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1972 (397)
1Author    E. KönigRequires cookie*
 Title    The Nephelauxetic Effect — Calculation and Accuracy of the Interelectronic Repulsion Parameters II. Application to d 3 and d 7 Single Crystal Spectra at Cryogenic Temperatures  
 Abstract    Expressions are reviewed which may be used to determine 10 Dq and B from the spin-allowed bands in the optical spectra of d 3 and d 7 electron systems within octahedral and tetrahedral sym metry. Application to low-temperature single crystal spectra demonstrates that (i) the semi-empiri-cal ligand field theory reproduces transition energies with sufficient accuracy; (ii) differences in the values of 10 Dq and B observed with different fitting methods may be attributed to the in-accuracy of experimental data; (iii) there are generally valid values of B35 and /?33 for each com-plex ion. 
  Reference    (Z. Naturforsch. 27b, 1—5 [1972]; received September 28 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0001.pdf 
 Identifier    ZNB-1972-27b-0001 
 Volume    27 
2Author    H. Breuer, H.-H PerkampusRequires cookie*
 Title    Auswertung nmr-spektroskopischer Messungen der Mischassoziation yon Nucleosid-Derivaten bei vergleichbaren Konzentrationsverhältnissen Evaluation of NMR-spectroscopical Results about Co-association of Nucleoside Derivatives in Comparable Concentrations  
 Abstract    In this paper we described a method how to calculate from NMR the association — caused by H-bonds — of two components. These components may be present in equal concentration and may be partially self-associated. The may act as H-donors and acceptors. The method is demonstrated using some nucleoside derivatives as examples. 
  Reference    (Z. Naturforsch. 27b, 6—12 [1972]; eingegangen am 31. August 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0006.pdf 
 Identifier    ZNB-1972-27b-0006 
 Volume    27 
3Author    H. Breuer, H.-H PerkampusRequires cookie*
 Title    Untersuchungen über die Mischassoziation einiger Nucleosid- Derivate in Lösung Investigations about Co-association of some Nucleoside-derivatives in Solution  
 Abstract    The co-assoziation of four nucleoside-derivatives was investigated using NMR spectroscopy. It turned out that the constant of co-association is at least ten times as great as the value for self-assoziation it a Watson-Crick pair was used. Thermodynamic data were calculated from the temperature dependence of the assoziation constant. 
  Reference    (Z. Naturforsch. 27b, 12—21 [1972]; eingegangen am 31. August 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0012.pdf 
 Identifier    ZNB-1972-27b-0012 
 Volume    27 
4Author    B. Krebs, R. MattesRequires cookie*
 Title      
 Abstract    The Raman and infrared spectra of Mo03-2H,0 and Mo02Cl2-H20 have been assigned based on the known crystal structures of these compounds. In the region of the Mo — O-stretching frequencies the spectra of Mo03-2H20 and MO02C12 or W02C12 are very similar. The same is valid for MO02C12'H20 compared with Mo03 . The frequency ras(Mo —O —Mo) depends highly on the ratio of the bond lengths of the two bridge bonds. 
  Reference    (Z. Naturforsch. 27b, 22—25 [1972]; eingegangen am 14. Oktober 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0022.pdf 
 Identifier    ZNB-1972-27b-0022 
 Volume    27 
5Author    J. Dayal, R. C. MehrotraRequires cookie*
 Title    Aluminium Derivatives of Tridentate Bifunctional Schiff Bases Derived from Salicylaldehyde and Benzoylacetone  
 Abstract    Aluminium derivatives of tridentate bifunctional Schiff bases (general formula SBH,, where I S = salicylaldehyde and benzoylacetone and B = (CH2 —)2, —CH2—CH —CH3 and C6H5) in different stoichiometric ratios have been synthesised. The products Al(OPr') (SB) are soluble in benzene. The tertiary butoxy products have been prepared by the alcohol interchange technique. Infrared spectra of the new derivatives are reported. Thermogravimetric analyses have also been carried out. 
