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1989 (280)
1Author    Edmund Hartmann, Joachim SträhleRequires cookie*
 Title    Synthese und Kristallstruktur von tetramerem N,N'-Diphenylform am idinato-gold(I), [A u(PhN C H N Ph)]4 Synthesis and Structure of Tetrameric N,N'-Diphenylformamidinato Gold(I), [Au(PhNCHNPh) ] 4  
 Abstract    N .N '-D iphenylform am idinato G old(I). Synthesis, Crystal Structure N .N '-D iphenylform am idinato gold(I) (1) is obtained from N a(PhNCH NPh) and A ul in liquid amm onia. It can be recrystallized from toluene/rc-heptane to form colorless monoclinic crystals, the space group C 2/c, with the lattice C o n sta n tsa = 1781.7(7), b = 1159.0(5), c = 2518.7(8) pm./3 = 99.06(3)°. 1 is tetram eric in solution and in the solid state. In the tetram eric complex with the symmetry C2 the four Au atoms form a planar rhom bus with Au —Au distances between 295,7 and 322.7 pm. The am idinato ligands are arranged alternatively above and below the A u4-rhombus and function as bridging ligands for neighbouring A u atom s, which thereby reach a linear coordi­ nation with distances A u —N betw een 200.0 and 202. 
  Reference    (Z. Naturforsch. 44b, 1 [1989]; eingegangen am 4. O ktober 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0001 
 Volume    44 
2Author    Michel Mégnamisi-BélombéRequires cookie*
 Title    Synthesis and Crystal and Molecular Structure o f fratts-Dichloro(ethanedial dioxim ato(l—)-N,N ')(ethanedial dioxime-N,N')rhodium(III)  
 Abstract    /raAjs-Dichloro(ethanedial dioximato(1 —)-N ,N ')(ethanedial dioxim e-N ,N ')rhodium (III), X -Ray, Crystal Structure rrans-D ichloro(ethanedial-dioxim ato)(ethanediaI-dioxim e)rhodium (III), R hCl:(G H)(G H 2), has been synthesized and its structure determ ined by single crystal X-ray diffraction at room tem perature. C4H 7Cl2N4 0 4Rh. Mr = 348.94. monoclinic space group P 2 ,/a; a = 10.543(3). b = 8.363(2), c = 11.512(3)Ä ; ß = 92.79(2)°; V = 1024Ä3; Z = 4; Dc = 2.26 Mg m 3. Final Rw = 0.075 for 2035 reflections and 139 param eters. The coordination geometry around Rh is a dis­ torted (4+ 2) octahedron, with four chelating N atoms lying in the equatorial plane and the two Cl atom s in the apical positions. The H atoms of the oxime groups are involved in relatively weak /Tiframolecular O —H —O bridgings, as well as in very strong /m m nolecular bridgings which extend throughout the crystal structure and propagate nearly parallel to the [101] crystallographic direc­ tion. 
  Reference    (Z. Naturforsch. 44b, 5 [1989]; received July 15 1988) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0005.pdf 
 Identifier    ZNB-1989-44b-0005 
 Volume    44 
3Author    Requires cookie*
 Title    D ie Struktur von [(terf-C4H9)3 PI][W (C O )4l 3 ] — ein Beitrag zur Diskussion des Akzeptorverhaltens von Iodphosphoniumionen  
  Reference    (Z. Naturforsch. 44b, 9 [1989]) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0009.pdf 
 Identifier    ZNB-1989-44b-0009 
 Volume    44 
4Author    H.-W Jochims, E. Rühl, H. BaumgärtelRequires cookie*
 Title    Zur Photoionisation und Ionenfragmentation von SF4 Photoionization and Ion Fragmentation of SF4  
 Abstract    The ionization potentials of sulfurtetrafluoride have been measured using threshold photoelec­ tron spectroscopy and com pared with theoretical calculations. The decay of SF4+ has been studied by photoionization mass spectrom etry and photoion-photoelectron coincidence. The break-down graphs reveal competing decay processes. Bond dissociation energies in SF4+ have been calcu­ lated. 
