	38

76	Author	W-CH., =. Allyl, Matthias Moll, Helmut Behrens, Hans-Jürgen Seibold, Peter Merbach	Requires cookie*
	Title	Über Darstellung und Eigenschaften von Na[^ 3 -C3H5Fe(NO)(CO)CN] und ^ 3 -C3H5Fe(NO)(CO)CNMe Synthesis and Properties of Na[^3-C3H5Fe(NO)(CO)CN] and *2 3 -C3H5Fe(NO)(CO)CNMe (T? 3 -C3H5 = AUyl)
	Abstract	The allyl iron complexes r? 3 -C3H5Fe(NO)(CO)L (L = CN", CNMe) can be obtained by the reaction of rj 3 -C3H5Fe(NO)(CO)2 with NaN(SiMe3)2 and subsequent methylation.
	Reference	Z. Naturforsch. 38b, 409—410 (1983); eingegangen am 23. Dezember 1982
	Published	1983
	Keywords	Allyl Nitrosyl Carbonyl, Cyano, Isonitrile Iron Complexes
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	Identifier	ZNB-1983-38b-0409
	Volume	38

77	Author	Matthias Moll, Helmut Behrens, Karl-Heinz Trümmer, Peter Merbach	Requires cookie*
	Title	Über neue Cyano-nitrosylmanganate und Isonitril-nitrosyl-Komplexe des Mangans On New Cyano Nitrosyl Manganates and Isonitrile Nitrosyl Complexes of Manganese
	Abstract	The anionic cyano nitrosyl manganates [Mn(NO)(CO)3CN] _ and [Mn(NO)3CN]~ are formed by the reactions of Mn(NO)(CO)4 andMn(NO)3CO with NaN(SiMe3)2. The alkyla-tion of these anions with [R30]BF4 (R = Me, Et) leads to the corresponding isonitrile complexes Mn(NO)(CO)3CNR and Mn(NO)3CNR. IR, mass and 13 C NMR spectra indicate trigonal-bipyramidal coordination for nitrosyl tricarbonyl derivatives, with three CO ligands in facial positions and NO in the equatorial plane. Based on the temperature de-pendent 13 C NMR spectra of Mn(NO)(CO)3CNR and Mn(NO)(CO)4 the fluctional behaviour of these compounds could be demonstrated with /1G+ values of 48 kJ/mol or less for the CO exchange.
	Reference	Z. Naturforsch. 38b, 411—416 (1983); eingegangen am 23. Dezember 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0411
	Volume	38

78	Author	Ekkehard Lindner, Hartwig Rauleder, Wolfgang Hiller	Requires cookie*
	Title	Neuartige basische Liganden für die homogenkatalytische Homologisierung von Methanol zu Ethanol, I Synthese basischer, dreizähniger P-N-haltiger Chelatliganden und deren Verhalten gegenüber Carbonylverbindungen von Metallen der VI. Nebengruppe Novel Basic Ligands for the Homogeneous Catalytic Homologation of Methanol to Ethanol, I Synthesis of Basic Tridentate P-N Containing Chelate Ligands and their Behaviour Towards Carbonyl Compounds of Group VI Metals
	Abstract	Tridentate P-N-Ligands PhP(XC5H4N)2, Chelate Complexes of Cr, Mo, W, Structure of (OC)3W[PhP(NHC5H4N)2], NMR Spectra
	Reference	Z. Naturforsch. 38b, 417—425 (1983); eingegangen am 16. Dezember 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0417
	Volume	38

79	Author	Arndt Simon, -A, Karl Peters, Eva-Maria Peters, Harry Hahn	Requires cookie*
	Title	Verfeinerung der Kristallstruktur von Tripalladium-di-tetrathiophospliat Pd3(PS4)2 Refinement of the Crystal Structure of Tripalladium-di-tetrathiophosphate Pda(PS4)2
	Abstract	Tetrathiophosphate, X-Ray The structure of the title compound has been determined by X-ray crystallography. The title compound is synthesized from the elements at 600 °C. Its crystal structure, derived from powder data [3] is refined by single crystal diffractometer data. The structure is trigonal (P"3ml, o, = 684.1(1), c = 724.4(1) pm); Pd 2+ cations and PS4 3 -anions form a network with an anti-Claudetite (AS2O3) type structure. The PS4 units are distinctly distorted from ideal tetrahedral symmetry. The Pd atoms have a planar environment of 4 S atoms.
	Reference	Z. Naturforsch. 38b, 426—427 (1983); eingegangen am 15. Dezember 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0426
	Volume	38

80	Author	Marianne Baudler, Yusuf Aktalay, Karin Kazmierczak, Josef Hahn	Requires cookie*
	Title	Beiträge zur Chemie des Phosphors, 125 [1, 2]
	Abstract	Synthese und Struktur der Triorganyl-nonaphosphane(3) P9(i-Pr)3 und P9(t-Bu)3 Contributions to the Chemistry of Phosphorus, 125 [1, 2] Synthesis and Structure of the Triorganyl-nonaphosphanes(3) P9(i-Pr)3 and Pg(£-Bu)3 Triisopropyl -nonaphosphane (3), Tri -£er£-butyl -nonapliosphane (3), Nonaphosphane (3), 5,8,9-Triorganyl-tetracyclo[4.3.0.0 2 > 4 .0 3 ' 7 ]nonaphosphanes, Polycyclic Phosphanes
	Reference	Z. Naturforsch. 38b, 428—433 (1983); eingegangen am 16. Dezember 1982
	Published	1983
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	Identifier	ZNB-1983-38b-0428
	Volume	38

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