  Reference    (Z. Naturforsch. 27b, 25—29 [1972]; received September 22 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0025.pdf 
 Identifier    ZNB-1972-27b-0025 
 Volume    27 
6Author    M. Dizdaroglu, H. Scherz, C.Von SonntagRequires cookie*
 Title      
 Abstract    In the y-radiolysis of N20 saturated aqueous solutions of meso-erythritol (10~ 2 mol/1) the fol-lowing products (G-values) are formed: erythrose (1) (1.3), erythrulose (2) (1.4), 2-deoxy-tetrose (3) (0.70), butanediol-(3,4) -on-(2) (4) (0.75), butanediol-(l,4)-on-(2) (5) (~0.1), glycerol alde-hyde (6) (~0.1), glycol aldehyde (?) (7) (<0.1) and dimers (8) (0.45). The formation of the products can be explained by the attack of the water radicals ('OH and 'H) on the meso-erythritol to give primarily meso-erythritol radicals. These radicals may disproportionate (products: 1 and 2), eliminate water, or fragment. The dimers 8 and the products 3 — 5 contain deoxy-groups attached to a carbonyl function. Their precursors are meso-erythritol radicals which have split off water before dimerization or disproportionation. 6 and 7 seem to arise from /^-fragmentation processes of the primary meso-erythritol radicals. 
  Reference    (Z. Naturforsch. 27b, 29 [1972]; eingegangen am 23. August 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0029.pdf 
 Identifier    ZNB-1972-27b-0029 
 Volume    27 
7Author    C. V. SonntagRequires cookie*
 Title    85 nm Photolyse von Isopropanol und seiner Mischungen mit Wasser und «-Hexan 185 nm Photolysis of Isopropanol and its Mixtures with Water and n-Hexane  
 Abstract    In the 185 nm photolysis of liquid 02-free isopropanol the following products (quantum yields) are formed: hydrogen (0.75), acetone (0.72), pinacol (0.036), methane (0.046), acetaldehyde (0.04), propane (0.02"), r ..ane (0.0023) and carbon monoxide (0.0015). A detailed reaction scheme is proposed. The major primary processes are the formation of H-atoms by homolytic scission of the O — H-bond (61 — 69%), elimination of molecular hydrogen (21%) and molecular methane (5%). <?(H2) is strongly decreased by adding water which does not absorb an appreciable portion of the 185 nm light in the mixtures down to 1 mole/1 iso-propanol ($(H2) =0.21). In contrast to the strong effect of water there is no effect on <£(H,) by diluting isopropanol with n-hexane. From experiments with isopropanol-OD and 2-deutero-isopro-panol it is tentatively concluded that H-atoms stemming from the O — H-group of the alcohol are to about 65% the precursors of the hydrogen in these mixtures. 
  Reference    (Z. Naturforsch. 27b, 41—16 [1972]; eingegangen am 23. August 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0041.pdf 
 Identifier    ZNB-1972-27b-0041 
 Volume    27 
8Author    D. L. Mathur, G. V. BakoreRequires cookie*
 Title    Kinetics of Oxidation of Cyclohexanol by Ceric Ammonium Nitrate in Aq. HNOa  
 Abstract    The oxidation of cyclohexanol by ceric ion has been studied in the presence of nitric acid ( ~ 1 — 2.5 M). The rate dependence on alcohol suggests intermediate complex formation. The increase in hydrogen ion and nitrate ion concentrations retards the rate of oxidation. The results have been explained on the basis of Ce(OH)3®, as the reactive species. The value of Kh for the equilibrium Ce4 ©+H2 0 Ce(OH)3® + H© has been evaluated as 4.8 at 25 °C in nitric acid medium. A mechanism based on decomposition of Ce (IV)-alcohol complex and rupture of a-carbon hydrogen bond in the rate determining step has been put forward. 