  Reference    (Z. Naturforsch. 44b, 13—1 [1989]; eingegangen am 29. August 1988) 
  Published    1989 
  Keywords    T hreshold Photoelectron Spectra, A bsorption Spectra, Photoionization Mass Spectra, Break Down G raphs, Bond Energy 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0013.pdf 
 Identifier    ZNB-1989-44b-0013 
 Volume    44 
5Author    G. Hagenow3, H.-W Jochims3, J. Sawatzkib, R. Minkwitzb, H. Baumgärtel3Requires cookie*
 Title    Photoionisationsmassenspektren von MethyI(trifluormethyl)sulfan CH3SCF3 [1] Photoionization Mass Spectra of Methyl(trifluoromethyl)sulfan CH 3SCF3 [1]  
 Abstract    The ionization potential of C H 3SCF3 and the appearance potentials of fragm ent ions have been m easured in the photon energy range 9 —19 eV using synchrotron, radiation. From these results thermochem ical data of C H 3SCF3, C H 3SCF3+ and fragment ions have been evaluated. 
  Reference    (Z. Naturforsch. 44b, 17 [1989]; eingegangen am 29. A ugust 1988) 
  Published    1989 
  Keywords    Sulfane, H eat of Form ation, Photoionization, Bond Energy, Mass Spectra 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0017.pdf 
 Identifier    ZNB-1989-44b-0017 
 Volume    44 
6Author    H. Baumgärtel, H.-W Jochims, E. Rühl, O. Lösking, H. WillnerRequires cookie*
 Title    Photoionenspektroskopie an Schwefelchloridpentafluorid SF5CI, das Ionisationspotential von Schwefelpentafluorid SF5 Photoion Spectroscopy of Sulfurchloridepentafluoride SF5CI, the Ionization Potential of Sulfurpentafluoride SF5  
 Abstract    The appearance potentials of fragment ions from SF5C1 have been m easured in the energy range 12 — 20 eV by means of photoionization mass spectrometry. From these data, the ionization potential of SFs comes to 9.65 eV. 
  Reference    (Z. Naturforsch. 44b, 21 [1989]; eingegangen am 31. August 1988) 
  Published    1989 
  Keywords    Ionization Potential, Sulfurhalogenides, H eat of Form ation, Photoionization Mass Spectra 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0021.pdf 
 Identifier    ZNB-1989-44b-0021 
 Volume    44 
7Author    Hans-Ulrich Hummel, Uwe KornRequires cookie*
 Title    Dithiocarbimates from Sulfonamides, Part 1: Preparation and X-Ray Crystal Structures of K2[S2C = N —S 0 2—C6H5] *2 H 20 and K2[S2C = N -S 0 2-C 6H4-C 1] * 2 h 2o  
 Abstract    D ithiocarbim ates. Sulfonamides, X-Ray. Sulfones By reaction of the sulfonamides C6H 5 —SO; —NH : and p-C\ — C,,H4—SO: — N H : with CS2 in the presence of bases the corresponding dithiocarbim ates have been obtained in form of their potas­ sium salts and characterized by means of X-ray structural analysis. Both com pounds crystallize in the space group P2,/a with a = 29.778(3), b — 6.202(1). c = 7.169(1) A and ß = 90.33(2)° for K2[S2C = N -S 0 2-C 6H 5]-2 H 20 and a = 31.517(3). b = 7.189(1), c -6.196(1) Ä and ß = 90.10(1)° for the Cl-substituted species, respectively. A relation between both crystal structures becomes obvious when for K2[S2C = N — SO : —C6H4—C l]-2 H 20 the first space group setting is choosen; i.e. P I 12,/a. The dithiocarbim ates are built up of two planar moieties. One plane contains the S2C = N —SO framework of each anion while a second plane consists of the S —C,,HS group and the S —C6H 4—Cl group, respectively. The two planes are oriented nearly perpendicular to each other and give rise to conjugation involving the S 0 2 groups in the different systems. 
  Reference    (Z. Naturforsch. 44b, 24—28 [1989]; received June 22/Septem ber 27. 1988) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0024.pdf 
 Identifier    ZNB-1989-44b-0024 
 Volume    44 
8Author    Hans-Ulrich Hummel, Uwe KornRequires cookie*
 Title    Dithiocarbimates from Sulfonamides, Part 2: Preparation and X-Ray Crystal Structures o f (PPh4)2[Ni(S2C = N —S 0 2—Ph)2] and (PPh4)2[Ni(S2C = N —S 0 2—C6H4—CI)2] * 2 H20  
 Abstract    Nickel(II). N-Sulfonyldithiocarbim ates, X-Ray By reaction of K2[S2C N S 0 2C6H 5] • 2 H 20 and K2[S2C N S O ,Q H 4Cl] ■ 2 H .O , respectively, with N i(C H ,C O O)2 • 4 H 20 the complex anions [Ni(S2C = N -S Ö 2-C hH 5)2]2 ' and [Ni(S2C = N -S 0 2-C hH 4-C l) 2]2~ are formed and have been isolated in form of their (PPh4) salts. (PPh4)2[Ni(S2C =N —S 0 2—Ph)2] crystallizes monoclinicly. space group P2,/ö with a = 19.081(4), b = 9.106(1), c = 17.630(4) Ä and ß = 113.42(6)° with Z = 2. (PPh4)2[Ni(S2C = N —S 0 2—C(1H 4—C l)2] -2 H 20 crystallizes triclinicly, and the non-standard setting C l has been choosen with a = 15.732(3), b = 22.509(4), c = 9.521(1) Ä, a = 96.30(6), ß = 117.57(9), y = 88.93(5)° and Z = 2. Within the complex anions nickel has the site-symmetry 1 and is coordinated by four sulfur atom s with N i-S mean = 2.198 Ä. The Ni(S2C = N -S O) 2 units are essentially planar in both systems. This planarity gives rise to conjugation effects involving the S 0 2 group and the jr-system of S2C = N — as well as the lone pair on N. 
  Reference    (Z. Naturforsch. 44b, 29 [1989]; received June 22/Septem ber 27 1988) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0029.pdf 
 Identifier    ZNB-1989-44b-0029 
 Volume    44 
9Author    HerbertW. Roesky, Frank Schrumpf, Mathias NoltemeyerRequires cookie*
 Title    N eue Übergangsmetallkomplexe mit dem Liganden M e2S (0 )= N P P h 2= N — New Transition Metal Complexes with the Ligand Me2S (0) = NPPh2=N —  
 Abstract    X -Ray, Titanium , Vanadium, Tantalum S,S-Dimethylsulfoximinato-diphenyl-N-trimethylsilylphosphoranylidenamin (1) reacts in a molar ratio of 1:1 with TiCl4. CpTiCf, (Cp = C5H 5). VOC1, and Cp*TaCl4 (Cp* = C5M e5) to yield the 1:1 adduct l-T iC l4 (2) and the substituted products M e^S(0) = NPPh^ = N —TiCpCl^ (3), M e2S (0) = N PPh2=N —VOCl2 (4) and Me2S (0) = N PPh2 = N -T a C p * C l3 (5). The structures of 3, 4 and 5 show short metal-nitrogen bond lengths. 
  Reference    (Z. Naturforsch. 44b, 35 [1989]; eingegangen am 8. August 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0035 
 Volume    44 
10Author    WilhelmV. Dahlhoff, KaluluM. Taba, Richard MynottRequires cookie*
 Title    Dibenzoylmethane Reaction with Dichlorophenylphosphine: Oxygen Transfer from Carbon to Phosphorus via a Defined C2P 0 3 Phosphorane  
 Abstract    Tricyclic Phosphorane, Rearrangem ent to Phosphinic Acid Ester, 2D NM R Spectra, 13C NM R Spectra Dichlorophenylphosphine reacts with two equivalents of dibenzoylm ethane at —30 °C in the presence of triethylamine to give a tricyclic phosphorane interm ediate 4 which isomerizes to the m ore stable phosphinic acid ester 5 above 30 °C. The structures of 4 and 5 were determ ined by l3C, 'H shift correlated 2D NMR spectroscopy using 
  Reference    (Z. Naturforsch. 44b, 41 [1989]; received August 10 1988) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0041.pdf 
 Identifier    ZNB-1989-44b-0041 
 Volume    44 
11Author    Wolfgang Einholz, Gerhard Frey, Wolfgang HauboldRequires cookie*
 Title    Borylierung von Sulfamiden, Sulfoniminen und Sulfondiiminen Borylation of Sulfamides, Sulfonimines and Sulfonediimines  
 Abstract    The diborylated sulfamide 6a can be obtained from 2-chloro-l ,3-dim ethyl-l .3.2-diazaborolidine and the silylated sulfamide la , whereas (M e2N)2BCl and la yield the dithia-tetrazadiborocine 7b. Similarly, (M e2N)2BCl reacts with a) the sulfonimine 2a, b) the sul-fonediim ine 3a to give a) B (N M e:), and the bis-and tris(sulfonim ino)boranes 10b and 11, b) B (N M e2)3 and the dithiatetrazadiborocine 15b. The diborylated sulfamide 6c (R 2B = Ph:B) cannot be isolated. The synthesis of the m onoborylated sulfonim ines 9c, 9e and sulfonediim ines 13, 14 is described. 