  Reference    (Z. Naturforsch. 27b, 46—2450 [1972]) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0046.pdf 
 Identifier    ZNB-1972-27b-0046 
 Volume    27 
9Author    Herbert Schriefers, Rüdiger Ghraf, Birgit LehnenRequires cookie*
 Title    stendion-Verbindungen durch die mikrosomale UDP-Glucuronyl- Transferase der Rattenleber Glucuronidation of Hydroxy-compounds of Testosterone and Androstenedione by the Microsomal UDP Glucuronyl Transferase of Rat Liver  
 Abstract    The microsomal UDP glucuronyl transferase exhibits activities against hydroxy derivatives of androstenedione (hydroxyl groups in the positions 2/?, 6ß or 16a) between 5% and 21% of the extent shown against testosterone. 2ß-, 6ß-and 16a-hydroxyl groups are much less efficient in ac-cepting the glucuronic acid than the 17/Miydroxyl group. However, the acceptor function of the 17/?-hydroxyl group is restricted by other hydroxy sub-stituents in the testosterone molecule to an increasing extent represented by the following sequence: 2a, 6ß, 6a, 16a, and 7a. A special case is represented by 2/?-hydroxy-testosterone. The transferase displays a higher activity against this compound than against testosterone. Apparently the transferase approaches the steroid molecule from the a-side (with the /?-side there is also contact at the C-6 atom) requires the 17/?-hydroxyl group and the 3-oxo-4-ene system to display full activity. Thus the very high specificity of the transferase for testosterone explains the selective action of this enzyme on testosterone metabolism in the liver. This action is expressed by the fact, that in liver perfusates the percentage of testosterone in the glucuronide fraction is twice as large as the percentage of testosterone in the free steroid fraction. 
  Reference    (Z. Naturforsch. 27b, 49—52 [1972]; eingegangen am 13. August 1971. revidiert am 7. November 1971) 
  Published    1972 
  Keywords    Hydroxy-testosteron, Hydroxy-androstendion, Glucuronidierung UDP-Glucuronyl-Transferase, Substratspezifität 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0049.pdf 
 Identifier    ZNB-1972-27b-0049 
 Volume    27 
10Author    P. Pohl, H. WagnerRequires cookie*
 Title    Control of Fatty Acid and Lipid Biosynthesis in Euglena gracilis by Ammonia, Light and DCMU  
 Abstract    When Euglena gracilis was grown under white (fluorescent) light in media containing high concentrations of ammonium chloride (more than 0.005%), the main lipids synthesized were mono-galactosyl diglyceride, digalactosyl diglyceride, phosphatidyl glycerol, sulfolipid and the all eis 47,10-16:2, 47,10,13-16:3, Zl4,7,10,13-16:4, A9,12-18:2 and A9,12,15-18:3 fatty acids. At low levels of ammonium (less than 0.002%) these compounds were produced only in small amounts, while neutral lipids, phosphatidyl choline, phosphatidyl ethanolamine and the 14:0, 16:0 and 16:1 fatty acids predominated. When Euglena gracilis was grown in white light in the presence of dichlorophenyldimethylurea (DCMU) or in the dark, fatty acid and lipid biosyntheses followed the same pattern as in white light at low levels of ammonium. Similar results were obtained when nitrate served as the only nitrogen source in the light and in the dark. The results indicate that in Euglena gracilis there are a light independent and a light and ammonium dependent pathway of fatty acid biosynthesis. Both pathways seem to be in association with specific lipids. 
  Reference    (Z. Naturforsch. 27b, 53—61 [1972]; received October 9 1971 revised November 2 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0053.pdf 
 Identifier    ZNB-1972-27b-0053 
 Volume    27 
11Author    G. Pilwat, U. ZimmermannRequires cookie*
 Title    Potassium Transport in Escherichia coli B II. Dependence of the Intracellular Steady-state Potassium Concentration upon the Extracellular Potassium and Sodium Concentrations in E. coli B 525  
 Abstract    The stationary intracellular potassium concentration in E. coli B 525 has been studied as a function of the extracellular potassium and sodium concentrations. The ratio of extracellular to intracellular potassium concentration is shown to be a linear function of the extracellular potassium concentration if the extracellular sodium concentration is low (20 mmoles/1). In the case of high sodium concentration (100 mmoles/1) the ratio is indepen-dent of the extracellular potassium concentration if the potassium concentration is below 1,2 mmoles/1. In order to describe the distribution of potassium uniformly over the whole range of the extra-cellular potassium and sodium concentrations a carrier system with two sites has to be supposed. 
  Reference    (Z. Naturforsch. 27b, 62—67 [1972]; eingegangen am 3. April 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0062.pdf 
 Identifier    ZNB-1972-27b-0062 
 Volume    27 
12Author    Hans Hammerl, Walter KlingmüllerRequires cookie*
 Title    Influence of UV-Light on Gene-Conversion in Neurospora  
 Abstract    1. Crosses between wild type (dark ascospores) and the asco-mutant (light ascospores) were set up and the spores collected as unordered octads. The analysis of 1317 such octads revealed 69 with abnormal segregation of the asco-marker (5.2%). If crosses were irradiated with UV at a dose equivalent to 66% conidial killing, an increase of the number of aberrant octads was found. This increase was most pronounced if the crosses were exposed to the irradiation from one day before to 2 days after plasmogamy, when up to 8.7% aberrant octads were obtained. No effect was observed from 4 days after plasmogamy until the end of the sexual cycle. 2. The relative frequency of the 8 possible types of aberrant octads was analyzed separately for experiments without and for experiments with UV-irradiation. The distribution of these fre-quencies was the same for unirradiated and irradiated crosses, a finding which suggests that the conversion mechanism acting spontaneously and that acting upon UV-irradiation may be identical. In both cases, there was a strong bias in favour of octads of the 2 : 6 type (giving wild spores first) as compared to such of the 6: 2 type, also the frequency of the 0 : 8 type was higher than that of the 8 : 0 type. Hence, the conversion mechanism in this cross "prefers" to act from the wildtype to the mutant allele. 
  Reference    (Z. Naturforsch. 27b, 68—72 [1972]; received September 16 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0068.pdf 
 Identifier    ZNB-1972-27b-0068 
 Volume    27 
13Author    M. C. Bhandari, D. N. SenRequires cookie*
 Title    Growth Regulation Specificity Exhibited by Substances Present in the Fruit Pulp of Citrullus lanatus (Thunb.) Mansf  
 Abstract    The specific effect of the extract from the fruit pulp of Citrullus lanatus was demonstrated on the seed germination and seedling growth of Citrullus lanatus, Citrullus colocynthis and Penni-setum typhoideum. The extract from C. lanatus inhibited the germination of its own seeds, but promoted that of the other two species. The promoting substance for the growth of root and shoot was found at Rf 0.66. 
  Reference    (Z. Naturforsch. 27b, 72—75 [1972]; received June 5 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0072.pdf 
 Identifier    ZNB-1972-27b-0072 
 Volume    27 
14Author    E. Schwarzmann, U. R. BirkenbergRequires cookie*
 Title    Hydrothermale Synthese von VO(OH) Hydrothermal Synthesis of VO (OH)  
 Abstract    Bei der hydrothermalen Behandlung eines Gemisches von VHj.3 und V205 in einem der Oxidationsstufe von dreiwertigem Vanadin entsprechenden Verhältnis ent-steht VO (OH). Dieses Hydroxid kristallisiert in der Raumgruppe Pbnm und ist isostrukturell mit Diaspor AlO (OH) K Aus früheren Veröffentlichungen geht hervor, daß bei der Zugabe von Lauge zu V(III)-salzlösungen ein flockiger amorpher grüner Niederschlag von V (III) -oxidhydrat sich bildet, der infolge Oxidation rasch braun wird und noch nicht charakterisiert worden ist 2 . Auf hydrothermalem Wege gelang es nun erstmalig, ein kristallines V(III)-hydroxid zu erhalten. Zur Dar-stellung von VO(OH) wird V205 (reinst, Merck) und VHi.3 (Alfa Inorganics) in einem der Oxidationsstufe von dreiwertigem Vanadin entsprechenden Verhältnis sehr sorgfältig gemischt und unter Luftausschluß in 