  Reference    (Z. Naturforsch. 44b, 47 [1989]; eingegangen am 13. Septem ber 1988) 
  Published    1989 
  Keywords    Boron-Nitrogen Com pounds, Borylated Sulfam ides, Sulfonim ines, Sulfonediim ines, Synthesis, Spectroscopic Data 
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 Identifier    ZNB-1989-44b-0047 
 Volume    44 
12Author    Bernd Wrackmeyer, Klaus Schamei, Max HerberholdRequires cookie*
 Title    3C-und 1;,N-NMR-spektroskopische Untersuchungen einiger Pentacarbonylchrom-Aminophosphan-Komplexe 13C and '"'N NMR Spectroscopic Study of Some Pentacarbonylchromium-Aminophosphane Complexes  
 Abstract    A m inophosphanes, Pentacarbonylchromium C om plexes, 13C N M R , l5N NM R L,C and !>N NM R data are reported for the free aminophosphanes 'Bu, ,,P(NH :)" (n = 1 (1). 
  Reference    (Z. Naturforsch. 44b, 55 [1989]; eingegangen am 12. Septem ber 1988) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0055.pdf 
 Identifier    ZNB-1989-44b-0055 
 Volume    44 
13Author    Karl Hensen, Michael DräbingRequires cookie*
 Title    Phasendiagramme einiger Methylhalogensilane mit Pyridin und Lutidin Phase Diagrams of Methylhalogenosilanes with Pyridine and Lutidine  
 Abstract    By analyzing the phase diagrams of som e trim ethylhalogenosilane/pyridine-and methyl-trichlorosilane/lutidine-system s the existence of the incongruently m elting addition com pounds M e3SiF-(Pyridine)2, M e3SiCl • (Pyridine)2, M eSiCl, • (2.5-L utidine)2. M eSiC l, • (2.6-L utidine); , (M eSiC l3)2-3.5-Lutidine, and the congruently m elting com pounds M eSiC l, -2.4-L utidine. M eSiC l,-(3.5-L utidine)2 was proven. 
  Reference    (Z. Naturforsch. 44b, 63 [1989]; eingegangen am 6. M ai/29. August 1988) 
  Published    1989 
  Keywords    Phase Diagrams, Addition Com pounds Pyridine, Lutidine, M ethylhalogenosilanes 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0063.pdf 
 Identifier    ZNB-1989-44b-0063 
 Volume    44 
14Author    Walter Maringgele, Anton MellerRequires cookie*
 Title    Reaktionen der Natrium-Komplexe aromatischer Ether mit DichIor(diorganylamino)boranen Reactions of Sodium Complexes of Aromatic Ethers with Dichloro(diorganylamino)boranes  
 Abstract    A m inophenoxyborane, A m inonaphthoxyboranes, Borylethines. Solvate of Sodium naphtholate The reaction o f anisole with Na/K -alloy and subsequent reaction with dichloro(diisopropyl-amino)borane yields diisopropylam ino(diphenoxy)borane (1). In reacting the sodium com plex of 1-or 2-m ethoxynaphthalene, respectively, with dichloro(diorganylam ino)boranes the ether bond is cleaved. O ne obtains the m ethoxy-2-naphthoxy-diorganylam inoboranes (2 a —d) besides the di-2-naphthoxy-diorganylam inoboranes (3a—e), the 2-naphthoxy-bis(diorganylam ino)boranes (4a—b) and the solvated sodium -2-naphtholate (6). By-products are l,2-bis[(diisopropylam ino)-1-or 2-naphthoxyboryl]ethyne derivatives 5a and 5b, terized analytically and spectroscopically (MS; NM R: 
  Reference    (Z. Naturforsch. 44b, 67 [1989]; eingegangen am 3. O ktober 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0067 
 Volume    44 
15Author    G. Kliche, H. G. Von SchneringRequires cookie*
 Title    Schwingungsspektren der Clusterverbindung Nb6F15 Vibrational Spectrum of the Cluster Compound Nb6F15  
 Abstract    Metal Cluster Com pound. Vibrational Spectra. Normal C oordinate A nalysis. Force Constants Infrared and Raman spectra of the metal cluster com pound [NbhF 12]F;, (cubic Im3m; Z = 2) are reported. The three intense m odes observed in the Raman spectrum at 215. 267, and 337 cm 1 and a weak m ode observed in the infrared spectrum at 287 cm 1 are assigned to the T2ä, Ea" A ,ä, and T," vibrational modes of the Nbh octahedra. The assignm ent is supported by normal coordi­ nate analysis and Raman measurem ents at 47 kbar. The valence force constants are f(N b —F') = 2.04. f(N b —F'-") = 1.30 and f(N b -N b) = 0.97 N cm m etal-to-m etal interaction in the cluster. 