  Reference    (Z. Naturforsch. 27b, 76 [1972]; eingegangen am 5. November 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0076a_n.pdf 
 Identifier    ZNB-1972-27b-0076a_n 
 Volume    27 
15Author    E. Schwarzmann, U. R. BirkenbergRequires cookie*
 Title    Hydrothermale Synthese von VO(OH) Hydrothermal Synthesis of VO (OH)  
 Abstract    Bei der hydrothermalen Behandlung eines Gemisches von VHj.3 und V205 in einem der Oxidationsstufe von dreiwertigem Vanadin entsprechenden Verhältnis ent-steht VO (OH). Dieses Hydroxid kristallisiert in der Raumgruppe Pbnm und ist isostrukturell mit Diaspor AlO (OH) K Aus früheren Veröffentlichungen geht hervor, daß bei der Zugabe von Lauge zu V(III)-salzlösungen ein flockiger amorpher grüner Niederschlag von V (III) -oxidhydrat sich bildet, der infolge Oxidation rasch braun wird und noch nicht charakterisiert worden ist 2 . Auf hydrothermalem Wege gelang es nun erstmalig, ein kristallines V(III)-hydroxid zu erhalten. Zur Dar-stellung von VO(OH) wird V205 (reinst, Merck) und VHi.3 (Alfa Inorganics) in einem der Oxidationsstufe von dreiwertigem Vanadin entsprechenden Verhältnis sehr sorgfältig gemischt und unter Luftausschluß in 
  Reference    (Z. Naturforsch. 27b, 76 [1972]; eingegangen am 5. November 1971) 
  Published    1972 
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 Identifier    ZNB-1972-27b-0076b_n 
 Volume    27 
16Author    F. Seel, W. Gombler, U. R. BudenzRequires cookie*
 Title    Ergebnisse der Umsetzung von Chlorsulfen- säuredialkylamiden mit Silber-und Queck- silber(II)-fluorid Results of the Reaction of Chlorosulfenic Acid Dialkylamides with Silver and Mercury (II) Fluoride  
 Abstract    Wenn man die Dämpfe des Chlörsulfensäuredime-thylamids und -diäthylamids 1 bei niederen Drucken durch eine auf 120° erwärmte Säule von Silberfluorid leitet, entstehen als einzige Produkte die entsprechen-den Fluorsulfensäureamide, FSNR2 (R = CH3 bzw. C2H5); die Umsetzung mit Quecksilber (II) -fluorid bei 100° ergibt jedoch als Hauptprodukte Alkylimino-schivefeldifluoride, RNSF2. Fluorsulfensäuredialkyl-amide zersetzen sich in Glasgefäßen sehr rasch in Fluorsulfinsäuredialkylamide und Tetraalkyldiamino-disulfane: 
  Reference    (Z. Naturforsch. 27b, 78—79 [1972]; eingegangen am 10. November 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0078_n.pdf 
 Identifier    ZNB-1972-27b-0078_n 
 Volume    27 
17Author    Requires cookie*
 Title    Berichtigung  
 Abstract    Versuche, Ester der Fluorsulfensäure auf dem Wege ROSSOR — ROSC1 AgF ' Hg -ROSF darzustellen, blieben bis jetzt ohne Erfolg. Eine noch-malige Überprüfung der Konproportionierung S(OR)2 + S2F2FSOR + FS2OR zeigte, daß auch diese Um-1 Die Ausgangsprodukte wurden durch Umsetzung der Disul-fide R2NSSNR2 mit Sulfurylchlorid gewonnen. (Vgl. hierzu E. KÜHLE, Synthesis 1970, 560.) 2 B. COHEN U. A. G. MCDIARMID, J. chem. Soc. [London] A, 