  Reference    (Z. Naturforsch. 44b, 74—7 [1989]; eingegangen am 2. Septem ber 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0074 
 Volume    44 
16Author    Werner JahnRequires cookie*
 Title    Synthesis of Water Soluble Tetrairidium Clusters Suitable for Heavy Atom Labelling of Proteins  
 Abstract    The substitution of 4 CO ligands in Ir4(C O)i; by tris-(2-carbethoxyethyl)phosphine and sub­ sequent reaction with ammonia yielded water soluble Ir clusters which when m odified further can be used for heavy atom labelling of proteins. 
  Reference    (Z. Naturforsch. 44b, 79—82 [1989]; received July 6/O ctober 12. 1988 Water Soluble Tetrairidium Cluster) 
  Published    1989 
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 TEI-XML for    default:Reihe_B/44/ZNB-1989-44b-0079.pdf 
 Identifier    ZNB-1989-44b-0079 
 Volume    44 
17Author    L. Hornera, W. Rothb, AdolfRequires cookie*
 Title    Chemie an starren Grenzflächen, 9 [1] Eigenschaften und Verhalten Oniumgruppen-modifizierter Aerosile Einige Beispiele interpartikulärer Reaktionen Chemistry on Rigid Interfaces, 9 [1] Properties and Behaviour of Onium Group Modified Aerosils Some Examples of Interparticular Reactions  
 Abstract    b Dr. Karl Thom ae G m bH . Abt. Biochem ie. Postfach 1755. 7950 Biberach/Riß Migration o f Aerosils, Onium Groups. Interparticular "cross-linking" A erosils with covalently linked onium group 2 a —f catalyze the exchange o f halogene (Finkel-stein-R eaction) and migrate in an electric field depending on the nature o f the end groups and the kind o f the suspension medium. E lectroactive groups covalently linked with aerosil are electroreduced on mercury and lead cathodes. The possibility of an interparticular cross linking is dem onstrated. 
  Reference    (Z. Naturforsch. 44b, 83 [1989]; eingegangen am 10. August 1987/29. April 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0083 
 Volume    44 
18Author    NicholasC. Norman, PeterM. WebsterRequires cookie*
 Title    The Synthesis of Some Cyclopentadienyliron-Indium Complexes  
 Abstract    Treatm ent o f indium trichloride with three equivalents of the cyclopentadienyliron carbonyl anions, [F e(C O)2(?7-C5H 4R)] (R = H, Me) affords the tri-iron indium com plexes [In {F e(C O)2(//-C 5H 4R)},] (R = H. Me) as dark red crystalline materials. Both com pounds were characterized by spectroscopic and analytical methods. Infrared spectroscopy indicates that both com plexes are undissociated in solution in contrast to previously reported analogous m olybdenum containing species. 
  Reference    (Z. Naturforsch. 44b, 91 [1989]; received August 9. 1988) 
  Published    1989 
  Keywords    Synthesis Iron, Indium, Cyclopentadienyl, Carbonyl 
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 Identifier    ZNB-1989-44b-0091 
 Volume    44 
19Author    Herbert Plenio, HerbertW. RoeskyRequires cookie*
 Title    Syntheses of Dicyclopentadienyl-Titanium(IV) Substituted Carbodiimides  
  Reference    (Z. Naturforsch. 44b, 94 [1989]; eingegangen am 29. Juli 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0094_n 
 Volume    44 
20Author    Albrecht Krämer, Hans Pritzkow, Walter SiebertRequires cookie*
 Title    Synthese und Struktur von 2  
 Abstract    4.6.8-Tetrakis(diisopropylam ino)-2.4.6.8-tetrabora-tricycIo-[3.3.0.03,7]-octan Synthesis and Structure of 2.4.6.8-Tetrakis(diisopropylamino)-2.4.6.8-tetrabora-tricyclo-[3.3.0.01 ]-octane 1.2.5.6-T etrakis(diisopropylam ino)-l ,2,5,6-tetra-hyd ro-l,2,5,6-tetraborocine, 2.4.6.8-T etrakis(diisopropylam ino)-2.4,6,8-tetra-bora-tricyclo-[3.3.0.03'7]-octane 
  Reference    (Z. Naturforsch. 44b, 96 [1989]; eingegangen am 23. August 1988) 
  Published    1989 
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 Identifier    ZNB-1989-44b-0096_n 
 Volume    44 
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