  Reference    (Z. Naturforsch. 27b, 79 [1972]) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0079_n.pdf 
 Identifier    ZNB-1972-27b-0079_n 
 Volume    27 
18Author    H.-U Schuster, U. C., -J KistrupRequires cookie*
 Title    Die ternären Phasen Li2MnGe und Li2MnSn The Ternary Phases Li2MnGe and Li2MnSn  
 Abstract    In den Dreistoffsystemen Li — Mn — X mit X = Si, Ge, Sn oder Pb wurden Versuche zur Darstellung ter-närer Phasen der Stöchiometrie Li2MnX, LiMn2X und anderer Zusammensetzungen durchgeführt. Bei den Ver-suchen wurden entweder Gemenge der Elemente einge-setzt, oder es wurde von Pulvern vorher erschmolzener binärer Phasen des Mangans mit einem Element der 4. Hauptgruppe ausgegangen, die dann in Lithium-schmelze oder im Lithiumdampf erhitzt wurden. Zwei offenbar isotype tetragonale Phasen der Zusam-mensetzung Li2MnX konnten mit X = Ge bzw. Sn dar-gestellt werden. Zur Synthese wurden die Element-gemenge in Tantaltiegeln unter Argon zunächst 12 Stdn. auf etwa 700 °C vorerhitzt, dann zur Homo-genisierung zerrieben und gründlich vermengt und noch einmal mehrere Stdn. auf 850 °C (Li2MnGe) bzw. 780 °C (Li2MnSn) nacherhitzt. Die spröden metallisch grauen Präparate wurden an-schließend aus dem Tiegel gefräst. Ihre Pulver sind extrem feuchtigkeitsempfindlich, so daß alle Arbeiten am Präparat unter scharf getrocknetem Argon durch-geführt werden mußten. Zur Analyse wurden die Phasen in Mineralsäuren gelöst; das Lithium wurde flammenphotometrisch, das Mangan manganometrisch, das Zinn gravimetrisch als 
  Reference    (Z. Naturforsch. 27b, 80 [1972]; eingegangen am 21. Oktober 1972) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0080_n.pdf 
 Identifier    ZNB-1972-27b-0080_n 
 Volume    27 
19Author    H.-U Schuster, G. SchroederRequires cookie*
 Title    Neue ternäre Phasen des Lithiums und der 2. Nebengruppe mit Elementen der 5. Haupt- gruppe New Ternary Phases of Lithium with Elements of the 2b-Group and the 5b-Group  
 Abstract    In Erweiterung unserer Untersuchungen an ternären Lithiumverbindungen der 2. Nebengruppe mit Elemen-ten der 4. Hauptgruppe 1-3 haben wir auch Versuche mit Elementen der 5. Hauptgruppe durchgeführt. Eine Reihe entsprechender Magnesium-und Zinkverbindun-gen dieser Gruppe sind durch die Arbeiten von JuZA 
  Reference    (Z. Naturforsch. 27b, 81—82 [1972]; eingegangen am 26. Oktober 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0081_n.pdf 
 Identifier    ZNB-1972-27b-0081_n 
 Volume    27 
20Author    Hans-Dieter HausenRequires cookie*
 Title    Zur Kristall-und Molekülstruktur von Diäthylindium-Thioacetat Crystal and Molecular Structure of Diethylindium- thioacetate  
 Abstract    Durch Umsetzung von Triäthylindium mit Thioessig-säure erhielt WEIDLEIN 1 farblose Kristalle der Zusam-mensetzung (C2H5) 2InOSC — CH3 . Aufgrund IR-und Raman-spektroskopischer Untersuchungen schlug der genannte Autor monomere Vierring-Einheiten vor. 
  Reference    (Z. Naturforsch. 27b, 82—83 [1972]; eingegangen am 23. Oktober 1971) 
  Published    1972 
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 TEI-XML for    default:Reihe_B/27/ZNB-1972-27b-0082_n.pdf 
 Identifier    ZNB-1972-27b-0082_n 
 Volume    27 
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